• Transactions of Materials Processing
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• v.25 no.2
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• pp.96-101
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• 2016

The current study was conducted to elucidate the effect of cementite morphology and matrix-ferrite microstructure on sliding wear behavior in spheroidized high carbon (1wt. % C) steel. The high carbon steel was initially heat treated to obtain a full pearlite or a martensite microstructure before the spheroidization. The spheroidizing heat treatment was performed on the full pearlitic steel for 100 hours at 700℃ and tempering was performed on the martensitic steel for 3 hours at 650℃. A spheroidized cementite phase in a ferrite matrix was obtained for both the full pearlite and the martensite microstructures. Sliding wear tests were conducted using a pin-on-disk wear tester with the heat treated steel as the disk specimen. An alumina(Al₂O₃) ball was used as the pin counterpart during the test. After the spheroidizing heat treatment and the tempering, both pearlite and martensite exhibited similar microstructures of spheroidized cementite in a ferrite matrix. The spheroidized pearlite specimens had lower hardness than the tempered martensite; however, the wear resistance of the spheroidized pearlite was superior to that of the tempered martensite.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.6 no.1
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• pp.45-50
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• 1997

It is not clearly known how surface defects or inclusions of a medium carbon steel affect a fatigue strength. In this study, we used SM35C specimens with spheroidized cementite structure to eliminate dependence of micro structure of fatigue crack. The investigation was carried out by behavior of crack closure at non-propagation crack and effect of the fatigue limit according to the artificial defects size. Experimental findings are obtained as follows : (1) Fatigue crack initiation point of medium carbon steel with spheroidized cementite structure is at the surface defects. (2) Non-propagating crack length of smooth specimen is equal to the critical size of defect. (3) Considering the opening and closure behavior of fatigue crack, the defect shape results in various crack opening displacement, while it does not affects the fatigue limit level of medium carbon steel with spheroidized cementite structure. (4) The critical length of the non-propagation crack of smooth specimen is the same as critical size of defect in transient area which determines threshold condition in steel with spheroidized cementite structure.

• Transactions of Materials Processing
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• v.21 no.6
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• pp.354-359
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• 2012

Effects of a nitriding treatment on the tensile and high cycle fatigue properties were investigated by conducting ion-nitriding and gas nitro-caburizing treatments on the spheroidized SCr430B medium-carbon steel and performing tensile and tension-tension high cycle fatigue tests. The nitrided samples showed much lower strength and ductility compared to those in the initial as-spheroidized state and premature fracture occurred at the hardened layers. The micro-voids in the compound layer caused fatigue crack initiation. Thus, the removal of the compound layer with micro-voids remarkably improved the fatigue resistance to even beyond that of the as-spheroidized sample.

• Transactions of the Korean Society of Mechanical Engineers
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• v.12 no.2
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• pp.278-285
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• 1988

The Critical size of artificially induced micro-holes in 0.17%, 0.36% Carbon steel Specimens with Spheroidized Cementite and in 0.17% carbon steel specimens with martensite structure is compared with annealed pre-crack in order to discuss the physical meaning of the fatigue limit and evaluation of the tolerant micro flaw size at the stress level of the fatigue limit. Results obtained were summarized as follows; (1) In this study, non-propagating crack length of Smooth specimen and critical pre-crack length (lc) is coincide. (2) In the carbon steels with spheroidized cementite structure, critical pre-crack length (lc) and allowable micro-hole size (dc) is coincide each other at the fatigue limit level. (3) It has been published that there exists a particular size of micro-hole which has no effect on the fatigue limit. In this study, the micro-hole of critical size can be regarded as equivalent to a tolerant micro flaw which would not reduce the fatigue limit.

• Journal of the Korean Society for Heat Treatment
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• v.19 no.5
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• pp.270-279
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• 2006

The effects of eight types of spheroidizing annealing conditions including annealing temperature, annealing time, cooling rate, and furnace atmosphere on the microstructure and hardeness were determined in SCM440 steel which has been widely used for automotive parts. The well-spheroidized structure and minimum hardness were obtained when the steel was heat-treated at $770^{\circ}C$ for 6 hours, cooled to $720^{\circ}C$ at a cooling rate of $24^{\circ}C/h$, and then kept for 7 hours at the $720^{\circ}C$ followed by air cooling. In order to increase the productivity and to save the manufacturing cost, it is desirable to apply a faster cooling rate to the spheroidizing annealing. It was found that a cooling rate of $100^{\circ}C/hr$ was the fastest cooling rate applicable to the SCM440 steel among the four cooling rates used in this study. The microstructure consisted of ferrite and very fine spheroidized cementite when the steel was annealed for 13 hours at $720^{\circ}C$ below $A_{C1}$ temperature. This was caused by the short annealing time and the retarding effect of Cr and Mo on both the dissolution of pearlite to cementite and coarsening of spheroidized cementite. The steel heat treated in air showed the decarburized layer of about $125{\mu}m$ in thickness at the surface.

• Journal of Powder Materials
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• v.26 no.4
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• pp.305-310
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• 2019

In the present work, spheroidization of angular vanadium powders using a radio frequency (RF) thermal plasma process is investigated. Initially, angular vanadium powders are spheroidized successfully at an average particle size of $100{\mu}m$ using the RF-plasma process. It is difficult to avoid oxide layer formation on the surface of vanadium powder during the RF-plasma process. Titanium/vanadium/stainless steel functionally graded materials are manufactured with vanadium as the interlayer. Vanadium intermediate layers are deposited using both angular and spheroidized vanadium powders. Then, 17-4PH stainless steel is successfully deposited on the vanadium interlayer made from the angular powder. However, on the surface of the vanadium interlayer made from the spheroidized powder, delamination of 17-4PH occurs during deposition. The main cause of this phenomenon is presumed to be the high thickness of the vanadium interlayer and the relatively high level of surface oxidation of the interlayer.

• Journal of Korea Foundry Society
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• v.21 no.6
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• pp.328-335
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• 2001

The objective of this study is to investigate on manufacturing Al-scrap into hypereutectic Al-Si alloy by using electromagnetic force. The Fe element in the aluminium scrap was controlled by intermetallic compound method and using EMF(electromagnetic force). The most lumped compound was found after 10min holding at $690^{\circ}C$. A number of segregated compound was revealed when imposed to EMF at 30A. The refinement of primary Si particles was achieved by EMF stirring. Primary Si particles were refined and spheroidized most of all with the magnetic intensity of 180G for 10 min.

• Journal of Powder Materials
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• v.28 no.2
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• pp.97-102
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• 2021

Powder quality, including high flowability and spherical shape, determines the properties of additively manufactured products. Therefore, the cheap production of high-quality powders is critical in additive manufacturing. Radio frequency plasma treatment is an effective method to fabricate spherical powders by melting the surface of irregularly shaped powders; in the present work, mechanically milled Zr powders are spheroidized by radio frequency plasma treatment and their properties are compared with those of commercial Zircaloy-2 alloy powder. Spherical Zr particles are successfully fabricated by plasma treatment, although their flowability and impurity contents are poorer than those of the commercial Zircaloy-2 alloy powder. This result shows that radio-frequency plasma treatment with mechanically milled powders requires further research and development for manufacturing low-cost powders for additive manufacturing.

• Korean Journal of Materials Research
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• v.28 no.3
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• pp.174-181
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• 2018

Three kinds of STS304-Zr alloys were fabricated by varying the Zr content, and their microstructure and fracture properties were analyzed. Moreover, we performed heat treatment to improve their properties and studied their microstructure and fracture properties. The microstructure of the STS304-Zr alloys before and after the heat treatment process consisted of ${\alpha}-Fe$ and intermetallics: Zr(Cr, Ni, Fe)2 and Zr6Fe23. The volume fraction of the intermetallics increased with an increasing Zr content. The 11Zr specimen exhibited the lowest hardness and fine dimples and cleavage facets in a fractured surface. The 15Zr specimen had high hardness and fine cleavage facets. The 19Zr specimen had the highest hardness and large cleavage facets. After the heat treatment process, the intermetallics were spheroidized and their volume fraction increased. In addition, the specimens after the heat treatment process, the Laves phase (Zr(Cr, Ni, Fe) 2) decreased, the Zr6Fe23 phase increased and the Ni concentration in the intermetallics decreased. The hardness of all the specimens after the heat treatment process decreased because of the dislocations and residual stresses in ${\alpha}-Fe$, and the fine lamellar shaped eutectic microstructures changed into large ${\alpha}-Fe$ and spheroidized intermetallics. The cleavage facet size increased because of the decomposition of the fine lamellar-shaped eutectic microstructures and the increase in spheroidized intermetallics.

• Tribology and Lubricants
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• v.16 no.4
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• pp.253-258
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• 2000

Frictional behavior of wire electric discharge machined surfaces of spheroidized annealed STDll steel was investigated. The surfaces were produced with a various series of finish cuts where pulse energy was reduced with increase in the number of finish cuts. Roughness and micro-hardness of the surfaces were also measured. It is observed that the increase in the number of finish cuts produces the surface exhibiting lower frictional resistance followed by higher resistance after considerable wear. Effects of finish cuts on the friction characteristics are discussed with the aid of roughness and micro-hardness of the surfaces.