• Title/Summary/Keyword: Spherical Material

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Spark Plasma Sintering and Ultra-Precision Machining Characteristics of SiC

  • Son, Hyeon-Taek;Kim, Dae-Guen;Park, Soon-Sub;Lee, Jong-Hyeon
    • Korean Journal of Materials Research
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    • v.20 no.11
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    • pp.559-569
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    • 2010
  • The liquid-phase sintering method was used to prepare a glass lens forming core composed of SiC-$Al_2O_3-Y_2O_3$. Spark plasma sintering was used to obtain dense sintered bodies. The sintering characteristics of different SiC sources and compositions of additives were studied. Results revealed that, owing to its initial larger surface area, $\alpha$-SiC offers sinterability that is superior to that of $\beta$-SiC. A maximum density of $3.32\;g/cm^3$ (theoretical density [TD] of 99.7%) was obtained in $\alpha$-SiC-10 wt% ($6Al_2O_3-4Y_2O_3$) sintered at $1850^{\circ}C$ without high-energy ball milling. The maximum hardness and compression stress of the sintered body reached 2870 Hv and 1110 MPa, respectively. The optimum ultra-precision machining parameters were a grinding speed of 1243 m/min, work spindle rotation rate of 100 rpm, feed rate of 0.5 mm/min, and depth of cut of $0.2\;{\mu}m$. The surface roughnesses of the thus prepared final products were Ra = 4.3 nm and Rt = 55.3 nm for the aspheric lens forming core and Ra = 4.4 nm and Rt = 41.9 for the spherical lens forming core. These values were found to be sufficiently low, and the cores showed good compatibility between SiC and the diamond-like carbon (DLC) coating material. Thus, these glass lens forming cores have great potential for application in the lens industry.

Double membrane-bound particles associated with eriophyid mite-borne plant diseases of unknown etiology : a potentially new group of plant viruses\ulcorner

  • Ahn, Kyung-Ku;Kim, Kyung-Soo
    • Proceedings of the Korean Society of Plant Pathology Conference
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    • 1997.06a
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    • pp.5-21
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    • 1997
  • Unique virus-like particles were associated with five eriophyid mite-borne plant diseases of unknown etiology; fig mosaic, redbud yellow ringspot, rose orsette, thistle mosaic, and high plains disease of corn and wheat. Quasi-spherical, double membrane-bound particles (DMPs), 120 - 200 nm in diameter, were observed in the cytoplasm of all cell types in symptomatic leaves of infected plants. No DMPs were observed in symptomless plants. The DMPs in symptomatic thistles were associated with two types of inclusions, electron-dense amorphous material and tubular aggregates. Similar amorphous inclusions were also found in corn and wheat with high plains disease, while tubular inclusions were observed in figs with mosaic symptoms. The particles and inclusions were similar in some aspects to immature particles associated with viroplasms of animal and insect poxviruses and also to the double-enveloped particles of tomato spotted wilt virus associated with viroplasms during early stages of infection, but were unique and unlike any known plant viruses. The DMPs and associated viroplasm-like inclusions in the high plains disease were specifically immunogold labeled in situ with the disease-specific antiserum. Thread-like structures, similar to tenuivirus particles, present in the partially purified virus preparations were also immunogold labeled with the antiserum. It is suggested that the thread-like structures are derived from the DMP. In many cells of symptomatic corn and wheat samples, DMPs occurred together with flexuous rod-shaped particles and cylindrical inclusions of wheat streak mosaic potyvirus (WSMV), suggesting that the disease is caused by a mixed infection of WSMV and the agent represented by the DMPs. Based on cytopathology, symptomatology and mite and/or graft-transmissibility, the five diseases described in this paper are potentially caused by virus(es) and the DMPs associated with these diseases may represent virus particles. If the DMPs are indeed viral in nature, they would comprise a new group of plant viruses.

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Surface Characteristics of Porous Ti-6Al-4V Implants Fabricated by Electro-Discharge-Sintering in a Low Vacuum Atmosphere (저진공 분위기 전기방전소결에 의해 제조된 다공성 Ti-6Al-4V 임플란트의 표면특성 연구)

  • Hyun, C.Y.;Huh, J.K.;Lee, W.H.
    • Korean Journal of Materials Research
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    • v.16 no.3
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    • pp.178-182
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    • 2006
  • A single electro-discharge-sintering (EDS) pulse (1.0 kJ/0.7 g), from a $300{\mu}F$ capacitor, was applied to atomized spherical Ti-6Al-4V powder in a low vacuum to produce porous-surfaced implant compacts. A solid core surrounded by a porous layer was formed by a discharge in the middle of the compact. XPS (X-ray photoelectron spectroscopy) was used to study the surface characteristics of the implant material. C, O, and Ti were the main constituents, with smaller amounts of Al, V, and N. The implant surface was lightly oxidized and was primarily in the form of $TiO_2$ with a small amount of metallic Ti. A lightly etched EDS implant sample showed the surface form of metallic Ti, indicating that EDS breaks down the oxide film of the as-received Ti-6Al-4V powder during the discharge process. The EDS Ti-6Al-4V implant surface also contained small amounts of aluminum oxide in addition to $TiO_2$. However, V detected in the EDS Ti-6Al-4V implant surface, did not contribute to the formation of the oxide film..

Electrochemical Study of Electrode Material of Ni-MH Battery for HEV and PEMFC Fuel Cell (HEV 및 PEMFC 연료전지용 니켈수소 전지의 전극재료에 대한 전기화학적 평가)

  • Kim, Ho-Sung
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.20 no.2
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    • pp.24-28
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    • 2006
  • Electrochemical hydrogenation/dehydrogenation properties were studied for a single particle of a Mm-based(Mm : misch metal) hydrogen storage alloy($MmNi_{3.55}Co_{0.75}Mn_{0.4}Al_{0.3}$) for the anode of Ni-MH batteries. A carbon fiber microelectrode was manipulated to make electrical contact with an alloy particle, and the cyclic voltammetry and the galvanostatic charge/discharge experiments were performed. A single particle of the alloy showed the discharge capacity of 280[mAh/g], the value being 90[%] of the theoretical capacity. Data were compared with that of the composite film consisting of the alloy particles and a polymer binder, which is more practical form for Ni-MH batteries. Additionally, pulverization of the alloy particles are directly observed. Compared with the conventional composite film electrodes, the single particle measurements using the microelectrode gave more detailed, true information about the hydrogen storage alloy.

Fabrication of Porous β-TCP Bone Graft Substitutes Using PMMA Powder and their Biocompatibility Study (PMMA를 이용한 다공질 β-TCP 골충진제 제조 및 생체적합성 평가)

  • Song, Ho-Yeon;Youn, Min-Ho;Kim, Young-Hee;Min, Young-Ki;Yang, Hun-Mo;Lee, Byong-Taek
    • Korean Journal of Materials Research
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    • v.17 no.6
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    • pp.318-322
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    • 2007
  • Porous ${\beta}-tricalcium$ phosphate $({\beta}-TCP)$ bioceramic was fabricated by pressureless sintering using commercial HAp and different volume percentages of PMMA powders (30-60 vol.%). The range of spherical pore size was about $200-250\;{\mu}m$ in diameter. By increasing the PMMA content, the number of pores and their morphology were dramatically changed as well as decreased the material properties. In case of using 60 vol.% PMMA content, network-type pores were found, due to the necking of the PMMA powders. The values of relative density, elastic modulus, bending strength and hardness of the 60 vol.% PMMA content sample, sintered at $1500^{\circ}C$, were about 46%, 22.2 GPa, 5MPa and 182 Hv respectively. Human osteoblast-like MG-63 cells and osteoclast-like Raw 264.7 cells were well grown and fully covered all of the porous ${\beta}-TCP$ bodies sintered at $1500^{\circ}C$.

Design of 4:1 I$\mathbb{R}$ zoom afocal telescope (원적외선 대역 4 : 1 줌 망원경 광학계 설계)

  • 김현숙;김창우;홍석민
    • Korean Journal of Optics and Photonics
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    • v.9 no.3
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    • pp.134-141
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    • 1998
  • A high performance afocal zoom telescope has been designed to operate in the 7.6${\mu}{\textrm}{m}$ to 10.3${\mu}{\textrm}{m}$ waveband for thermal imaging system. This IR zoom telescope is characterized by using of two movable optical element groups, variator and compensator, with mechanically compensated method and the positioning of these groups is controlled by means of a computerized program. The optical performance over the entire 4:1 zoom range and $\pm$2.31~$\pm$9.36 degrees field of view is near diffraction limit while maintaining a constant F-number. The all refracting surfaces of this system except only one aspheric surface are spherical curvature and the material for the optical elements is selected Ge and ZnSe which is used for correction of chromatic aberration.

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THE HISTOLOGIC STUDY OF THE GRAFTED hBMP-I FOR IMMEDIATE IMPLANT FIXATION (발치 후 즉시 임플란트 식립시 이식된 hBMP-I의 조직학적 고찰)

  • Lee, Eun-Young;Kim, Kyoung-Won;Choi, Hee-Won;Um, In-Woong;Chung, Ho-Yong
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.30 no.4
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    • pp.316-322
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    • 2004
  • A low molecular weight component named bone morphogenetic protein(BMP) chemically isolated from the organic matrix of bone, induce postfetal connective tissue cells surrounding small blood vessels to differentiate into cartilage and bone. The end product of BMP is a spherical ossicle of lamella bone filled with red bone marrow for the functional loading. This is a important point that the graft material is embedded the defect site during the implant surgery. Because present knowledge of the relationship between BMP and bone regeneration arises mainly from studies of induced bone formation in heterotopic sites, it would be helpful to determine whether BMP plays any part in the process of bone healing. The BMPs have been shown to play crucial roles in normal skeletal development as well as bone healing and are able to activate transcription of genes involved in cellular migration, proliferation, and differentiation. The delivery of BMP on matrices has been efficacious in the treatment of defect bone in implant surgery. The purpose of the histologic study was to evaluate the effect of DLB(demineralized lyophilized bone) coated with purified human BMP(hBMP-I) in immediate implant surgery with bony defect to obtain the functional structure of implant asap. The ability of a graft of hBMP-I to accelerate bony defect repair provides a rationale for its use in immediate implant surgery that have large bone defect in edentulous area.

The effect of thickness on luminous properties of ceramic phosphor plate for high-power LD (고출력 LD 용 형광체 세라믹 플레이트의 두께에 따른 광학 특성)

  • Ji, Eun Kyung;Lee, Chul Woo;Song, Young Hyun;Jeong, Byung Woo;Jung, Mong Kown;Yoon, Dae-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.2
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    • pp.80-83
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    • 2016
  • In the present paper, garnet structured $Y_3Al_5O_{12}:Ce^{3+}$ (YAG : Ce) ceramic phosphor plate (CPP) for high power laser diode (LD) was prepared and optical properties were analyzed. We synthesized monodispersed spherical nano-sized YAG : Ce particles by liquid phase method, fabricated phosphor ceramic plate with the addition of $Al_2O_3$. $75{\mu}m$ and $100{\mu}m$ thick YAG : Ce CPPs were compared in terms of the factors of conversion efficacy, thermal quenching, luminance and correlated color temperature (CCT). In conclusion, conversion efficacy decreased by 25 % in both samples and $100{\mu}m$ thick sample provides better optical properties of thermal quenching, maximum light conversion efficacy and maximum luminance value.

Measurement and Analysis of Conduction Noise through Microstrip Line Attached with Composite Sheets of Iron Particles and Rubber Matrix (마이크로스트립 전송선로를 이용한 순철 압분체-고무 복합재의 전도노이즈 흡수특성 측정 및 해석)

  • Kim, Sun-Tae;Oh, Byung-Ki;Kim, Sung-Soo;Cho, Han-Sin;Lee, Jae-Hee
    • Journal of the Korean Magnetics Society
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    • v.14 no.5
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    • pp.174-179
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    • 2004
  • Attenuation of conduction noise through microstrip line attached with the high lossy iron flakes-rubber composites has been investigated in GHz frequencies. Microstrip line was designed with characteristic impedance of 50 $\Omega$ and a length corresponding to the center frequency of 3 GHz. Iron flakes were fabricated by mechanical forging of spherical iron powders using an attrition mill. The fabricated microstrip line shows a ideal propagation characteristics of S$\sub$11/ < -60 dB and S$\sub$21/ = 0 dB. Attaching a noise absorbing sheet on the microstrip line, S$\sub$11/ increases to about -10 dB and S$\sub$21/ decreases to -20~-60 dB depending on the length of absorbing sheet. The calculated power loss is as high as 80% in the frequency range 2~8 GHz. It is suggested that the most critical material parameter is magnetic loss for the enhancement of noise attenuation.

Analysis of High Velocity Impact on SFRC Panels Using ABAQUS (ABAQUS를 이용한 강섬유보강 콘크리트 패널의 고속 충돌 거동 해석)

  • Son, Seok-Kwon;Jang, Seok-Joon;Yun, Hyun-Do;Kim, Yong-Hwan
    • Journal of the Korea Concrete Institute
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    • v.28 no.2
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    • pp.141-148
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    • 2016
  • This paper employed finite element method (FEM) to study the dynamic response of Steel Fiber-Reinforced Concrete(SFRC) panels subjected to impact loading by spherical projectiles. The material properties and non-linear stress-strain curves of SFRC were obtained by compression test and flexural test. Various parametric studies, such as the effect of fiber volume fraction and thickness of panels, are made and numerical analyses are compared with experiments conducted. It is shown that protective performance of concrete panels will be improved by adding steel fiber. Area loss rates and weight loss rates are decreased with increasing fiber volume fraction. Also, penetration modes can be expected by FEM, showing well agreement with experiment. Results can be applied for designing the protection of military structures and other facilities against high-velocity projectiles.