• Title/Summary/Keyword: Spectrum Range

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Measurement of Quality Parameters of Honey by Reflectance Spectra

  • Park, Chang-Hyun;Yang, Won-Jun;Sohn, Jae-Hyung;Kim, Jong-Hoon
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1530-1530
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    • 2001
  • The objectives of this study were to develop models to predict quality parameters of Korean bee-honeys by visible and NIR spectroscopic technique. Two kinds of bee-honey fronl acacia and polyflower sources were tested in this study. The honeys were harvested in the spring of 2000 and stored in the storage facility at 20$^{\circ}C$ during experiments. Total of 394 samples of honey were analyzed. Reflectance spectra, moisture contents, ash, invert sugar, sucrose, F/G (fructose/glucose) ratio, HMF (hydroxymethyl furfural), and C12/C13 ratio of honeys were measured. The average values for the tested honeys were 19.9% of moisture contents, 0.12% of ash, 68.4% of invert sugar, 5.7% of sucrose, 1.27 of F/G(fructose/glucose) ratio, 14.4 mg/kg of HMF, and -19.1 of C12/C13 ratio. A spectrophotometer, equipped with a single-beam scanning monochromator (NIR Systems, Model 6500, USA) and a horizontal setup module, was used to collect reflectance data from honey. The reflectance spectra were measured in wavelength ranges of 400∼2,498 nm. with 2 nm of interval. Thirty-two repetitive scans were averaged, transformed to log(1/Reflectance), and then were stored in a microcomputer file, forming one spectrum per measurement. A sample cell and reflectance plate were made to hold honey samples constantly. Spectra of honey samples were divided into a calibration set and a validation set. The calibration set was used during model development, and the validation set was used to predict quality parameters from unknown spectra. The PLS(Partial Least Square) models were developed to predict the quality parameters of honeys. The first and the second derivatives of raw spectra were also used to develop the models with proper smoothing gap. The MSC (multiplicative scatter correction) and the SNV & Dtr.(standard normal variate and detranding) preprocessing were applied to all spectra to minimize sample-to-sample light scatter differences. The PLS models showed good relationships between predicted and measured quality parameters of honeys in the wavelength range of 1100∼2200 nm. However, the PLS analysis was not good enough to predict HMF of honeys.

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UNDERSTANDING THE H STATISTIC DURING ROUTINE ANALYSIS OF ANIMAL FATS.

  • Juan, Garcia-Olmo;Ana, Garrido-Varo;Emiliano, De-Pedro
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1243-1243
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    • 2001
  • During two consecutive years, it was developed global calibrations for the prediction of fatty acids on Iberian pig fat. These equations should analyse well samples of that animal fat because of their high accuracy (SECV/sub C16:0/ = 0.26%; SECV/sub C18:0/ = 0.28%; SECV/sub C18:1/ = 0.26%; SECV/sub C18:2/ = 0.15%) and their broad covering composition range. In some cases, when new samples are predicted H (Mahalanobis distance) values higher than 3 (recommended value for agricultural products by the ISI software) are obtained. However, there are not any obvious factors which tells that samples scanned are very different to the spectral mean of the calibration population. Furthermore, these samples are well predicted according to the SEP values. The objective of the present work is to deepen the understanding of the H statistic when analysing animal fats. Three different validation files were predicted with equations obtained from January '97 to April '98. The Set A has spectra of 20 samples not included on the calibration file and scanned in May of 1998. The Set B has spectra of 20 samples included on the calibration file and scanned again in November '99. The Set C contains 150 spectra of one sample representative of the mean values (for fatty acids composition) of the calibration file. This sample was analysed three times per week during June '99 to July '00. The H mean values for the Set A, Set B and Set C were respectively 1.35, 14.39 and 11.71. These anomalous values for the Set B and C make not sense because Set B contains replicate subsamples of the same samples scanned during calibration development and Set C only contains spectra of one sample which represent the mean spectrum of the calibration files. Results will be shown to demonstrate that small day to day variations are responsible of the high H values. When a PCA and LIB file are created with calibration samples and spectra of the Set C modelling day to day variations, the H values for Set A, Set B and Set C were respectively 1.83, 2.16 and 0.93.

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Investigation of Sound Pressure Detection of Fiber Optic Sensor in Transformer Oil According to TLS and CW Laser Source (TLS와 CW 광원에 따른 트랜스포머 오일 내에서 광섬유 센서의 음압 감지 특성 연구)

  • Lee, Jong-Kil
    • The Journal of the Acoustical Society of Korea
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    • v.30 no.1
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    • pp.33-41
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    • 2011
  • To substitute TLS in the hybrid system which is combined with Sagnac interferometer and fiber bragg grating (FBG) it is necessary to investigate how the laser source (TLS and CW) and sensor material variate the response of fiber optic sensor. Two different hollow cylinder type mandrel materials are proposed which are PTFE and PTFE+carbon and 18 m optical fiber is wounded at the mandrel surface. CW laser source experiments had been done in the oil tank which is filled with transformer oil in the 1 kHz~20 kHz frequency range. Also Sagnac interferometer fiber optic sensor is combined with FBG called hybrid system and TLS used as a light source. Based on the experimental results PTFE sensor showed more higher magnitude of detection signal rather than carbon sensor and this result is agreement with the McMahon's theoretical results. Phase variation is inversely proportional to the elastic modulus of the mandrel material. In PTFE fiber sensor, tunable laser source showed more higher performance rather than CW case. Therefore, TLS fiber optic sensor can be applied to the hybrid system which is combined with Sagnac and FBG.

Morphological Characteristics and Control Factors of Bedforms in Southern Gyeonggi Bay, Yellow Sea (황해 경기만 남부해역에 발달된 층면구조의 형태적 특징과 제어 요인)

  • Kum, Byung-Cheol;Shin, Dong-Hyeok;Jung, Seom-Kyu;Lee, Yong-Kuk;Oh, Jae-Kyung
    • Journal of the Korean earth science society
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    • v.31 no.6
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    • pp.608-624
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    • 2010
  • Morphological surveys of southern Gyeonggi Bay in the Yellow Sea were conducted for2 years (2006 and 2007) by using multibeam echosounder for investigating the morphological features of bedforms. The subaqueous dunes are shown in various shapes (A~F type) and continuous spectrum of heights and lengths of transverse-to-current dunes on the wide range of sedimentary types. The height-length power-law correlation of dunes is $H_{mean}=0.0393L^{0.8984}$ (r=0.66). The comparison between Flemming (1988)'s correlation and height-length correlation of this study indicates that the subaqueous dunes in the study area are equilibrated in the present hydrological and sedimentary environment. The major controlling factors to thedevelopment and maintenance of subaqueous dunes are both strong tidal currents and the abundant availability of sand. Marine sand mining, artificial impact, changes from the original shape to an irregular shape of the subaqueous dunes with a shorter wavelength and lower height, which has influence on the development and maintenance of bedform because it causes a decrease of the availability of sediment. Water depth and sedimentary characteristics, and othercontrolling factors seem to play limited roles in the development and maintenance of subaqueous dunes.

The Microtremor HVSRs in the SW Korean Peninsula I: Characteristics of the HVSR Peak Frequency and Amplification (한반도 남서부의 상시미동 HVSR 연구 I: 정점주파수와 증폭효과의 특성)

  • Jung, Hee-Ok;Kim, Hyoung-Jun;Jo, Bong-Gon;Park, Nam-Ryul
    • Journal of the Korean earth science society
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    • v.31 no.6
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    • pp.541-554
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    • 2010
  • Fifteen min-microtremor data sets were collected at 136 sites from a coastal area of Kunsan and 117 sites from an inland area of Jeonju located in SW Korea, and were analyzed for the HVSR (Horizontal to Vertical Spectral Ratio) of the sites. The microtremor spectra of the coastal area have stronger energy in the lower frequency range from 1-6 Hz than those of the coastal area. This result can be attributed to the effect of the waves and tides in the Keum river and the Yellow sea. Twenty four hours of measurement of the microtremor indicated that the microtremor spectrum correlates with the human activities, but the microtremor HVSR peak was observed consistently at the characteristic frequency for the site. The HVSR peaks were grouped into 4 types -"single peak", "double peak", "broad peak" or "no peak"- based on their shapes. More than 90% of the data sets exhibit peak frequencies ($F_0$) which can be easily identified. The distribution of $F_0$ reveals a close relationship with the topography and local geology of the areas, exhibiting high F0s in the hillside areas and low $F_0s$ in the reclaimed land area. While the amplitudes of microtremor HVSR peak frequencies are less than 4 in the downstream of the inland area, those of the recently reclaimed land in the coastal area are extremely high (more than 10). The results of this study indicate that detailed HVSR studies are essential for the earthquake hazard reduction of reclaimed lands.

In-situ Monitoring of GaN Epilayers by Spectral Reflectance (분광 반사법을 이용한 GaN 박막의 실시간 관찰)

  • Na, Hyun-Seok
    • Journal of the Korean Vacuum Society
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    • v.20 no.5
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    • pp.361-366
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    • 2011
  • An in-situ, real-time monitoring of GaN epilayers grown by low pressure metalorganic chemical vapor deposition system modified for spectral reflectance was performed. Reflectance spectrums from 190~861 nm were observed using p-polarized light with incident angle of $75^{\circ}$. All reflectance spectrums showed interference oscillation caused by multiple reflection within GaN epilayers, and the spectrum from GaN with low crystalline quality showed weak reflectance intensity and much low amplitude of the oscillation because many defects in GaN resulted in light scattering and absorption. Signal variation of reflected light which was selected around strong constructive wavelength range was also observed during $NH_3$ supplying and $NH_3$ cut-off. There was no significant change in signal intensity when $NH_3$ cut-off for 10 sec, but it showed higher intensity when $NH_3$ was cut off for over 30 sec and its intensity kept unchanged. This result indicates that GaN surface was N-terminated during $NH_3$ supplying but Ga-terminated during $NH_3$ cut-off because of high nitrogen equilibrium vapor pressure of GaN, and metallic Ga-terminated surface caused slightly higher reflectance intensity.

Adsorption Characteristics of Cadmium ions from Aqueous Solution using by-product of Brewing (주정오니를 활용한 수중의 카드뮴(Cd) 흡착 특성)

  • Kim, Min-Su;Ham, Kwang-Joon;Ok, Yong-Sik;Gang, Seon-Hong
    • Korean Journal of Environmental Agriculture
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    • v.29 no.2
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    • pp.152-158
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    • 2010
  • Biosorption is considered to be an alternative method to replace the present adsorbent systems for the treatment of metal contaminated wastewater. In this study, by-product which was abandoned from brewing factory was used to remove metal component in aqueous solution. The experimental results showed that the range of the removal efficiency is 60~91% and adsorption equilibrium was reached in about 3 hr. FT-IR and stereo microscope has been used to observe the surface conditions and changes in functional groups by calcination. At the end of elution, the amount of nitrogen and phosphorus in water was increased 11 and 7 times compare raw sample to calcinated samples. The Langmuir isotherm adequately described the adsorption of waste materials and the maximum adsorption capacity was 28.17 mg/g for Cd. The overall results suggested that waste material might can be used for biosorption of Cd.

An Antifungal Subatance, 2,4-Diacetylphloroglucinol Produced from Antagonistic Bacterium Pseudo-monas fluorescens 2112 Against Phytophthora capsici (Phytophthora capsici를 길항하는 Pseudononas fluorescens 2112가 생산하는 항진균 항생물질 2,4-diacetylphloroglucinol)

  • 이은탁;김상달
    • Microbiology and Biotechnology Letters
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    • v.29 no.1
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    • pp.37-42
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    • 2001
  • An antifungal substance was purified from culture broth of Pseudomonas flulorescens 2112 that showed a broad-spectrum antagonistic activity against various phytopathogenic fungi including capsici. The substance was identified as 2,4-diacetylphloro-glucinol basd on NMR analysis. The 2,4-diacetylphloroglcinol showed antibiotic activity in broad acidic range from pH 1.0 to pH 9.0. About 83% of initial activity was remained after incubation for 30min ar $60^{\circ}C$, however, the activity was dropped up to 50% after 30 min incubation in $80^{\circ}C$. When the nucleotides of P. capsici treated with 2,4-diacetylphloroglucinol were labeled with[$^{3}$ H]-Adenin, the newly synthesized and radioactive-labeled RNA was significantly reduced than those of untreated P. capsici. indicating that the 2,4-diacetylphloroglucinol inhibits RNA synthesis.

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Bioequivalence of Broadcef Capsule to Cefradine Yuhan Capsule (Cephradine 500 mg) (유한세프라딘 캅셀(세프라딘 500 mg)에 대한 브로드세프 캅셀의 생물학적 동등성)

  • Cho, Hea-Young;Lee, Suk;Kang, Hyun-Ah;Oh, In-Joon;Lim, Dong-Koo;Moon, Jai-Dong;Lee, Yong-Bok
    • Journal of Pharmaceutical Investigation
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    • v.32 no.3
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    • pp.215-221
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    • 2002
  • Cephradine is a first generation cephalosporin and has broad spectrum antibacterial activity against gram-positive and gram-negative microorganisms, through inhibition of bacterial cell wall synthesis. Cephradine is useful for treatment of infections of the urinary and respiratory tract, skin and soft tissues. The purpose of the present study was to evaluate the bioequivalence of two cephradine capsules, Cefradine Yuhan (YuHan Corporation) and Broadcef (Ilsung Pharmaceuticals Co. Ltd.), according to the guidelines of Korea Food and Drug Administration (KFDA). The cephradine release from the two cephradine capsules in vitro was tested using KP VII Apparatus II method with various different kinds of dissolution media (pH 1.2, 4.0, 6.8 buffer solution and water). Twenty normal male volunteers, $23.10{\pm}2.90$ years in age and $67.69{\pm}8.04\;kg$ in body weight, were divided into two groups and a randomized $2{\times}2$ cross-over study was employed. After one capsule containing 500 mg as cephradine was orally administered, blood was taken at predetermined time intervals and the concentrations of cephradine in serum were determined using HPLC method with UV detector. The dissolution profiles of two cephradine capsules were very similar at all dissolution media. Besides, the pharmacokinetic parameters such as $AVC_t,\;C_{max}\;and\;T_{max}$ were calculated and ANOVA test was utilized for the statistical analysis of the parameters using logarithmically transformed $AVC_t\;and\;C_{max}$ and untransformed $T_{max}$. The results showed that the differences in $AVC_t,\;C_{max}\;and\;T_{max}$ between two capsules based on the Cefradine Yuhan were -2.87%, -0.96% and -4.85%, respectively. There were no sequence effects between two capsules in these parameters. The 90% confidence intervals using logarithmically transformed data were within the acceptance range of 1og(0.8) to log(1.25) $(e.g.,\;log(0.93){\sim}log(1.02)\;and\;log(0.88){\sim}log(1.13)\;for \;AVC_t\;and\;C_{max},\;respectively)$. The 90% confidence interval using untransformed data was within ${\pm}20%$ $(e.g., \;-17.54{\sim}7.78\;for\;T_{max})$. All parameters met the criteria of KFDA guideline for bioequivalence, indicating that Broadcef capsule is bioequivalent to Cefradine Yuhan capsule.

A Sensing Channel Scheduling Scheme for Improving the Cognition Ability in Cognitive Radio Systems (인지 라디오 시스템에서 주파수 상황인지 능력 향상을 위한 감지 채널 스케줄링 기법)

  • Han, Jeong-Ae;Jeon, Wha-Sook
    • Journal of KIISE:Information Networking
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    • v.35 no.2
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    • pp.130-138
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    • 2008
  • The scheme for recognizing the channel availability is one of the most important research issues in cognitive radio systems utilizing unused frequency bands. In this paper, we propose a novel scheme of selecting sensing channel in order to improve the sensing ability of frequency status in cognitive radio ad hoc networks. To fully exploit the sensing ability of each cognitive radio user, we adopt a master for a cluster which is made of several cognitive radio users. By gathering and analyzing the sensing information from cognitive radio users in the cluster, the cooperative sensing is realized. Since the transmission range of a licensed user is limited, it is possible that a master determines different sensing channels to each cognitive radio users based on their location. By making cognitive radio users sense different channels, the proposed scheme can recognize the state of wireless spectrum fast and precisely. Using the simulation, we compare the performance of the proposed scheme with those of two different compared schemes that one makes cognitive radio users recognize the frequency status based on their own sensing results and the other shares frequency status information but does not utilize the location information of licensed user. Simulation results show that the proposed scheme provides available channels as many as possible while detecting the activation of licensed user immediately.