• Title/Summary/Keyword: Spectrum Monitoring

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Determination of panthenol, cholecalciferol and tocopherol in cosmetic products by gas chromatography-mass spectrometry in SIM mode

  • Hye-Jin Jeong;Myo
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.22 no.2
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    • pp.153-160
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    • 1996
  • A novel simple method to detect vitamins in cosmetic products by gas chromatography-mass spectrometry(GC-MS) has been developed. Three vitamins(panthenol, cholecalciferol and tocopherol) were used for this study. Vitamins were prepared by dissolving in tetrahydrofuran(THF), and silylated with bis-trimethylsilyltrifluoroacetamide-trichloromethylsilane(BSTFA). Silated vitamins were separated on a fuses-silica capillary column coated with DB-5. The identification of each vitamin was accomplished by retention time and mass spectrum library search with a computer, and the quantitation was made in the selected-ion monitoring(SIM) mode of GC-MS. SIM mode had given sensitivity to determine 50pg of panthenol, 285pg of cholecalciferol and 130pg of tocopherol. Linearity was maintained over the range 0.005-0.20% for each vitamin. Each cosmetic product(i.e. hair tonic and lotion) was found to contain amounts of the vitamins. This method was sensitive and gave 77.5-99.9% recovery of each vitamin from these cosmetic products. From these results, we concluded that silylation with BSTFA followed by GC-MS analysis allows the simple, covenient and exact determination of panthenol, cholecalciferol and tocopherol.

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Use of Speckle Pattern for Monitoring Thermal Energy Behavior of Battery Cathode

  • Kim, Byungwhan;Jang, Junyoung
    • Journal of the Optical Society of Korea
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    • v.20 no.3
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    • pp.396-400
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    • 2016
  • Laser speckle patterns were used to monitor variations of thermal voltages of a cathode during a battery discharge. Discharge voltages measured with an oscilloscope were utilized as a figure of merit of thermal voltages in Zn metal. Using an optical imaging system, speckle patterns were taken for zinc metal surface over a time period of 3 minutes. Pixel sum distribution functions (PSDFs) were extracted from speckle patterns. Accumulated pixel sums quantified from PSDFs over an optimized grayscale range strongly correlated with discharge voltages. This suggested that dark matter or particles may have the capability of both absorbing and radiating thermal energies simultaneously. The black body-like properties were able to be validated by identifying coincidences with distinct features of a black body spectrum. The pixels belonging to the grayscale range were confirmed to represent dark matter of a speckle pattern. It was clear that dark matter was part of surface plasmon carriers. The proposed sensing system can be applied to monitor thermal energy variations in any material.

Bioengineering Approaches to Quantitation of Diagnosis and Treatment Monitoring for Patients with Liver Cancer: Ultrasonic Image Processing by Kalman Filtering (의공학적 기법에 의한 간암의 검진과 치료경과의 정량 : 칼만 필터링 기법에 의한 초음파 영상 처리)

  • 우광방;남상일
    • Journal of Biomedical Engineering Research
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    • v.6 no.1
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    • pp.5-12
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    • 1985
  • In this paper Kalman filtering technique is applied to ultrasound signal to improve resolution capability, Ivhlch is in use of diagnostic imaging systems. The main advantage of Kalman filter algorithm for the analysis of reflected ultrasound signal is its recursive structure which can be easily adapted to tlme varing system. Because soft-tissues, such as liver, act as distributed acoustic low-pass filters which continually change the propagating pulse. tIne can put to practical use above advantage to find a suitable signal generallng model. In state-space description of the system, the 6th order system produces tl)e 1)esc spectral approximation to the source pulse As a result of spectrum analysis, 6th order estimator for two closely spaced ((p.5 mm) reflectors enhances resolution by 4dB-lOdB. By using this result, the possibility to detect even minute tumor is demonstrated.

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A Study on the Evaluation of Internal Leak in Valve for Nuclear Power Plant Using Acoustic Emission Method (음향방출법에 의한 원자력발전소 밸브내부 누설평가에 관한 연구)

  • Lee, Sang-Guk;Lee, Sun-Ki;Lee, Jun-Shin
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.284-289
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    • 2004
  • The objective this study is to estimate the feasibility of acoustic emission method for the internal leak from the valves in nuclear power plants. From the experimental results, it was suggested that the acoustic emission method for monitoring of leak was feasible. When the background levels are higher than the acoustic signals from leak, we can detect the leak analyzing the spectrum of the remainders which take the background noise from the acoustic signals.

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Design and Analysis of a Memoryless Minimum Bandwidth Birnary Line Code MB58 (Memoryless 최소대역폭 2진 선로부호 MB58의 설계 및 분석)

  • 김정환;김대영
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.17 no.10
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    • pp.1074-1080
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    • 1992
  • A(5,8) block binary line code is proposed. The new line code called MB58 has the properties of being dc-free and runlength-limited, and it is strictly bandwidth-limited to the Nyquist frequency, such that bandwidth efficiency is improved. This new code is a memoryless code with a simple decoding rule and capability of error monitoring. The power spectrum and the eye pattern of the new code are obtained by simulation, wherein spectral nulls at DC(f=0) and Nyquist frequency (f=1/2Ts) are clearly identified.

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Flashover Prediction of Polymeric Insulators Using PD Signal Time-Frequency Analysis and BPA Neural Network Technique

  • Narayanan, V. Jayaprakash;Karthik, B.;Chandrasekar, S.
    • Journal of Electrical Engineering and Technology
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    • v.9 no.4
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    • pp.1375-1384
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    • 2014
  • Flashover of power transmission line insulators is a major threat to the reliable operation of power system. This paper deals with the flashover prediction of polymeric insulators used in power transmission line applications using the novel condition monitoring technique developed by PD signal time-frequency map and neural network technique. Laboratory experiments on polymeric insulators were carried out as per IEC 60507 under AC voltage, at different humidity and contamination levels using NaCl as a contaminant. Partial discharge signals were acquired using advanced ultra wide band detection system. Salient features from the Time-Frequency map and PRPD pattern at different pollution levels were extracted. The flashover prediction of polymeric insulators was automated using artificial neural network (ANN) with back propagation algorithm (BPA). From the results, it can be speculated that PD signal feature extraction along with back propagation classification is a well suited technique to predict flashover of polymeric insulators.

Exciting Frequency Detection of Latticed fence Structure Using Fiber Optic Interferometer Sensor (간섭계형 광섬유 센서를 이용한 격자형 구조물의 외부 가진 진동수 탐지)

  • 이종길
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.5
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    • pp.142-148
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    • 2004
  • In this paper, to detect exciting frequency on the latticed fence structure, fiber optic sensor using Sagnac interferometer was fabricated and tested. The latticed structure fabricated with dimension of 180 cm wide and 180 cm high, the optical fiber, 50 m in length, distributed and fixed on the latticed structure. Single mode fiber, a laser with 1,550 m wavelength, and $3{\times}3$ coupler were used. Excited vibration signal applied to the latticed structure from 200 Hz to 1 KHz. The detected optical signals were compared to the detected acceleration signals and analyzed on the time and frequency domain. Based on the experimental results, fiber optic sensor using Sagnac interferometer detected exciting frequency, effectively. This system can be applied to the structural health monitoring system.

Research on the Effect of Cutter Wear on the Torsional Vibration of Spindle in Milling (밀링가공에서 공구마모와 스핀들의 비틀림 진동과의 상관관계에 관한 연구)

  • Kim, Seog-Gwan
    • Journal of the Korean Society for Precision Engineering
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    • v.16 no.9
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    • pp.62-67
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    • 1999
  • In milling, cutting tool ins directly attached to spindle and this tells that spindle can provide very useful information on the cutting tool condition such as wear or breakage. Since spindle is rotating at a high speed, measuring spindle velocity using a noncontacting measurement system gives the best information which can be obtained. Due to the force applied to spindle through cutting tool, velocity of spindle changes. And any change in cutting tool condition affects cutting force and consequently spindle vibration. With the intent of continuously monitoring cutting tool condition in intermittent machining operations in a benign manner, a noncontacting velocity measurement system using a laser Doppler velocimeter was assembled to measure spindle torsional vibration. Spindle vibration was measured and analysis of it in the frequency domain yielded a measure which corresponded to amount of cutting tool wear in milling.

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Delayed fast neutron as an indicator of burn-up for nuclear fuel elements

  • Akyurek, T.;Shoaib, S.B.;Usman, S.
    • Nuclear Engineering and Technology
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    • v.53 no.10
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    • pp.3127-3132
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    • 2021
  • Feasibility study of burn-up analysis and monitoring using delayed fast neutrons was investigated at Missouri University of Science and Technology Reactor (MSTR). Burnt and fresh fuel elements were used to collect delayed fast neutron data for different power levels. Total reactivity varied depending on the burn-up rate of fuel elements for each core configuration. The regulating rod worth was 2.07E-04 𝚫k/k/in and 1.95E-04 𝚫k/k/in for T121 and T122 core configurations at 11 inch, respectively. Delayed fast neutron spectrum of F1 (burnt) and F16 (fresh) fuel elements were analyzed further, and a strong correlation was observed between delayed fast neutron emission and burn-up. According to the analyzed peaks in burnt and fresh fuels, reactor power dependency was observed and it was determined that delayed neutron provided more reliable results at reactor powers of 50 kW and above.

KVN unveils the plasma physics of AGN

  • Trippe, Sascha
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.2
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    • pp.51.3-51.3
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    • 2019
  • Its ability to measure the polarization of light at four frequencies makes the KVN a "plasma physics observatory" that can probe the internal physics (e.g., magnetic fields, outflow geometries) of AGN radio jets and cores. We initiated a Key Science Program, the Plasma-physics of Active Galactic Nuclei (PAGaN) project, dedicated to polarimetric monitoring of 14 radio-bright AGN. We have been able to measure the Faraday rotation measure of the cores of our targets as function of frequency; the observed scaling relation is in good agreement with conically expanding outflows to first order. We are further probing a polarized hotspot in the jet of 3C84 and possible systematic differences in the Faraday rotation in BL Lacertae objects and flat spectrum radio quasars.

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