• Title/Summary/Keyword: Specimen stability

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Changes of Performance of Soil-Cement Barrier due to Migration of Acids (산 이동에 따른 심층혼합기둥체 차수벽의 성능변화)

  • 정문경;천찬란;이주형;김강석
    • Proceedings of the Korean Geotechical Society Conference
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    • 2003.03a
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    • pp.189-196
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    • 2003
  • Soil-cement column is often used as a contaminant barrier. This study presents the results of experimental study performed to investigate the changes of properties of soil-cement column under the attack of acids. Sulfuric nitric, and ascetic acid were used as contaminants. Specimen were made of clayey and sandy soils with addition of cement and water Permeability of soil-cement decreased with time during permeability test. When significant amount of acid percolated the specimen, permeability increased and compressive strength decreased due to the dissolution and leaching of cement and its chemical reaction compounds. Sulfuric and nitric acid were more effective than ascetic acid in deteriorating soil-cement column. Amount of acid required to lower the pH of soil cement below 12 was calculated from the results of permeability tests. This leads to a conclusion that, under the conditions employed in this study, the chemical stability of soil-cement column could be maintained against acid attack for longer than generally accepted lifetime of contaminant barriers.

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A Study on the Surface Deterioration Evaluation of Epoxy Resin Coating as Anticorrosive Material of Concrete Water Tank Using Ozone($O_3$) (오존 정수처리 음용수조 구조물에 사용하는 에폭시 수지 방수.방식재의 표면특성 평가)

  • 오상근;강효진;곽규성
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.11a
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    • pp.513-518
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    • 2003
  • Recently, advanced systems for water treatment are introduced for water quality improvement. One of those systems is water treatment method using ozone($O_3$). For it has strong oxidizing energy, it is necessary to have materisl stability against $O_3$. In this paper, epoxy resin specimens using as anticorrosive material of concrete structure for drink water are used to serve as a material of deterioration evaluation. It is to be studied weight loss, surface corrosion of specimens, ingredient analysis of floating particle, a solute of chemical ingredient by way of accelerated ozone testing. As the results of experiment, specimen weight is decreased. The surface of specimen is eroded heavily and showed a loss of gloss and floating particle, and in the stability for drinking water, harmful ingredient is not detected in the water.

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Variation of Dielectric Properties and Phase Stabilities with Substitution of A-Site in $Pb(Zn_{0.6}Mg_{0.4})_{1/3}Nb_{2/3}O_3$[PZMN] System ($Pb(Zn_{0.6}Mg_{0.4})_{1/3}Nb_{2/3}O_3$ [PZMN] 계에서 A-자리 치환에 따른 상안정화 및 유전 특성 변화)

  • 김봉철;김정주;김남경;조상희
    • Journal of the Korean Ceramic Society
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    • v.33 no.10
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    • pp.1131-1137
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    • 1996
  • The dielectric properties and phase stabilities of Pb(Zn0.6Mg0.4)1/3Nb2/3O3 [PZMN]system were investigated into substitution of A-site with Ba, Sr and Ca ions. The A-site substitutions led to the complexity of components of perovskite phase and then DPT coefficient increased. The A-site substitutions of Ba or Sr ion perovskite single phase could be easily formed by columbite process due to increase of perovskite phase stability. The variation of lattice parameters in specimen obeyed Vegard's law and curie temperature and dielectric constant of specimen decreased linearly. But Ca substitution led to perovskite phae instability. The lattice parameter dielectric constant and curie temperature of specimens drasticaly decreased with formation of pyrochlore phase.

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Effects of Ce on the Mechanical Alloying Behavior and Thermal Stability of Al-8wt.%Fe Powder (Al-8wt.%Fe 분말의 기계적 합금화 거동과 열적안정성에 미치는 Ce의 영향)

  • 오광진
    • Journal of Powder Materials
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    • v.1 no.1
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    • pp.4-14
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    • 1994
  • The effects of Ce on the mechanical alloying behavior and the thermal stability of Al-8wt.%Fe were investigated. The steady states of Al-8wt.%Fe and Al-8wt.%Fe-4wt.%Ce powders with 1.5 wt.% stearic acid as a process control agent were reached after mechanical alloying for 1000 minuties and 1300 minuties respectively at the conditions of the impeller revolving velocity of 300 rpm and the ball to powder input ratio of 50 : 1. The hardness of Al-8wt.%Fe specimen hot extruded and isothermally aged at various temperatures for up to 1000 hours decreased rapidly at 50$0^{\circ}C$ and its high temperature ultimate tensile strength began to decrease at 40$0^{\circ}C$ with increasing aging time. The decrease in the hardness and ultimate tensile strength of the specimen were reduced substantially by addition of Ce. It was thought to be due to the formation of thermally stable A14Ce and All3Fe3Ce intermetallic compounds.

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The Analysis of Fatigue Damage in Structure under Variable Load (변동 하중을 받는 구조물에서의 피로 파손 해석)

  • 한문식;조재웅
    • Transactions of the Korean Society of Automotive Engineers
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    • v.12 no.4
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    • pp.85-93
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    • 2004
  • The variable fatigue load is simulated in this study, The stability and the life of the material are analyzed theoretically by the program of Ansys workbench. These results are successfully applied to the practical structures to predict the prevention of fracture and the endurance, The life and the damage on the every part of the fatigue specimen can be predicted. As the available lives are compared for every loading variation, the rainflow and damage matrix results can be helpful in determining the effects of small stress cycles in any loading history. The rainflow and damage matrices illustrate the possible effects of infinite life. The safety and stability of fatigue specimen according to the variable load can be estimated by using the results of this study.

Color Stability and Surface Roughness of Single-Shade Composite Resin after Finishing and Polishing

  • Hyewon Shin;Haeni Kim;Minho Hong;Juhyun Lee
    • Journal of the korean academy of Pediatric Dentistry
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    • v.51 no.3
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    • pp.197-207
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    • 2024
  • This study aims to evaluate the color stability and surface roughness of the single-shade composite resin after finishing and polishing for primary molars. A single-shade composite resin (OM, OMNICHROMA) and two multi-shade composite resins (FT, FiltekTM Z350XT; ES, ESTELITE® SIGMA QUICK) were included. The specimens were divided into three subgroups using different polishing methods: control, Sof-Lex XT, and Sof-Lex Diamond. For color stability tests, cavities were prepared on extracted primary second molars and restored with experimental composite resins. Each specimen was immersed in the coffee solution for 48 hours. The color difference of each specimen was calculated. For surface roughness tests, cylindrical specimens were crafted with experimental composite resins. Surface roughness was analyzed using an atomic force microscope and a scanning electron microscope. In the color stability tests, FT demonstrated a significantly lower ΔEab than ES among the control groups, but no significant differences were observed between the ΔEab values of OM and FT or OM and ES. Additionally, no significant differences were found between the Sof-Lex XT and Sof-Lex Diamond subgroups in the three composite groups. Moreover, no significant differences in the surface roughness were found between the three composite groups, regardless of the polishing methods. The single-shade composite resin demonstrated comparable color stability and surface roughness to that of the multi-shade composite resins regardless of the polishing methods used in restoring primary molars. The single-shade composite resin is expected to be applicable in clinical pediatric dentistry reducing chair time due to the easy shade matching procedures.

Effects of Ca Implantation on the Sintering and Crack Healing Behavior of High Purity $Al_2$O$_3$ Using Micro-Lithographic Technique-III: Stability of Crack-Like Pore (Ion Implantation으로 Ca를 첨가된 단결정 $Al_2$O$_3$의 Crack-Like Pore의 Healing 거동-III: Stability of Crack-Like Pore)

  • 김배연
    • Journal of the Korean Ceramic Society
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    • v.36 no.9
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    • pp.887-892
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    • 1999
  • The inner crack-like pore with controlled amount of Ca impurity in the high purity alumina single crystal sapphire had been created by micro-fabrication technique which includes ion implanation photo-lithography Ar ion milling and hot press technique. The crack-like pores in two-hour hot pressed specimen were extremely stable even after heat treating at 1,80$0^{\circ}C$ for 5 hours almost no healing was observed. But the crack-like pores in one-hour hot pressed specimen at 1,30$0^{\circ}C$ were healed by heat treatment and the amount of healing was increased with the heat treatment time and temperature and the amount of Ca addition. The edges of crack-like pore parallel to <1100> direction in (001) basal plane were stable but the edges normal to this direction in (00101) plane <1120> direction were unstable to facetting This means that the surface energy of alumina along the <1100> direction in (0001) basal plane in much lower than <1120> direction.

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Thermal Comfort and Tactile Wearing Performance of Wool/nylon Fabrics for Tra-biz Garment (울/나일론 tra-biz 의류용 직물 소재의 열적 쾌적성과 착용특성)

  • Kim, Hyun Ah
    • Fashion & Textile Research Journal
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    • v.18 no.6
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    • pp.878-888
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    • 2016
  • In this study, wool/nylon(50/50%) blend yarn and its fabrics for tra-biz(complex word of travel+business) garment were prepared, and its wear comfort characteristics were investigated through thermal manikin and human-body wearing experiment. In addition, tactile wearing performance from fabric mechanical properties and the dimensional stability and the pilling of the fabric specimen during wearing and dry-cleaning were measured and compared with those of wool 100% fabric specimen. Heat keepability of the wool/nylon(50/50%) blend fabric by thermal manikin experiment was superior than that of wool 100% fabric, this result was verified with human-body wearing experiment and its result coincided well with this experimental result. Tactile wearing performance of the wool/nylon(50/50%) fabric from fabric mechanical properties measured by FAST system was better than that of the wool 100% fabric. The dimensional stability of the wool/nylon(50/50%) fabric was more stable than that of the wool 100% fabric. Because relaxation shrinkage was lower and hygral expansion of wool 100% fabric was more high. However, the breathability and pilling property of the wool/nylon(50/50%) fabric were inferior than those of the wool 100% fabric. The possibility of application for tra-biz garment of wool/nylon(50/50%) blend fabric was observed because of good heat keepability, tactile wearing performance and washing fastness.

Fabrication of Porous Cu by Freeze-drying Process of Camphene Slurry with CuO-coated Cu Powders (CuO가 코팅된 Cu 분말을 혼합한 Camphene 슬러리의 동결건조에 의한 Cu 다공체 제조)

  • Bang, Su-Ryong;Oh, Sung-Tag
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.191-195
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    • 2014
  • This study reports a simple way of fabricating the porous Cu with unidirectional pore channels by freeze drying camphene slurry with Cu oxide coated Cu powders. The coated powders were prepared by calcination of ball-milled powder mixture of Cu and Cu-nitrate. Improved dispersion stability of camphene slurry could be achieved using the Cu oxide coated Cu powders instead of pure Cu powders. Pores in the frozen specimen at $-25^{\circ}C$ were generated by sublimation of the camphene during drying in air, and the green bodies were sintered at $750^{\circ}C$ for 1 h in $H_2$ atmosphere. XRD analysis revealed that the coated layer of Cu oxide was completely converted to Cu phase without any reaction phases by hydrogen heat treatment. The porous Cu specimen prepared from pure Cu powders showed partly large pores with unidirectional pore channels, but most of pores were randomly distributed. In contrast, large and aligned parallel pores to the camphene growth direction were clearly observed in the sample using Cu oxide coated Cu powders. Pore formation behavior depending on the initial powders was discussed based on the degree of powder rearrangement and dispersion stability in slurry.

A Study on the Structural Stability of a Jig for Evaluating the Vibration Durability of a Hydraulic Hose (유압 호스의 진동 내구성 평가를 위한 지그의 구조적 안정성에 관한 연구)

  • Kim, Chae-Sil;Jun, Min-Seong
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.20 no.1
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    • pp.125-131
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    • 2021
  • For the vibration reliability tests, the jigs for mounting the test specimen on a vibration reliability tester are required. The dynamic stabilities of the jigs should be verified before the tests for obtaining the accurate reliability of the test specimen. This paper proposes an analytical technology for ensuring the dynamic structural stability for the test setup including the jig. The technology includes the mode analyses for checking resonance, the harmonic analyses for evaluating the dynamic structural stability of test setup including the jig, and the fatigue analyses for obtaining the durable reliability time with calculating the life cycles at the area of weakness. The cause investigation of the damaged jig during vibration reliability test of a rubber hose and the design of new revised jig are performed by using the technology. The vibration reliability test for the rubber hose with the new revised jig by analysis results is successfully conducted without any problem. Therefore the jig's design technology proposed in this paper may be useful for other items as well.