• Title/Summary/Keyword: Specimen

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The Effect of Seawater on Hydration of Clinker Minerals (I) Effects of SO42- and Cl- ions (시멘트 클린커 광물의 수화에 미치는 해수성분의 영향 (I)SO42- 및 Cl-이온에 의한 영향)

  • 신도철;송태웅;한기성;최상흘
    • Journal of the Korean Ceramic Society
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    • v.24 no.1
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    • pp.77-85
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    • 1987
  • Hardened cement paste is mainly affected by corrosion of sulphate and chlorine ions in sea water. In this investigation, many specimens were made with the cement clinker minerals such as C3S, C3A, C4AF and their mixture according to cement composition added various blending materials. After the specimens were immersed in 4% MgSO4 and MgCl2 solutions, the product of reaction, the microstructure of specimen and Ca+2 ion leached in the solution were studied. The formation of Ca(OH)2 in the specimen of C3S is reduced relatively by adding pozzolanic admixtures. The chlorine ion is easily diffuse into the C3S specimen and produced CaCl2 compound, and it makes the specimen porous by leaching out itself into the solution. The specimen of C3A, C4AF are broken down by expanding reaction of ettringite and gypsum compound produced in the MgSO4 solution. At a later period, the ettringite is transformed into gypsum and 5MgO.2Al2O3·15H2O. The C3A in the MgCl2 solution combines chlorine ion to form Friedel's salt and prevents the diffusion reaction of chlorine ion into the specimen. Granulated slag shows inferior effect on the resistance of the specimen in MgSO4 solution by forming ettringite and gypsum, but good result in MgCl2 solution. Pozzolanic materials, on the whole, offer noticable effect on the resistance of the specimen in both solutions.

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Deformational Characteristics of Compacted Subgrade Soils in Korea with Specimen Construction Methods (시편 성형기법에 따른 국내 다짐 노상토의 변형특성)

  • Kweon, Gi-Chul;Hwang, Chang-Il
    • International Journal of Highway Engineering
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    • v.9 no.4
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    • pp.55-63
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    • 2007
  • Deformational characteristics of subgrade soils are important properties in the mechanistic analysis and design of pavement system. In this study, to evaluate the effect of specimen construction methods on deformational characteristics of subgrade soils in Korea, resonant column tests were performed for specimens constructed by various methods. Specimen construction method affected to the modulus value but the variation in the normalized modulus reduction curve was almost identical. The effects of specimen construction method on modulus are decreased with increasing confining pressure. The average maximum variation in the modulus value with different specimen construction methods was estimated as 16.8%. The differences in the modulus value of the specimens with same water content and dry density conditions that made by gyratory compaction and impact compaction were very small within 5.2%. The impact compaction method was proposed as a specimen construction method for determining the design input parameter testing considering that impact compaction method is much simpler and require less expensive specimen construction equipment and setup than gyratory compaction method.

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Observation of Shrinkage Features of Cross Sectional Surface of Wood by LV-SEM (저진공주사현미경(LV-SEM)을 이용한 목재횡단면의 수축거동관찰)

  • Kang, Chunwon;Matsumura, Junji;Kang, Wook
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.3
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    • pp.17-23
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    • 2008
  • The purpose of this study is to estimate the shrinkage of wood by LV-SEM (Low-Vacuum Scanning Electron Microscope) which can observe wetted wood sample. The shrinkage of small sample specimen by the dehumidification in the specimen chamber was investigated and compared with that of normal wood specimen. The observation of cross sectional surface of wood from wetted condition to dried condition can be achieved in about twenty minutes by means of the dehumidification in the specimen chamber of LV-SEM. The volumetric shrinkage of earlywood was almost the same as that of latewood. The shrinkage of SEM observation specimen was similar to that of normal wood specimen. From the correlation of the shrinkages between SEM observation specimen and normal wood specimen, it is surmised that the shrinkage of wood is more strictly dominated by shrinkage of latewood than that of earlywood.

Observation of thermal properties of dental 3D printer materials (치과용 DLP 3D Printer 가공체의 열특성 관찰)

  • Song, Joon-Boo;Park, Yu-Jin;Choi, Sung-Min
    • Journal of Technologic Dentistry
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    • v.43 no.3
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    • pp.71-76
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    • 2021
  • Purpose: In this study, thermal properties were observed by measuring the extent of thermal expansion and the amount of thermal residue that appears upon burnout on a workpiece made by using a dental digital light processing (DLP) three-dimensional (3D) printer. Methods: Thermal properties of workpieces manufactured by using two 3D printers were observed. The specimens were designed in cylindrical form with dimensions 10 mm in diameter and 10 mm in height. The control specimen was made of wax, and the experimental specimen was made of resin. The thermal expansion rate was measured by applying heat to three types of specimens, and burnout residue was measured. Results: The thermal expansion rate of the wax pattern (WP) specimen was 0.93%±0.05%, of the RP1 specimen was 1.30%±0.08%, and of the RP2 specimen was 1.20%±0.09%. Measuring the recovered residue yielded residual amounts of 0.2% for the WP specimen, 1.1% for the RP2 specimen, and 1.8% for the RP1 specimen. Conclusion: 1. From measurements of the workpieces manufactured by dental DLP 3D printing, the thermal expansion rate was found to be higher than that of wax. 2. As a result of measuring burnout residues on the workpieces manufactured by dental DLP 3D printing, the required summoning temperature to obtain suitable castings was determined to >750℃.

Effects of Specimen Size and Testing Velocity on Puncture Properties of Short-fiber Reinforced Chloroprene Rubber (시편 크기 및 시험속도가 단섬유 강화 클로로프렌 고무의 관통 특성에 미치는 영향)

  • Ryu, Sang-Ryeoul;Lee, Dong-Joo
    • Composites Research
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    • v.20 no.6
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    • pp.28-33
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    • 2007
  • The puncture properties of short-fiber reinforced rubber were investigated as functions of fiber aspect ratio(AR: length of fiber/diameter of fiber), fiber content, specimen size and testing velocity. The puncture stresses of the matrix and short-fiber reinforced rubber decreased with specimen size, and increased with testing velocity at same specimen size. As the fiber AR increased the puncture stress at given fiber content also increased. The problem of the specimen shape was investigated by the comparison of the tensile strength with puncture stress. The forces acting in the membrane wall of the matrix and the short-fiber reinforced rubber showed a similar data regardless of specimen size. And those increased with testing velocity at same specimen size. As the fiber AR increased the force acting in the wall at given fiber content also increased. Overall, it was found that the specimen size, testing velocity had an important effects on the puncture properties.

Effects of loading frequency and specimen size on the liquefaction resistance of clean sand

  • Sung-Sik Park;Dong-Eun Lee;Dong-Kiem-Lam Tran
    • Geomechanics and Engineering
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    • v.37 no.2
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    • pp.123-133
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    • 2024
  • This study investigates the effects of loading frequency (f) and specimen size on the liquefaction resistance of clean sand. A series of cyclic direct simple shear tests were conducted on Jumunjin sand with varying consolidated relative densities (40% and 80%), f values (0.05, 0.10, and 0.20 Hz), and diameter to height (D/H) ratios (3.63, 3.18, 2.82, and 2.54). The results demonstrated the significant influence of f and D/H ratio on the number of cycles to liquefaction (Ncyc-liq) and the cyclic resistance ratio (CRR15). It was observed that increasing f linearly increased Ncyc-liq. Increasing the specimen height also led to higher Ncyc-liq values irrespective of the f or relative density. Moreover, a positive correlation between CRR15 and f indicated that higher f yielded higher CRR15. This relationship was more pronounced in dense sand than in loose sand. Specimen height also significantly affected CRR15, with increasing the specimen height resulting in higher CRR15 values. Furthermore, the effect of f on CRR15 was less significant compared to the influence of specimen height. The effect of f on the normalized cyclic resistance ratio (NCRR) was relatively negligible for loose sand but more substantial for dense sand depending on the D/H ratio. Data analysis revealed that the NCRR generally decreases as the D/H ratio increases. An interpolation formula was provided to calculate the NCRR based on the D/H ratio regardless of the f and relative density.

Fabrication of Nano-Size Specimens for Tensile Test Employing Nano-Indentation Device (나노 인장시험을 위한 압축 시험기용 인장시편 제작에 관한 연구)

  • Lim, Tae Woo;Yang, Dong-Yol
    • Journal of the Korean Society for Precision Engineering
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    • v.32 no.10
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    • pp.911-916
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    • 2015
  • In the nano/micro scale, material properties are dependent on the size-scale of a structure. However, conventional micro-scale tensile tests have limitations to obtain reliable values of nano-scale material properties owing to residual stress and elastic slippage in the gripping/aligning process. The indenter-driven nano-scale tensile test provides prominent advantages simple testing device, high-quality nano-scale metallic specimen with negligible residual stress. In this paper, two-types of specimens (a specimen with multi-testing parts and a specimen with a single-testing part) are discussed. Focused ion beam (FIB) is employed to fabricate a nano-scale specimen from a thin nickel film. Using the specimen with a single-testing part, we obtained a nano-scale stress-strain curve of electroplated nickel film.

A study of hydrogen embrittlement behavior in E.B welded 250,300 grade 18% Ni maraging steel (전자비임 용접한 250 및 300 Grade 18% Ni Maraging 강의 수소취화 거동에 관한 연구)

  • 윤한상;정병호
    • Journal of Welding and Joining
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    • v.5 no.2
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    • pp.53-59
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    • 1987
  • The effect of applied stress, current density and heat-treatment after welding on the time to fracture, fracture behavior was investigated by the method of constant load tensile testing under catholic charging with hydrogen in E.B. welded 250,300 Grade 18% Ni Maraging steel sheet. The main results obtained are as follows: 1. All specimen showed the characteristic delayed failure and the time to fracture showed decreasing tendency with the increase in current density and applied stress. 2. Hydrogen embitterment susceptibility of notched specimen after solution-treatment and aging after welding was more increased than that of aged smooth specimen and as welded specimen. 3. Fracture surface showed a typical intergranular fracture on the border, a dimple pattern in the center of specimen and some quasi-cleavage fracture between the intergranular and the dimple.

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A Study on the Influence of Aggregate on the Estimation of Compressive Strength by Small Size Core (소구경 코어에 의한 콘크리트 압축강도 추정에 미치는 골재의 영향에 관한 연구)

  • 김경민;백병훈;한민철;윤기원;한천구;송성진
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2002.11a
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    • pp.51-54
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    • 2002
  • This study is intended to investigate an influence of the kinds and the maximum size of aggregate on the compressive strength of small size core specimen. According to the results, the compressive strength of standard specimen is large in order of basalt, granite and limestone aggregate, and shows increasing tendency as the maximum size of aggregate grows large. The compressive strength of concrete using basalt aggregate shows similar tendency to granite aggregate, and that of concrete using limestone aggregate decreases slightly, compared with granite aggregate. The reducing ratio of the compressive strength of 25mm core specimen is least when the maximum size of aggregate is 10mm. But the compressive strength of 50 and 100mm core specimen is almost not influenced by the maximum size of aggregate.

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Deformation of the Rolled Plate with Hydrogen Absorption-Desorption Cycling (수소저장-방출싸이클링에 의한 압연판재의 변형)

  • 정영관;김경훈;정선환;김창덕;이근진;박규섭
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.05a
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    • pp.861-864
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    • 2002
  • Deformation of the specimen was investigated on hydrogen absorption-desorption cycling. In order to study this problem, the cold rolled palladium thin plate as the specimen had been used. By using the electrochemical method, the palladium plate specimen was cyclically hydrogenated in the 0.1 mol $H_2SO_4$ electrolyte. As results, it is noted that the thickness of the plate specimen gradually increased in increasing hydrogenation cycles whereas the width and the length decreased. Also, grains in the plate specimen were greatly deformed after hydrogenation cycling. But hydrogen absorption rate scarcely changed.

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