• Title/Summary/Keyword: Specific surface are

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Characterization of the Microporosity of Activated Carbon Fiber (활성탄소섬유의 미세기공 특성화)

  • 진항교;이정민;유승곤
    • Journal of the Korean Vacuum Society
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    • v.2 no.4
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    • pp.491-500
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    • 1993
  • The adsorption of nitrogen (77K) and carbon dioxide(273K) was performed on a series of activated carbon fiber. Theadsorption iotherm of nitrogen was typical type 1 and that of carbon dioxide was convex. As the specific surface area increases, there are linear increases in BET constant C mean pore diameter, the width of pore size distribution, wide micropore volume, total micropore volume, total pore volume and external surface area, however, narrow micropore volume was nealy constant . The total micorpore volume fraction in total pore volume is above 97%.

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Effect of the Variation of Speccfic Gravity and the Addition of Water Repellent Agent on the Physical Properties of Autoclaved Lightweight Concrete (비중의 변화와 발수제 첨가가 경량기포콘크리트의 물성에 미치는 영향)

  • 노재성;황의환;홍성수;이범재
    • Magazine of the Korea Concrete Institute
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    • v.9 no.2
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    • pp.137-144
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    • 1997
  • The effcct of specific g~avity cont~olled In the .range fiom O.4 to 0.7 by particle size and added amount of A1 powder in the presence or absence of water repellent agent on the physical properties of ALC was examined to evaluate frost resistance and durability. The compressive sttcngth and the tensile strength are increased and independency with water repellent agent when the specific gravity is increased in the range from 0.4 to 0.7. According as the added amount of water repellent agent was increased. frost resistance was improved and absorption ratio was decreased. ALC produced from fine Al powder has a low volume reduction by scaling and a sound apperance after freezing/thawing test and top surface freezing test.

Rotor High-Speed Noise Prediction with a Combined CFD-Kirchhoff Method (CFD와 Kirchhoff 방법의 결합을 이용한 로터의 고속 충격소음 해석)

  • 이수갑;윤태석
    • Journal of KSNVE
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    • v.6 no.5
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    • pp.607-616
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    • 1996
  • A combined computational fluid dynamics(CFD)-Kirchhoff method is presented for predicting high-speed impulsive noise generated by a hovering blade. Two types of Kirchhoff integral formula are used; one for the classical linear Kirchhoff formulation and the other for the nonlinear Kirchhoff formulation. An Euler finite difference solver is solved first to obtain the flow field close to the blade, and then this flow field is used as an input to a Kirchhoff formulation to predict the acoustic far-field. These formulas are used at Mach numbers of 0.90 and 0.95 to investigate the effectiveness of the linear and nonlinear Kirchhoff formulas for delocalized flow. During these calculiations, the retarded time equation is also carefully examined, in particular, for the cases of the control surface located outside of the sonic cylinder, where multiple roots are obtained. Predicted results of acoustic far-field pressure with the linear Kirchhoff formulation agree well with experimental data when the control surface is at the certain location(R=1.46), but the correlation is getting worse before or after this specific location of the control surface due to the delocalized nonlinear aerodynamic flow field. Calculations based on the nonlinear Kirchhoff equation using a linear sonic cylinder as a control surface show a reasonable agreement with experimental data in negative amplitudes for both tip Mach numbers of 0.90 and 0.95, except some computational integration problems over a shock. This concliudes that a nonlinear formulation is necessary if the control surface is close to the blade and the flow is delocalized.

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Bone-like Apatite Formation on Ultrafine-Structure in Modified Electrolytic Solution

  • Jang, Jae-Myung;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.155-155
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    • 2017
  • Surface modifications are commonly utilized to adjust the properties of the titanium and its alloy surface to the specific needs of the medical applications, but there are disadvantages such as poor osteoconductive properties and low adhesion of bone cell to implant surface. In order to improve these disadvantages, changes in surface properties have an important effect on osseointegration during implantation. In this paper we applied new technological method for improving a unique surface modification using the characteristic of an electrolytic Solution. Thus, in the electrolyte containing NaF in Na2SO4, TiO2 nanoporous was uniformly formed, and HAp nanoparticles were electrodeposited around the TiO2 nanopores, but in the electrolyte containing NH4F in (NH4)H2PO4, the coarse protrusions including HAp nano particles were regularly deposited onto the TiO2 barrier layer. The surface characteristics and the distributed elements and have been investigated by EDS analysis, and ultra-fine structure of surface are carried out using FE-SEM. To investigate the behavior of the anion, the analysis of chemical states was performed by XPS, and the narrow spectrums for Ti2P, Ca 2p, and P 2p seems to be almost similar depending on the characteristics of the electrolyte solution respectively. In addition, Ca 2p spectrum could be resolved into two peaks for Ca 2p3/2 and 2p1/2 at 347.4 and 351.3 eV, which are related to hydroxyapatite. And, the P peak can also be deconvoluted into two peaks for P1/2 and P3/2 levels with binding energy 134.2 and 133.4 eV, respectively. From the result of soaking test, the apatite morphologys were well-formed onto the modified surface according to the different conditions.

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Implementation of Small Sized Designs for Economic Estimation of Second-Order Models (2차 모형의 경제적 추정을 위한 소형실험계획의 활용)

  • Kim, Jeong-Suk;Byeon, Jae-Hyeon
    • Proceedings of the Korean Operations and Management Science Society Conference
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    • 2006.11a
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    • pp.531-534
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    • 2006
  • Response surface methodology (RSM) is a useful collection of experimentation techniques for developing, improving, and optimizing products and processes. When we are to estimate second-order regression model and optimize quality characteristic by RSM, central composite designs and Box-Behnken designs are widely in use. However, in developing cutting-edge products, it is very crucial to reduce the time of experimentation as much as possible. In this paper small-sized second-order designs are introduced and their estimation abilities are compared in terms of D-optimality, A-optimality, and variance of regression coefficients, ease of experimentation, number of experiments. Then we present a guideline of using specific designs for specific experimentation circumstances. The result of this study will be beneficial to experimenters who face experiments which are expensive, difficult, or time-consuming.

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An Experimental Study on the Lapping of Titanium Alloy (티타늄합금의 래핑가공에 관한 실험적 연구)

  • Park, Ji-Ho;Kim, Won-Il
    • Journal of the Korean Society of Industry Convergence
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    • v.8 no.1
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    • pp.25-29
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    • 2005
  • Titanium specially has high specific strength, excellent mechanical properties as fatigue strength and fracture ductility, good corrosion resistance, and therefore are broadly applied to the various fields. It is required the developmennt for the skills of wire-cut electrical discharge machining(WEDM), but the WEDMed surface was found to be worst due to the attached components of wire. Therefore precision maching method like lapping is necessary for getting high quilty surface. Roughness of lapped surface, surface hardness to each process depth and improved method of surface shape were stuided experimentally, by changing of grain size of diamond lap material and lapping pressure with constant speed in lapping process.

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Searching Algorithm for Finite Element Analysis of 2-D Contact Problems (2차원 접촉문제의 유한요소 해석을 위한 탐색알고리즘)

  • 장동환;최호준;고병두;조승한;황병복
    • Journal of the Korean Society for Precision Engineering
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    • v.20 no.12
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    • pp.148-158
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    • 2003
  • In this paper, efficient and accurate contact search algorithm is proposed for the contact problems by the finite element method. A slave node and a maser contact segment is defined using the side of a finite element on the contact surface. The specific goal is to develop techniques of reducing the nonsmoothness of the contact interactions arising from the finite element discretization of the contact surface. Contact detection is accomplished by monitoring the territory of the slave nodes throughout the calculation for possible penetration of a master surface. To establish the validity of the proposed algorithm, some different process and geometries examples were simulated. Efforts are focused on the error rate that is based on the penetrated area through the simulations fur large deformation with contact surface between deformable bodies. A proposed algorithm offers improvements in contact detection from the simulation results.

Wear Resistance Characteristics of Iron System MAG Weld Overlays with Chromium and Niobium Carbide Composite (Cr 및 Nb 복합탄화물에 의한 철계 MAG용접 오버fp이의 내마모 특성)

  • 김종철;박경채
    • Journal of Welding and Joining
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    • v.20 no.3
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    • pp.54-59
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    • 2002
  • Overlays is a treatment of the surface and near-surface regions of a material to allow the surface to perform functions that are distinct from those frictions demanded far the bulk of the material. Welding, thermal spray, quenching, carburizing and nitration have been used as the surface treatment. Especially, weld overlay is a relatively thick layer of filler metal applied to a carbon or low-alloy steel base metal for the purpose of providing a wear resistant surface. In this study, weld overlay was performed by MAG welding on the base metal(SS400) with filler metal which contain composite powders($Cr_3C_2+Mn+Mo+NbC$) and solid wire(JIS-YGW11). Characteristics of hardness and wear resistance on overlays were analyzed by EDS, EPMA, XRD and microstructures. Carbide formations were $M(Cr, Fe)_7C_3$ and NbC phases. And carbide volume fraction, hardness and specific wear resistance of overlays were increased with increasing powder feed rate and decreasing wire fred rate. Hardness and wear resistance were almost proportioned to carbide volume fraction of overlay.

Mineralogical Changes of Oyster Shells by Calcination: A Comparative Study with Limestone (소성에 따른 굴패각의 광물학적 특성변화: 석회석과의 비교 연구)

  • Lee, Jin Won;Choi, Seung-Hyun;Kim, Seok-Hwi;Cha, Wang Seog;Kim, Kangjoo;Moon, Bo-Kyung
    • Economic and Environmental Geology
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    • v.51 no.6
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    • pp.485-492
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    • 2018
  • About 300 thousand tones of oyster shells are produced annually and, thus, their massive recycling methods are required. Recently, a method, utilizing them as wet desulfurization materials after removal of organic matters and changing $CaCO_3$ phase into CaO through calcination, is under consideration. This study investigates the mineralogical changes (specific surface area, phase changes, surface state, etc.) of oyster shells by calcination and their characteristics were compared with those of limestone. Uncalcined oyster shells showed the higher specific surface area than limestone because the former are composed of platy and columnar structures. In contrast, investigated limestone showed a dense structure. The phase change of oyster shells occurred at lower temperature than that of limestone. The specific surface area of oyster shell decreased significantly after calcination while limestone depicted a drastic increase. Small amount of Na contained in oyster shell was suggested as the cause of this phenomenon; in that, it acted as a flux causing melting and sintering of oyster materials at lower temperature. Because of this, an additional phenomenon was observed that a part of shell materials remained untransformed even at higher calcination temperature and after longer treatment period due to the sintered surface, which covers the rest parts. Further studies investigating the effect of this phenomena from the perspective of desulfurization is required.

Investigation of Cutting Conditions for Stable Machining and Machinability Evaluation in Milling Process of Al7050-T7451 by Response Surface Methodology (Al7050-T7451 소재의 밀링가공에서 반응표면법에 의한 가공성평가 및 가공안정화를 위한 절삭조건선정)

  • Koo, Joon-Young;Cho, Mun-Ho;Kim, Hyuk;Kim, Jeong-Suk
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.23 no.3
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    • pp.284-290
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    • 2014
  • Aluminum alloy is a core material for structural parts of aircraft and automobiles to reduce the weight and maintain high specific strength. This study evaluates the machinability and investigates the optimal cutting conditions considering the surface integrity and productivity for Al7050-T7451 milling. The machining variables considered are the feed per tooth, spindle speed, axial depth of the cut, and radial depth of the cut. The machinability evaluation of Al7050-T7451 is conducted by analyzing the cutting force signals, acceleration signals, AE signals, and machined surface conditions. The optimal cutting conditions are determined by analyzing the experimental results using response surface methodology for stable machining considering the productivity and surface integrity.