• 한국자동차공학회논문집
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• 제5권3호
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• pp.54-65
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• 1997

To quantify the LII signals from soot particle of flames in diesel engine cylinder, a new method has been proposed for correcting LII signal attenuated by soot particles between the measuring point and the detector. It has been verified by an experiment on a laminar jet ethylene-air diffusion flame. Being proportional to the attenuation, the ratio of LII signal at two different detection wavelengths can be used to correct the measured LIIsignal and obtain the unattenuated LII signal, from which the soot volume fraction in the flame can be estimated. Both the 1064-nm and frequency-doubled 532-nm beams from the Nd : YAG laser are used. Single-shot, one-dimensional(1-D) line images are recorded on the intensified CCD camera, with the rectangular-profile laser beam using 1-mm-diameter pinhole. Two broadband optical interference filters having the center wavelengths of 647 nm and 400 nm respectively and a bandwidth of 10 nm are used. This two-wavelength correction has been applied to the ethylene-air coannular laminar diffusion flame, previously studied on soot formation by the laser extinction method in this laboratory. The results by the LII measurement technique and the conventional laser extinction method at the height of 40 nm above the jet exit agreed well with each other except around outside of the peaks of soot concentration, where the soot concentration was relatively high and resulting attenuation of the LII signal was large. The radial profile shape of soot concentration was not changed a lot, but the absolute value of the soot volume fraction around outside edge changed from 4ppm to 6.5 ppm at r=2.8mm after correction. This means that the attenuation of LII signal was approximately 40% at this point, which is higher than the average attenuation rate of this flame, 10~15%.

• 한국가시화정보학회지
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• 제2권1호
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• pp.12-17
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• 2004

The physical characteristics of soot near the soot inception point were investigated with various measurements. In-situ measurements of particle size and volume fraction were introduced based on time resolved laser-induced incandescence (TIRE-LII) and laser-induced ion mobility (LIIM). The one has more convenience and accuracy than conventional LII technique and the other works best for particle sizes of a few nanometers at high concentrations in a uniform concentration field. A complementary ex-situ measurement of particle size is nano differential mobility analyzer (Nano-DMA), which recently developed for measuring particle sizes between 2nm and 100nm and provides high-resolution size information for early soot. Particles will be also collected on transmission electron microscope (TEM) grids using rapid thermophoretic sampling and analyzed for morphology. These measurements will allow fresh and original insight into the characterizing soot inception process. The measured physical properties of incipient soot will clarify the controlling growth mechanism combined with chemical ones, and the dominant mechanism for soot modeling can be deduced from the information.

• 한국분무공학회지
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• 제17권4호
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• pp.185-191
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• 2012

Particulate matters (PM) that is generated by most diesel engine is regulated by the mass concentration measured by the conventional method it had been. Recently, Europe PMP (Particle Measurement Program) decided to start the regulation of vehicle's nano-sized particle number (PN) from the year of 2011 because of nano-particle's higher degree of harm to the human body. So firstly, the standard level of PN emission is introduced in the Euro 5/6 emissions regulation with a limit of $6{\times}10^{11}$ per km for light duty vehicle. Also KPMP(Korea Particle Measurement Program) was organized to copy quickly international technical trend. In this paper, it was investigated the nano-sized PN measurement characteristics for different particle generators between spray type and soot type. And the difference ratio between particle generators, the characteristic of PN concentration, counting efficiency and linearity was analyzed. Then, we make conclusions as followed. When particle diameter is increased, counting efficiency of two generators is decreased. Also Secondary calibration method is more higher 3% than Primary calibration method. Finally, SOF which is included in soot particles is not totally removed so it have great influence on test result of counting efficiency and linearity.

• 한국연소학회:학술대회논문집
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• 한국연소학회 2006년도 제32회 KOSCO SYMPOSIUM 논문집
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• pp.157-163
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• 2006

A new technique utilizing LII signal for the measurement of flow velocities of laminar diffusion flames has been investigated. Soot particles in ethylene diffusion flames are heated by a modulated Ar-ion laser beam. LII signals and their phase angles are measured using a lock-in amplifier at the different flame heights and the axial flow velocity are obtained from the measured phase angle delay. The measured velocities are similar to those from LDV measurements under the same operating conditions. The effects of laser power, LII signal wavelength, and modulation frequency are not sensitive to the velocity measurement. However, the choice of an optical chopper blade type could affect the measurement result. The use of a 6/5 chopper blade showed the better result that is possibly due to the square shape of modulated laser beam. This study successfully demonstrated that axial flow velocities of laminar diffusion flames can be measured by a new technique utilizing LII signal, which does not need particle seeding unlikely to LDV or PIV techniques.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 추계학술대회
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• pp.1140-1145
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• 2004

Laser-induced incandescence (LII) is introduced as a valuable tool for the characterization of nanoparticles in flame environments. This technique is based on the heating of the particles by a short laser pulse and the subsequent detection of the thermal radiation. It has been applied successfully for the investigation of soot in different fields of application. The evaluation of the temporal decay of the laser-induced incandescence (LII) signal from soot particles is introduced as a technique to obtain two-dimensional distributions of particle sizes and is applied to a laminar diffusion flame. This novel approach to soot sizing exhibits several theoretical and technical advantages compared with the established combination of elastic scattering and LII, especially as it yields absolute sizes of primary particles without requiring calibration. With this technique a spatially resolved 2-D measurement of soot primary particle sizes is feasible in a combination process form the ratio of emission signals obtained at two delay times after a laser pulse, as the cooling behavior is characteristic of particle size.

• 대한기계학회논문집B
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• 제29권12호
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• pp.1335-1343
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• 2005

The calibration technique of Time Resolved Laser Induced Incandescence was investigated both experimentally and numerically by using standard-sized carbon black particles for the instantaneous soot measurement at exhaust tail pipe in engine. The carbon black particles (19nm, 25nm, 45nm and 58nm) used in this study are similar, though not identical, to soot particle generated from flame not only in morphology but also in micro-structure. The amount of soot loading in flow was controled by a diluted gas (nitrogen) and was measured by the gravimetric method at exhaust pipe in calibrator. The successful calibrations of primary particle size and soot mass fraction were carried out at the range from 19nm to 58nm and from $0.25mg/m^3$ to $37mg/m^3$ respectively. And based on these results the numerical simulation of LII signal was tuned and the effect of an exhaust temperature variation on the decay rate of LII signal was corrected.

• 동력기계공학회지
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• 제16권4호
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• pp.5-11
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• 2012

There were some papers for diesel engine performance tests using BDF, but few article deals with the temperature and soot concentration of Bio diesel flame. Since the flame temperature of diesel engines is so high and change rapidly, an optical method for measurement of flame temperature is known as the most effective one. The two-color method regarding the visible wavelength radiation for the soot particles in flame was applied on Bio diesel flame in order to measure flame temperature and soot concentration in a diesel engine. Photo detecting device was newly designed and employed TSL250R, photo-diode, to pick-up the light information emitted from the combustion flame. As a result, real flame temperature T, as a flame brightness temperature, through Ta1, Ta2, were obtained and finally the characteristics of KL value as a soot concentration reveal the difference of combustion information between diesel fuel, blending oil and Bio diesel fuel oil.

• 한국자동차공학회논문집
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• 제13권1호
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• pp.51-59
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• 2005

Co-flow laminar diffusion flames' temperature has been studied experimentally for ethylene$(C_2H_4)$ using a co-flow burner in order to investigate the characteristics of diffusion flame's temperature distribution. The temperature distributions in the flame were measured by rapid insertion of a R-type thermocouple. The measurement area was divided into three zones. 1st area was expect to created PAH zone, Il nd area was expect to form soot zone, which is known to generate most soot volume fraction, and III rd area was expect to from soot oxidization zone. Also The temperature along the flame y-axis as a fuel quantity was measured. As a results, we have measured temperature neglecting the effect of soot particles attached to the thermocouple junction, which is close to the nozzle and upstream zone has a unstable flow in co-flow diffusion flame and acquires that the flame y-axis temperature has a uniform temperature in the generated soot volume fraction zone(II nd).

• 한국안전학회지
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• 제25권6호
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• pp.9-13
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• 2010

An experimental study for characteristics of soot were conducted at the post-flame region in jet diffusion flames, where carbon dioxide was used as additives in oxidizer stream. Light-extinction method was performed using He-Ne laser with wave length at 632.8nm for the measurement of relative soot density and soot volume fraction with dimensionless extinction coefficient, $K_e$ and mass specific extinction coefficient, ${\sigma}_s$. To increase of resolution, laser light was modified for sheet-form using concave, convex lenses and slit. C/H ratio was introduced for quantitative analysis of soot growth which is expressed by carbonization and dehydrogen. Also transmission electron microscopy(TEM) was used for observation of morphological shape. The results show that the relative soot density in the post-flame region was lower when carbon dioxide was added in oxidizer stream because of reduction of flame temperature.

• 한국연소학회:학술대회논문집
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• 한국연소학회 2000년도 제21회 KOSCO SYMPOSIUM 논문집
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• pp.175-182
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• 2000

Flame temperatures were measured and compared using a rapid insertion technique and a two-color pyrometry with Abel inversion process in co-flow ethylene diffusion flames. The measured line-of-sight temperature showed very limited usefulness in understanding the detailed soot formation/oxidation process in a co-flow diffusion flame. The flame temperatures could be measured with reasonable accuracy for the soot laden regions in ethylene diffusion flames using two-color pyrometry with an Abel inversion technique. Two-color-pyrometry with Abel inversion was demonstrated as a useful temperature measurement technique for co-flow diffusion flames, expecially under pressure conditions, where a thermocouple is not applicable. The soot volume fraction could be also obtained using tow-color pyrometry with Abel inversion, which provides important information for understanding the soot formation/oxidation mechanism in diffusion flames.