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Two-dimensional deformation measurement in the centrifuge model test using particle image velocimetry

  • Li, J.C.;Zhu, B.;Ye, X.W.;Liu, T.W.;Chen, Y.M.
    • Smart Structures and Systems
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    • v.24 no.6
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    • pp.793-802
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    • 2019
  • The centrifuge model test is usually used for two-dimensional deformation and instability study of the soil slopes. As a typical loose slope, the municipal solid waste (MSW) landfill is easy to slide with large deformation, under high water levels or large earthquakes. A series of centrifuge model tests of landfill slide induced by rising water level and earthquake were carried out. The particle image velocimetry (PIV), laser displacement transducer (LDT) and marker tracer (MT) methods were used to measure the deformation of the landfill under different centrifugal accelerations, water levels and earthquake magnitudes. The PIV method realized the observation of continuous deformation of the landfill model, and its results were consistent with those by LDT, which had higher precision than the MT method. The deformation of the landfill was mainly vertically downward and increased linearly with the rising centrifugal acceleration. When the water level rose, the horizontal deformation of the landfill developed gradually due to the seepage, and a global slide surface formed when the critical water level was reached. The seismic deformation of the landfill was mainly vertical at a low water level, but significant horizontal deformation occurred under a high water level. The results of the tests and analyses verified the applicability of PIV in the two-dimensional deformation measurement in the centrifuge model tests of the MSW landfill, and provide an important basis for revealing the instability mechanism of landfills under extreme hydraulic and seismic conditions.

Ultrasonic, Chemical Stability and Preparation of Self-Assembled Fullerene$[C_{70}]$-Gold Nanoparticle Films (자기조립 풀러렌$[C_{70}]$-금 나노입자 필름 제조와 초음파적, 화학적 안정성)

  • Ko, Weon-Bae;Shon, Young-Seok
    • Elastomers and Composites
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    • v.40 no.4
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    • pp.272-276
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    • 2005
  • [ $C_{70}$ ]-gold nanoparticle multilayer films were self-assembled using a 'dirt-ball' method on the reactive surface of glass slides functionalized with 3-aminopropyltrimethoxysilane. The functionalized glass slides were soaked in the solution containing both unmodified $C_{70}$ and ${\omega}$-amino-functionalized gold nanoparticles. Organic reaction (amination) facilitated the assembly of multilayer $C_{70}$-gold nanoparticle films, which have grown up to several layers. Chemical stability of $C_{70}$-gold nanoparticle films was studied by monitoring the changes in absorbance after the immersion of the films in acidic solution. In addition, ultrasonic stability of these nanoparticle films was studied by exposing them to ultrasonic irradiated surrounding, which resulted in partial desorption and a little aggregation of nanoparticles on solid surfaces.

Precise Static Contact Angle Measurements Using Pythagolas Rule (피타고라스 원리를 이용한 정적 접촉각 정밀 각도 측정방법)

  • Choi, Jin-Yeong;Kwon, Dong-Jun;Wang, Zuo-Jia;Shin, Pyeong-Su;Park, Joung-Man
    • Journal of Adhesion and Interface
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    • v.15 no.2
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    • pp.57-62
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    • 2014
  • Pythagolas rule was used for investigation of static contact angle in particular figures. Static contact angle measurement was important to evaluate the wettability between solid and liquid. Optimum measurement method and standardization of calculation for static contact angle were investigated for practical application. Optimum diameter of droplet for static contact angle measurement was confirmed as 1 mm. Contact angle measurement using Pythagolas rule was also used to calculate advancing, receding angle and wettability of different surface condition. At last, it was concluded that the Pythagolas rule method was more accurate than general lineation method for static contact angle measurement.

Solubility and Conformation of Silk Fibroin Membrane

  • Kweon, Hae-Yong;Kang, Seok-Woo;Lee, Kwang-Gill;Park, Kwang-Young;Jo, You-Young;Kang, Pil-Don;Sung, Gyoo-Byung;Lee, Heui-Sam;Yeo, Joo-Hong;Shin, Kyu-Hwan;Park, Chan-Hum
    • International Journal of Industrial Entomology and Biomaterials
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    • v.22 no.2
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    • pp.101-105
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    • 2011
  • Transparency and insolubility of eardrum patch against exudates are important for otolaryngological surgery. The author prepared silk fibroin (SF) films with various concentrations and temperature and then examined solubility and conformation of SF films. SF films were transparent regardless of the various preparation conditions. Although most SF films are soluble in 1X PBS solution at $37^{\circ}C$ for 1 h, the SF film with 3.4% with $60^{\circ}C$ was insoluble. Scanning electron microscopy (SEM) showed that the SF films have solid and smooth surface. Fourier transform infrared spectroscopy (FT-IR) and differential scanning calorimetry (DSC) results showed that the conformation of SF films was influenced by the preparation conditions including SF concentration and casting temperature. In conclusion, SF membrane with transparence and insolubility against exudates could be considered as eardrum patch resources.

Effect of Low-Plastic Fine Content on the Engineering Properties of Kaolinite-Sand Mixture (저소성 세립분 함량이 카올리나이트-모래 혼합토의 공학적 특성에 미치는 영향)

  • Kaothon, Panyabot;Lee, Su-Hyung;Choi, Yeong-Tae;Yune, Chan-Young
    • Journal of the Korean Geotechnical Society
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    • v.37 no.7
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    • pp.35-42
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    • 2021
  • An experimental study was carried out on kaolinite-sand mixtures with various proportions of kaolinite content. To investigate physical behaviour of mixtures, index properties and compaction test results were analysed in various aspects. Moreover, to clearly see the interaction between kaolinite and sand particles, the observational analysis through microscopic image analysis device was conducted. The test results showed that an increase in the amount of kaolinite could create a strong bonding structure which resulted in higher specific surface available for activities of kaolinite particles. Also, an increase in the amount of the kaolinite resulted in an increase in the percentage of water sorption. Then it could accelerate the occupation rate of water which tended to take up the space that would have been occupied by solid particles, and accordingly, resulted in the decreased maximum dry unit weight and increased initial void ratio. Based on the microscopic image analysis, the samples were individually classified into three types of mixture such as sand dominant, intermediate fine content, and fine dominant. In addition, the fine and coarse grains seem to interact well in the mixtures with the fine content ranging from 25 to 40%.

Effects of Particle Size and High Pressure Process on the Extraction Yield of Oil Compounds from Soybean Powder Using Hexane and Supercritical Fluid (입자 크기와 초고압 처리에 따른 유기용매와 초임계 유체 추출법에서의 대두유 추출수율의 변화)

  • Yoon, Won-Byong
    • Food Engineering Progress
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    • v.15 no.3
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    • pp.203-208
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    • 2011
  • Effects of particle size and high pressure processing on the extraction rate of oil compounds from soybean powder were evaluated by Soxhlet method using hexane and supercritical fluid extraction (SFE) using $CO_{2}$. SFE was carried out at 4,000 psi and $50^{\circ}C$ for 4 hr. The mean particle sizes were varied from 26.7 to 862.0 ${\mu}m$ by controlling milling time. Saturation solubility increased as the particle size decreased. At large particle size, high pressure processing (HPP) showed higher extraction yield in both hexane extraction and SFE, but, as the particle size decreased, the HPP was irrelevant to the extraction yield in SFE. The higher extraction rate obtained from the smaller particle size. The scanning electronic microscopy of soybean powder treated by HPP showed pores on the surface of the particle. The higher extraction rate and yield from HPP treatment might be due to the less internal resistance of transferring the solvent and miscellar in the solid matrix by collapsing of tissues.

Improved Coating of PEDOT : PSS onto CVD Graphene by the Addition of PVA (PVA의 첨가에 의한 CVD 그래핀상 PEDOT : PSS의 코팅성 향상)

  • Park, Min Ui;Shin, Chaeyeon;Kim, Hyeji;Kim, Seung Yeon;Choi, Young Ju;Chung, Dae-won
    • Applied Chemistry for Engineering
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    • v.29 no.6
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    • pp.734-739
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    • 2018
  • We successfully coated poly(3,4-ethylenedioxythiophene) : poly(styrene sulfonate) (PEDOT : PSS) on CVD graphene by adding poly(vinyl alcohol) (PVA) to PEDOT : PSS. Extensive studies on the wettability of coating solutions and electrical properties of formed films led us to conclude that PVA with 89% of the degree of saponification and the molecular weight of less than $100,000gmol^{-1}$ produced optimum results. Furthermore, the optimum content of PVA was found to be 5% of PEDOT : PSS by the solid weight. The film coated by PEDOT : PSS with PVA on CVD graphene displayed a conspicuous improvement in the surface roughness, adhesive property, bending durability and stability in resistance at $160^{\circ}C$, compared to those of using CVD graphene films.

Multi-slit prompt-gamma camera for locating of distal dose falloff in proton therapy

  • Park, Jong Hoon;Kim, Sung Hun;Ku, Youngmo;Kim, Chan Hyeong;Lee, Han Rim;Jeong, Jong Hwi;Lee, Se Byeong;Shin, Dong Ho
    • Nuclear Engineering and Technology
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    • v.51 no.5
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    • pp.1406-1416
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    • 2019
  • In this research, a multi-slit prompt-gamma camera was developed to locate the distal dose falloff of the proton beam spots in spot scanning proton therapy. To see the performance of the developed camera, therapeutic proton beams were delivered to a solid plate phantom and then the prompt gammas from the phantom were measured using the camera. Our results show that the camera locates the 90% distal dose falloff (= d90%), within about 2-3 mm of error for the spots which are composed $3.8{\times}10^8$ protons or more. The measured location of d90% is not very sensitive to the irradiation depth of the proton beam (i.e., the depth of proton beam from the phantom surface toward which the camera is located). Considering the number of protons per spot for the most distal spots in typical treatment cases (i.e., 2 Gy dose divided in 2 fields), the camera can locate d90% only for a fraction of the spots depending on the treatment cases. However, the information of those spots is still valuable in that, in the multi-slit prompt-gamma camera, the distal dose falloff of the spots is located solely based on prompt gamma measurement, i.e., not referring to Monte Carlo simulation.

Global Fitting Functions for Kinetics of Fe-Selective Chlorination in Ilmenite and Successive Chlorination of Beneficiated TiO2 (일메나이트 중 철의 선택적 염화와 선광된 TiO2의 추가 염화반응에 대한 글로벌 피팅함수)

  • Chung, Dong-Kyu;Won, Yong Sun;Kim, Yong-Ha;Jung, Eun-Jin;Song, Duk-Yong
    • Korean Journal of Materials Research
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    • v.29 no.7
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    • pp.412-424
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    • 2019
  • Global fitting functions for Fe-selective chlorination in ilmenite($FeTiO_2$) and successive chlorination of beneficiated $TiO_2$ are proposed and validated based on a comparison with experimental data collected from the literature. The Fe-selective chlorination reaction is expressed by the unreacted shrinking core model, which covers the diffusion-controlling step of chlorinated Fe gas that escapes through porous materials of beneficiated $TiO_2$ formed by Fe-selective chlorination, and the chemical reaction-controlling step of the surface reaction of unreacted solid ilmenite. The fitting function is applied for both chemical controlling steps of the unreacted shrinking core model. The validation shows that our fitting function is quite effective to fit with experimental data by minimum and maximum values of determination coefficients of $R^2$ as low as 0.9698 and 0.9988, respectively, for operating parameters such as temperature, $Cl_2$ pressure, carbon ratio and particle size that change comprehensively. The global fitting functions proposed in this study are expressed simply as exponential functions of chlorination rate(X) vs. time(t), and each of them are validated by a single equation for various reaction conditions. There is therefore a certain practical merit for the optimal process design and performance analysis for field engineers of chlorination reactions of ilmenite and $TiO_2$.

Dielectric and Electrical Characteristics of Lead-Free Complex Electronic Material: Ba0.8Ca0.2(Ti0.8Zr0.1Ce0.1)O3

  • Sahu, Manisha;Hajra, Sugato;Choudhary, Ram Naresh Prasad
    • Korean Journal of Materials Research
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    • v.29 no.8
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    • pp.469-476
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    • 2019
  • A lead-free bulk ceramic having a chemical formula $Ba_{0.8}Ca_{0.2}(Ti_{0.8}Zr_{0.1}Ce_{0.1})O_3$ (further termed as BCTZCO) is synthesized using mixed oxide route. The structural, dielectric, impedance, and conductivity properties, as well as the modulus of the synthesized sample are discussed in the present work. Analysis of X-ray diffraction data obtained at room temperature reveals the existence of some impurity phases. The natural surface morphology shows close packing of grains with few voids. Attempts have been made to study the (a) effect of microstructures containing grains, grain boundaries, and electrodes on impedance and capacitive characteristics, (b) relationship between properties and crystal structure, and (c) nature of the relaxation mechanism of the prepared samples. The relationship between the structure and physical properties is established. The frequency and temperature dependence of the dielectric properties reveal that this complex system has a high dielectric constant and low tangent loss. An analysis of impedance and related parameters illuminates the contributions of grains. The activation energy is determined for only the high temperature region in the temperature dependent AC conductivity graph. Deviation from the Debye behavior is seen in the Nyquist plot at different temperatures. The relaxation mechanism and the electrical transport properties in the sample are investigated with the help of various spectroscopic (i.e., dielectric, modulus, and impedance) techniques. This lead free sample will serve as a base for device engineering.