• Title/Summary/Keyword: Solid surface

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Study of Post Excimer Laser Annealing effect on Silicide Mediated Polycrystalline Silicon. (실리사이드 매개 결정화된 다결정 실리콘 박막의 후속 엑시머 레이저 어닐링 효과에 대한 연구)

  • Choo, Byoung-Kwon;Park, Seoung-Jin;Kim, Kyung-Ho;Son, Yong-Duck;Oh, Jae-Hwan;Choi, Jong-Hyun;Jang, Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.05a
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    • pp.173-176
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    • 2004
  • In this study we investigated post ELA(Excimer Laser Annealing) effect on SMC (Silicide Mediated Crystalization) poly-Si (Polycrystalline Silicon) to improve the characteristics of poly-Si. Combining SMC and XeCl ELA were used to crystallize the a-Si (amorphous Silicon) at various ELA energy density for LTPS (Low Temperature Polycrystalline Silicon). We fabricated the conventional SMC poly-Si with no SPC (Solid Phase Crystallization) phase using UV heating method[1] and irradiated excimer laser on SMC poly-Si, so called SMC-ELA poly-Si. After using post ELA we can get better surface morphology than conventional ELA poly-Si and enhance characteristics of SMC poly-Si. We also observed the threshold energy density regime in SMC-ELA poly-Si like conventional ELA poly-Si.

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The image construction of the surface and subsurface defects using complex amplitude of the reflected ultrasonic signals from the solid (초음파 반사신호의 복소 진폭을 이용한 교체 내부 결함의 영상 구조)

  • Kim, Hyun;Lim, Ho;Kim, Ki-Yeoul;Koo, Kil-Mo
    • The Journal of Information Technology
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    • v.4 no.2
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    • pp.129-136
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    • 2001
  • Most of the acoustic microscopes have been constructed acoustic image by simply measuring the amplitude of the reflected signal from the specimen. This method fails to produce images of good quality because the change in amplitude is not sensitive enough to specimen with fine variation. In this paper, we have been constructed the acoustic microscope system which has been able to measure simultaneously the amplitude and phase of the reflected ultrasonic signal. And also we have been constructed the amplitude and phase images for the 500 won coin as a sample and the alumium spacimen with internal round defect, and compared and analyzed these images. In expermental result, the phase image have shown better sensitive than the amplitude image and given better contrast for the micro height variation of specimen. It will be expected that the phase image can be used as an additional bit of information to improve ambiguituities in amplitude image on nondestructive testing for specimen with fine variation.

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Volumetric Capacitance of In-Plane- and Out-of-Plane-Structured Multilayer Graphene Supercapacitors

  • Yoo, Jungjoon;Kim, Yongil;Lee, Chan-Woo;Yoon, Hana;Yoo, Seunghwan;Jeong, Hakgeun
    • Journal of Electrochemical Science and Technology
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    • v.8 no.3
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    • pp.250-256
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    • 2017
  • A graphene electrode with a novel in-plane structure is proposed and successfully adopted for use in supercapacitor applications. The in-plane structure allows electrolyte ions to interact with all the graphene layers in the electrode, thereby maximizing the utilization of the electrochemical surface area. This novel structure contrasts with the conventional out-of-plane stacked structure of such supercapacitors. We herein compare the volumetric capacitances of in-plane- and out-of-plane-structured devices with reduced multi-layer graphene oxide films as electrodes. The in-plane-structured device exhibits a capacitance 2.5 times higher (i.e., $327F\;cm^{-3}$) than that of the out-of-plane-structured device, in addition to an energy density of $11.4mWh\;cm^{-3}$, which is higher than that of lithium-ion thin-film batteries and is the highest among in-plane-structured ultra-small graphene-based supercapacitors reported to date. Therefore, this study demonstrates the potential of in-plane-structured supercapacitors with high volumetric performances as ultra-small energy storage devices.

The Effect of Heat Treatment on the Microstructures and Mechanical Properties of Inconel 713C Alloy Vacuum Investment Castings (진공 정밀주조한 Inconel 713C 합금의 조직과 기계적 성질에 미치는 열처리의 영향)

  • Yoo, Byung-Ki;Choi, Hak-Kyu;Park, Heung-Il;Jeong, Hae-Yong
    • Journal of Korea Foundry Society
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    • v.40 no.2
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    • pp.16-24
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    • 2020
  • The effect of a heat treatment on the microstructure and mechanical properties of Inconel 713C alloy vacuum investment castings were investigated. The microstructure of the as-cast state was observed, showing well-developed dendrite structures and distributed carbide particles and solidified massive precipitates in the grain or grain boundary during solidification, in this case the γ′ phase and MC particles. During a heat treatment, the γ phase matrix was reinforced by solid solution elements, carbide particles from the film morphology precipitated along the grain boundary, and many micro-precipitates of second γ′ phases 0.2 ㎛~2 ㎛ in size were newly formed in the γ phase matrix according to SEM-EDS analysis results. The tensile strength at a high temperature (850℃) decreased slightly becoming comparable with the room-temperature result, while the hardness value of the specimen after the vacuum heat treatment increased by approximately 19%, becoming similar to that of the as-cast condition. However, the impact values at room temperature and low temperature (-196℃) were approximated; this alloy was mostly not affected by an impact at a low temperature. In the observations of the fracture surface morphologies of the specimens after the tensile tests, the fractures at room temperature were a mix of brittle and ductile fractures, and an intergranular fracture in the inter-dendrite structure and some dimples in the matrix were observed, whereas the fractures at high temperatures were ductile fractures, with many dimples arising due to precipitation. It was found that a reinforced matrix and precipitates of carbide and the γ′ phase due to the heat treatment had significant effects, contributing greatly to the excellent mechanical properties.

A Convenient System for Film Dosimetry Using NIH-image Software

  • Kurooka, Masahiko;Koyama, Syuji;Obata, Yasunori;Homma, Mitsuhiko;Imai, Kuniharu;Tabushi, Katsuyoshi
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.260-262
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    • 2002
  • An accurate measurement of dose distribution is indispensable to perform radiation therapy planning. A measurement technique using a radiographic film, which is called a film dosimetry, is widely used because it is easy to obtain a dose distribution with a good special resolution. In this study, we tried to develop an analyzing system for the film dosimetry using usual office automation equipments such as a personal computer and an image scanner. A film was sandwiched between two solid water phantom blocks (30 ${\times}$ 30 ${\times}$ 15cm). The film was exposed with Cobalt-60 ${\gamma}$-ray whose beam axis was parallel to the film surface. The density distribution on the exposed film was stored in a personal computer through an image scanner (8bits) and the film density was shown as the digital value with NIH-image software. Isodose curves were obtained from the relationship between the digital value and the absorbed dose calculated from percentage depth dose and absorbed dose at the reference point. The isodose curves were also obtained using an Isodose plotter, for reference. The measurements were carried out for 31cGy (exposure time: 120seconds) and 80cGy (exposure time: 300seconds) at the reference point. While the isodose curves obtained with our system were drawn up to 60% dose range for the case of 80cGy, the isodose curves could be drawn up to 80% dose range for the case of 31cGy. Furthermore, the isodose curves almost agreed with that obtained with the isodose plotter in low dose range. However, further improvement of our system is necessary in high dose range.

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Study on Real-Time Digital Filter Design as Function of Scanning Frequency of Focused Electron Beam (집속 전자 빔 장치에서 스캔 주파수에 따른 실시간 디지털 필터 설계에 관한 연구)

  • Kim, Seung-Jae;Oh, Se-Kyu;Yang, Kyung-Sun;Jung, Kwang-Oh;Kim, Dong-Hwan
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.35 no.5
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    • pp.479-485
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    • 2011
  • To acquire images in a thermionic-scanning electron-beam system, a scanning unit is needed to control the electron beam emitted from the tungsten filament source. In scanning the electron beam on the solid surface, the signalto-noise ratio depends on the scanning frequency. We used a digital filter to reduce noise by analyzing the real-time frequency of a secondary electron signal. The noise and the true image signal were well separated. We designed the digital filter via a DSP floating-point operation, and the noise elimination resulted in enhanced image quality in a highresolution mode.

Waste Reuse in Sugar Industries

  • Ansari, Abdul Khalique
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.122-131
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    • 2001
  • Pakistan being the 6$^{th}$ largest sugar producer has over 75 sugar mills with annual production capacity of about 2.4 million tons during 1996-97. The contribution of Sindh with 27 sugar mills is recorded over 50% of the total sugar production. The majority of the mills in Pakistan use the Defecation-Remelt-Phosphitation (DRP; 24 mills), Defecation-Remelt-Carbonation (DRC; 21 mills) and Defecation-Remelt Carbonation and Sulphitation (DRCS; 11 mills) process. Seven of the 75 sugar mills in Pakistan also produce industrial alcohol from molasses, a by- product of sugar manufacturing process. These sugar industries also produce fly ash, which have been found to contain unburned carbon and reach as far as four-kilo meter area with the wind direction, threatening the community health of people living around, besides posing other aesthetic problems. The untreated wastewater, in many cases, finds its way to open surface drains causing serious threat to livestock, flora and fauna. One study showed that fly ash emitted from the chimneys contain particle size ranging from 38 ${\mu}{\textrm}{m}$ to 1000 ${\mu}{\textrm}{m}$. About 50 per cent of each fly ash samples were above 300 ${\mu}{\textrm}{m}$ in size and were mostly unburned Carbon particles, which produced 85% weight loss on burning in air atmosphere at 1000${\mu}{\textrm}{m}$. This fly ash (mostly carbon) was the main cause of many health and aesthetic problems in the sugar mill vicinity. The environmental challenge for the local sugar mills is associated with liquid waste gaseous emission and solid waste. This paper discusses various waste recycling technologies and practices in sugar industries of Pakistan. The application of EM technology and Biogas technology has proved very successful in reusing the sugar industry wastewater and mud, which otherwise were going waste.

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Electrochemical Studies of Lithium Ion Battery Current Collector in the Aprotic Electrolytes: I. Al Current Collector (비수용성 전해질내 리튬이온전지용 집전체의 전기화학적 특성 연구: I. Al 집전체)

  • Park, Heai-Ku
    • Applied Chemistry for Engineering
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    • v.10 no.4
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    • pp.620-627
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    • 1999
  • Electrochemical properties of the Al current collector being used in lithium ion batteries have been studied in the 4 different aprotic electrolytes(1 M $LiBF_4$ EC : DMC, 1 M $LiBF_4$ EC : EMC. 1 M $LiPF_6$ EC : DMC. 1 M $LiPF_6$ EC : EMC) employing cyclic voltammetry and impedance measurement. Al electrode showed a wide range of the electrochemical window(0.5~4.1 V vs. $Li/Li^{+}$). However, solid interfacial materials has been formed on the Al surface due to reduction of impurities($H_2O$, $O_2$, etc), lithium salts, and electrolytes at low applied potentials, and aluminum oxides in the highly oxidizing potential as well. Especially, Al current collector was susceptible to localized in consequence of impurities in electrolytes.

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Determination of Analytical Method for the Insecticide Clothianidin and its Metabolites in Soil and Surface Water (토양 및 토양수 중 살충제 Clothianidin 및 대사산물 잔류분석법 확립)

  • Choi, Young-Joon;Kwon, Chan-Hyeok;Han, Byung-Soo;Lee, Young-Deuk
    • Korean Journal of Environmental Agriculture
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    • v.33 no.2
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    • pp.69-77
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    • 2014
  • BACKGROUND: The purpose of this study was to investigate the effects of clothianidin on the soil in terms of clothianidin dissipation and degradation to evaluate its safety in order to provide an analytical foundation for clothianidin and the 5 metabolites related to it. METHODS AND RESULTS: High-performance liquid chromatography(HPLC) was used to separate clothianidin and its metabolites in this study. In soil, after suppressing dissociation-proned ions with weak alkalic $NH_4OH$ and extracting the metabolites with methanol, clothianidin, Methylaminoimidazole(MAI), Methylnitroguanidine(MNG), Thiazolylmethylurea(TZMU) and Thiazolylnitroguanidine(TZNG). Thiazolylmethylguanidine(TMG) were extracted with the addition of neutral $NH_4OAC$ to increasing the intensity of ions. Compounding elements were separated by using Hydrometrix ($ChemElut^{TM}$) and ion-exchanging Solid-phase extraction(SPE) Strong cation-exchanger(SCX) and C18 were used. The recovery rates of clothianidin and 5 metabolites in soil and water ranged from 87.4% to 104.3%. A standard deviation of our analysis for the soil and water samples were less than 5%. CONCLUSION: Well accepted detection limits for clothianidin and 5 metabolites in soil samples based on a dissipation analysis is 0.005 mg/kg and 0.001 mg/L in water samples. The dissipation concentration of this study was decided to be enough to evaluate the dissipation levels of clothianidin and its metabolites.

A geochemical study on the saline waters circulating in an ash disposal pond of Seocheon Power Plant. Korea

  • Kim, Kang-Joo;Park, Seong-Min;Kim, Jin-San;Natarajan Rajmohan;Hwang, Gab-Soo;Yun, Seong-Taek;Kim, Hyun-Jung;Kim, Suk-Hwi
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.09a
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    • pp.338-341
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    • 2004
  • This study was carried out to understand the geochemistry of saline water circulating in an ash disposal pond of Seocheon power plant, Korea. For this study, ash pond waters, slurry water and seawater samples were collected and analyzed for major ions and trace elements. Results show that ash pond waters and slurry water are alkaline in nature due to high calcium content, and have high concentration of Ca, B, Li, As, Ba, Al, Si and Mn over seawater, suggest that these elements leached from fly ash even at high alkaline condition and ionic strength. Slurry water has high concentration of B, Ba, Li, Mn, Si and Sr compare to ash pond waters, expresses that these elements seem to be easily reached at initial stage fly ash-water interaction, and also might be associated with the surface of the fly ash particles. Additionally, PHREEQC program predicted several secondary solid phases, which are also influenced in the leaching of elements in to the saline water.

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