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The Effect of Heat Treatment on the Microstructures and Mechanical Properties of Inconel 713C Alloy Vacuum Investment Castings

진공 정밀주조한 Inconel 713C 합금의 조직과 기계적 성질에 미치는 열처리의 영향

  • Received : 2020.01.06
  • Accepted : 2020.03.10
  • Published : 2020.04.30

Abstract

The effect of a heat treatment on the microstructure and mechanical properties of Inconel 713C alloy vacuum investment castings were investigated. The microstructure of the as-cast state was observed, showing well-developed dendrite structures and distributed carbide particles and solidified massive precipitates in the grain or grain boundary during solidification, in this case the γ′ phase and MC particles. During a heat treatment, the γ phase matrix was reinforced by solid solution elements, carbide particles from the film morphology precipitated along the grain boundary, and many micro-precipitates of second γ′ phases 0.2 ㎛~2 ㎛ in size were newly formed in the γ phase matrix according to SEM-EDS analysis results. The tensile strength at a high temperature (850℃) decreased slightly becoming comparable with the room-temperature result, while the hardness value of the specimen after the vacuum heat treatment increased by approximately 19%, becoming similar to that of the as-cast condition. However, the impact values at room temperature and low temperature (-196℃) were approximated; this alloy was mostly not affected by an impact at a low temperature. In the observations of the fracture surface morphologies of the specimens after the tensile tests, the fractures at room temperature were a mix of brittle and ductile fractures, and an intergranular fracture in the inter-dendrite structure and some dimples in the matrix were observed, whereas the fractures at high temperatures were ductile fractures, with many dimples arising due to precipitation. It was found that a reinforced matrix and precipitates of carbide and the γ′ phase due to the heat treatment had significant effects, contributing greatly to the excellent mechanical properties.

Keywords

References

  1. W. Betteridge, D. Sc., F. Inst. P., F. I. M. and J. Heslop, Ph. D. F.IM., The Nimonic Alloys, Edward Arnold(Publishers) Limited, London (1974) 302-323.
  2. C.H. White, The Development of Gas Turbine Materials, G.W. Meetham (Ed.), Appl. Sci. Pub., London (1981) 89.
  3. W. Felix, The role of materials in gas turbines engineering, High-Temperature Material in Gas Turbines, Elsevier, Amsterdam (1974) 15-20.
  4. J.R. Davis, ASM Specialty Handbook, Heat-Resistant Materials, ASM International Materials, OH (1997) 222-227.
  5. "Engineering Properties of Alloy 713C", U. S. Patent #2,570, 193, produced under license from The International Nickel Company, Inc.
  6. AMS 5391, "Inconel 713C, Inconel 713LC Ni alloy"
  7. Hubert Matysiak, et. al.,"The microstructure degradation of the IN 713C nickel-based superalloy after the stress rupture tests", Journal of Materials Engineering and Performance, 23 (2014) 3305-3313. https://doi.org/10.1007/s11665-014-1123-4
  8. AMS Handbook, Vol 15 Casting, ASM International, OH (2004) 646-660.
  9. Investment casting handbook, Investment casting Institute, Revised (1979) Printed and by FEP International Private Limited, Jurong, Singapore (1979)
  10. ASM Handbook Vol. 15, 10th edition, Nickel and Nickel alloys. ASM International, OH 815-819.
  11. ASM Handbook Vol. 9, Metallography and Microstructures of heat-Resistant alloys, ASM International, OH 820-827.
  12. AMS 5391, "Ni alloy, Corrosion and Heat Resistant Investment Castings".
  13. ASM Handbook Vol. 15, 10th edition. Nickel and Nickel alloy, ASM International, OH 815-819.
  14. C. T. Sims and W. C. Hagel, The Superalloy, wiley, New York (1972) 70-74.
  15. Mathew J and Donachie, JR. Superalloys Source Book, ASM International, OH (1984) 65-66.
  16. F. Schubert, "Temperature and time dependent transformation, Application to Heat Treatment of High Temperature Alloys, Phase Stability in Temperature Alloy" (1980) 119-149.
  17. F. Zupanic a, T Boncina a, A Krizman a and F.D Tichelaar ba, Journal of Alloys and Compounds, "Structure of continuously cast Ni-based superalloy Inconel 713C", 329 (2001) 290-297. https://doi.org/10.1016/S0925-8388(01)01676-0
  18. F. Binczyk and J. Sleziona, Archives of Foundry Engineering, "Phase transformations and microstructure of IN-713C nickel superalloy", 9 (2009) 109-112.
  19. Yoo BK, Park HI, Bae CH, Kim SG and Jeong YH, "Effect of tungsten contents and heat treatment on the microstructures and mechanical properties of hastelloy C-276 alloy investment castings", J. Korea Foundry Society, 37 (2017) 21-29. https://doi.org/10.7777/jkfs.2017.37.1.21
  20. L., Rakoczy, M. Grudzien., R. Cygan and A. Zielin.Ska-Lipiec, Arch. Metall. Mater., "Effect of cobalt aluminate content and pouring temperature on microstructure, tensile strength and creep rupture of inconel 713C castings", 63 (2018) 1537-1545.