• Title/Summary/Keyword: SmCo

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Heat treatment characteristics of medium carbon steel by CW Nd:YAG Laser (CW Nd:YAG 레이저를 이용한 중탄소강의 열처리특성)

  • Shin H.J.;Yoo Y.T.;Ahn D.G.;Im K.
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.438-443
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    • 2005
  • Laser surface hardening is an effective technique used to improve the tribological properties and also to increase the service life of automobile components such as camshafts, crankshatfs, lorry brake drums and gears. High power CO2 lasers and Nd:YAG lasers are employed for localized hardening of materials and hence are of potential application in the automobile industries. The heat is conducted rapidly into the bulk of the specimen causing self-quenching to occur and the formation of martensitic structure. In this investigation, the microstructure features occurring in Nd:YAG laser hardening SM45C steel are discussed with the use of optical microscopic and scanning electron microscopic analysis. Moreover, This paper describes the optimism of the processing parameters for maximum hardened depth of SM45C steel specimens of 3mm thickness by using CW Nd:YAG laser. Travel speed was varied from 0.6m/min to 1.0m/min. The maximum hardness and case depth fo SM45C steel are 780Hv and 0.4mm by laser hardening.

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The Influence of Grain Size on the Fatigue Crack Propagation Behavior in the Low Carbon Steel (SM26C) (저탄소강재(SM25C)의 피로크랙 전파거동에 미치는 결정립 크기의 영향)

  • 김건호
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.76-82
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    • 2002
  • In this study, the rotary bending fatigue test was carried out with low carbon steel(SM25C). The specimens were heat-treated in order to change the grain size, and investigated items are fatigue limit, small crack initiation, fatigue crack propagation behavior and possibility of fatigue life prediction according to the different grain size. The summarized result are as follows ; Fatigue limit of the smooth specimen was dependent upon the grain size. The fatigue crack initiation of the small grain size specimen was delayed more than that of the large grain size specimen. And the small cracks of small grain size specimen were distributed in the narrow region of the main crack circumference contrary to the large grain size specimen. The main crack was grown along the grain boundary having co-alliance with small cracks. The experiment material has quantitatively disclosed the possibility of fatigue life prediction because the fatigue crack propagation behavior is dependent upon the grain size.

pH-Induced Micellization of Biodegradable Block Copolymers Containing Sulfamethazine

  • Shim, Woo-Sun;Lee, Jae-Sung;Lee, Doo-Sung
    • Macromolecular Research
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    • v.13 no.4
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    • pp.344-351
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    • 2005
  • pH-sensitive block copolymers were synthesized by coupling reaction of sulfamethazine and amphiphilic diblock copolymer, and their micellization-demicellization behavior was investigated. Sulfamethazine (SM), a derivative of sulfonamide, was introduced as a pH responsive moiety while methoxy poly(ethylene glycol)poly(D,L-lactide) (MPEG-PDLLA) and methoxy poly(ethylene glycol)-poly($D,L-lactide-co-{\varepsilon}-caprolactone$) (MPEG-PCLA) were used as biodegradable amphiphilic diblock copolymers. After the sulfamethazine was carboxylated by the reaction with succinic anhydride, the diblock copolymer was conjugated with sulfamethazine by coupling reaction in the presence of DCC. The critical micelle concentration (CMC) and mean diameter of the micelles were examined at various pH conditions through fluorescence spectroscopy, dynamic light scattering and transmission electron microscopy. For MPEG-PDLLA-SM and MPEG-PCLA-SM solutions, the pH-dependent micellization-demicellization was achieved within a narrow pH band, which was not observed in the MPEG-PDLLA and MPEG-PCLA solutions. The micelle showed a spherical morphology and had a very narrow size distribution. This pH-sensitive block copolymer shows potential as a site-targeted drug carrier.

Determination of Silymarin and Silybin Diastereomers in Korean Milk Thistle using HPLC/UV Analysis (HPLC 분석을 통한 한국산 밀크씨슬 중 실리마린과 실리빈의 정량)

  • Kim, Juree;Paje, Leo Adrianne;Choi, Jung Won;Lee, Hak-Dong;Shim, Jae Suk;Shim, Jeehyoung;Geraldino, Paul John L.;Lee, Sanghyun
    • Korean Journal of Pharmacognosy
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    • v.51 no.4
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    • pp.297-301
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    • 2020
  • Silymarin (SM) and silybin diastereomers (SD) in milk thistle (Silybum marianum) were determined using high-performance liquid chromatography and quantified using a reverse-phase column in a gradient elution system. UV detection was performed at 288 nm. The content of SM and SD in milk thistle was 3.236 and 0.553 mg/g DW, respectively. Determining the presence and quantifying the content of SM and SD in milk thistle are vital for the pharmaceutical industry to identify optimal sources for developing health supplements or therapeutics.

Microstructure and wear performance of WC-6.5%Co cladding layer by electric resistance welding (저항 클래딩법에 의해 형성된 내마모성 WC-6.5Co 클래딩층의 미크로조직 및 내마모성능)

  • Lee, Jin-U;Bae, Myeong-Il;Kim, Sang-Jin;Lee, Yeong-Ho
    • Proceedings of the KWS Conference
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    • 2006.10a
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    • pp.120-122
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    • 2006
  • This study deals with characterizations of microstructure and wear performance of a cladding layer, product on 1.9 mm-thick mild steel plate by the electric resistance welding, of composite metal powder of Coarse WC-6.5%Co and high carbon alloy(SHA). The cladding layer was examined and tested fur microstructural features, chemical composition, hardness, wear performance and wear mechanism. The cladding layer have two different matrix were observed by an optical microscope and EPMA. The one was the coarse WC-6.5Co structure. The other was the melted SHA with surrounding the WC-6.5Co structure. The hardness of WC-6.5Co was 1210HV. The hardness of SHA was 640HV. In comparison by wear rate, the cladding layer showed the remarkable wear performance that was 15 times of SM490 and about 62% of D2.

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Effect of Addition Elements on the Production of the 2-17 Type High Performance of the Rare Earth Permanent Magnet Materials by the Reduction and Diffusion Process (환원·확산법에 의한 2-17형 고성능 희토류영구자석 재료의 제조에 있어서 첨가원소의 영향)

  • Song, Chang-Been;Cho, Tong-Rae
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.4
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    • pp.333-339
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    • 1995
  • The reduction and diffusion process(R-D process) is an economical way to produce the functional materials which contain rare-earth elements and has been applied to the production of rare-earth magnet meterials($SmCo_5$, $Nd_{15}Fe_{77}B_8$), magneto-optical(MO) target materials and hydrogen storage alloy, etc. However, because of difficult to control of the final composition, the R-D process has not been applied to production of the 2-17 type rare earth permanent magnet materials which contain several elements. Therefore, this work was as a basic study for the production of the 2-17 type rare earth permanent materials with composition $Sm(Co_{0.72}Fe_{0.21}Cu_{0.05}Zr_{0.03})_{7.9}$ by the R-D process, the following were mainy examined ; the amount of metallic calcium as a reductant, homogenization condition of the alloy after the R-D reaction, masuring of magnetic properties of the sample after step aging. The sample prepared by the R-D process contained a little more oxygen than that prepared by the melting method, however, showed almost the same magnetic properties.

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