• Title/Summary/Keyword: Slurry mixing

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Evaluation of Gelation Characteristics with The Variation of Additive Contents in The Alumina Slurry for Gel Casting Process (겔 캐스팅 공정을 위한 알루미나 슬러리에서의 첨가제 함량 변화에 따른 겔화특성 평가)

  • Chung, J.K.;Oh, C.Y.;Ha, T.K.
    • Transactions of Materials Processing
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    • v.31 no.5
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    • pp.290-295
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    • 2022
  • Recently, the use of high-tech ceramic parts in functional electronic parts, automobile parts and semiconductor equipment parts is increasing. These ceramics materials are required to have high reproducibility, reliability, large size and complex shapes. The researchers initiated the work to develop a new shaping method called gel casting, which allows high performance ceramic materials with a complex shape to be produced. The manufacturing process parameters of gel casting include uniform mixing of the initiator, bubble removal, and slip injection. In this study, we analyzed the dispersion and gelation characteristics according to the change in the additive content of the alumina slurry in the gel casting process. The alumina slurry for gel casting was prepared by mixing a solvent, a monomer and a dispersant through a ball mill. Alumina powder and a gelation initiator were added to the mixed solution, and ball milling was performed for 24 hours. A viscosity of 6,435 cps and a stable zeta potential value were obtained under the conditions of alumina powder content of 55 vol% and dispersant 2.0 wt%. After curing for 12 hours by adding aps 0.1wt%, TEMED 0.2wt%, and Monomer 3, 5wt%, it was possible to separate from the molding cup, confirming that the gelation was completed.

Microstructure and Magnetic Properties of Nanostructured Fe-Co Alloy Powders Produced by Chemical Solution Mixing and Hydrogen Reduction Methods (화학용액혼합과 수소환원법으로 제조된 나노 구조 Fe-Co 합금분말의 미세구조 및 자성 특성)

  • 박현우;이백희;이규환;김영도
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.333-336
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    • 2003
  • The purpose of this study is the fabrication of nano-sized Fe-Co alloy powders with soft magnetic properties by the slurry mixing and hydrogen reduction (SMHR) process. $FeCl_2$0 and $CoCl_2$ powders with 99.9% purities were used for synthesizing nanostructured Fe-Co alloy powder. Nano-sized Fe-Co alloy powders were successfully fabricated using SMHR, which was performed at 50$0^{\circ}C$ for 1 h in H$_2$ atmosphere. The fabricated Fe-Co alloy powders showed $\alpha$' phase (ordered body centered cubic) with the average particle size of 45 nm. The SMHR powder exhibited low coercivity force of 32.5 Oe and saturation magnetization of 214 emu/g.

A District Cooling System using Ice Slurry for the Uncertain Cooling Load of the Future (미래의 불확실한 냉방부하에 대한 아이스슬러리를 이용한 지역냉방시스템)

  • Lee, Yoon-Pyo;Ahn, Young-Hwan;Yoon, Seok-Mann
    • Proceedings of the SAREK Conference
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    • 2006.06a
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    • pp.233-238
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    • 2006
  • A new district cooling system using ice slurry for the uncertain cooling load of the future is presented. The chilled water produced by the absorption chillers is used for the base cooling load. The temperature of the chilled water is reduced by mixing of ice slurry depending on increasing of the cooling load. Finally, IPF of the ice slurry is increased up to 10% at the peak load. The transporting mass flow rate is decreased down to 44.7%, and the diameter of the main pipe is decreased down to 66.7%, but the diameter of the branched pipe is designed as the same size of the chilled water.

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Effect of curing temperature on the properties of ground granulated blast furnace slag-cement bentonite slurry

  • Kim, Taeyeon;Lee, Bongjik;Hong, Seongwon
    • Geomechanics and Engineering
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    • v.29 no.3
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    • pp.237-247
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    • 2022
  • To investigate the curing temperature effect on the engineering properties of ground granulated blast furnace slag-cement bentonite (GGBS-CB) slurry for cutoff walls, the laboratory experiments including the setting time, unconfined compressive strength, and permeability tests were carried out. The mixing procedure for GGBS-CB slurry was as follows: (1) montmorillonite-based bentonite slurry was first fabricated and hydrated for four hours, and (2) cement or GGBS with cement was added to the bentonite slurry. The dosage range of GGBS was from 0 to 90 % of cement by mass fraction. The GGBS-CB slurry specimens were cured and stored in environmental chamber at temperature of 14±1, 21±1, 28±1℃ and humidity of 95±2% until target days. The highest average temperature of three seasons in South Korea was selected and used for the tests. The experimental results indicated that in early age (less than 28 days) of curing the engineering properties of GGBS-CB slurry were primarily affected by the curing temperature, whereas the replacement ratio of GGBS became a main factor to determine the properties of the slurry as the curing time increased.

Effect of the Application of a Suspended and a Mixing-in-Pipe Type Aerator on the Liquid Fertilization of Pig Manure Slurry (현수, 배관 내 혼합 폭기방식 적용이 돼지분뇨 슬러리의 액상 비료화에 미치는 영향)

  • Jeong, Kwang Hwa;Kim, Jung-Kon;Khan, Modabber Ahmed;Kwag, Jung-Hoon;Han, Duk-Woo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.22 no.4
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    • pp.62-71
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    • 2014
  • Three types of diffuser systems were manufactured and applied to investigate the effect of liquid fertilization of pig manure slurry by application of aeration processes. In the first type reactor, commonly used diffuser system, which diffuse air upward by diffusing aerator fixed at the bottom of the reactor is installed. In case of the second type, air diffuser is installed 10 cm above of the bottom of a reactor. In the third type reactor, the venturi-type air diffuser is installed at circulation pipe, which return pig slurry in the reactor(mixing-in-pipe process). The pig manure slurry separated to solid/liquid was flowed into the experimental reactor, and left as it for one week to precipitate solids. The concentration of organic matter, T-N, T-P and BOD in the raw pig manure slurry flowed into the reactor of bottom-fixed type aeration process were 1.82%, 4,400 mg/L, 360 mg/L and 13,542 mg/L, respectively. After aeration the concentration of organic matters, T-N, T-P and BOD in the slurry were 2.01%, 4,400 mg/L, 420 mg/L and 16,824 mg/L, respectively. The concentration of organic matter, T-N, T-P and BOD in the mixing-in-pipe type changed from 1.58%, 3,700 mg/L, 260 mg/L and 15,735 mg/L to 1.96%, 4,000 mg/L, 340 mg/L, and 18,098 mg/L, respectively. Changes of the concentration of organic matter, T-N, T-P and BOD of the pig manure slurry collected from the middle layers of two aeration reactors; bottom aeration process and the mixing-in-pipe process, were 10.4%, 0%, 16.7% and 24.2% and 24.0%, 8.1%, 30.8% and 15.0%, respectively. The thickness of foam layer generated on the surface of pig manure slurry in aeration tank was thinner in mixing-in-pipe reactor than bottom-fixed type aeration reactor.

Effects of Solids Content and Mixing Speed in Treatment of Petroleum Hydrocarbon Contaminated Soils using a Bioreactor (고형물함량 및 혼합강도가 생물반응기를 이용한 석유계탄화수소 오염토양의 처리에 미치는 영향)

  • 김수철;남궁완;박대원
    • Journal of Korea Soil Environment Society
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    • v.2 no.3
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    • pp.23-30
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    • 1997
  • The purpose of this study was to evaluate effects of solids content and mixing speed in treatment of petroleum hydrocarbon contaminated soils using a slurry-phase bioreactor. Performance results on slurry-phase bioremediation of diesel fuel contaminated soil were generated at the bench-scale level. The fate of TPH(Total Petroleum Hydrocarbon) was evaluated in combination with biological treatment. Abiotic and biotic fate of the TPH were determined using soil not previously exposed to compounds in diesel fuel. The reactor volume for given throughput can be reduced by maximizing the solids content. Applications of 50% and 20% solids content(dry weight basis) were showed a little difference(57.5% : 61.6%) in biological TPH removal rate each other. Mixing and particle suspension are critical to desorption and biological degradation. In this standpoint, this study was performed using two mixing speed. When the reactor was operated at 70rpm, it had a better result in the particle suspension and TPH removal rate than the reactor with mixer rotated at 20rpm. In the reactor applied 20rpm, it was resulted in failure of particle suspension.

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Mixed Nano Silica Colloidal Slurry for Reliability Improvement of Sapphire Wafer CMP Process (사파이어 웨이퍼 CMP 공정 신뢰성 향상을 위한 혼합 나노실리카 콜로이달 슬러리)

  • Chung, Chan Hong
    • Journal of Applied Reliability
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    • v.14 no.1
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    • pp.11-19
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    • 2014
  • A colloidal silica slurry has been manufactured by mixing nano silica powders having different grain size to improve the reliability of Sapphire wafer CMP process. The main reliability problem of CMP process such as the breaking of wafer can be prevented by reducing the size of particles in a slurry. While existing commercial colloidal silica slurries are usually made of single grain size silica powder of about 120nm, in the present study 40nm and 100nm silica powders are mixed to achieve a similar removal rate. The new colloidal silica slurry showed wafer removal rate of $3.04{\mu}m/120min$ while that of a commercial colloidal silica slurry was $3.03{\mu}m/120min$. The roughness was less than $4{\AA}$ and scratch was 0. It is also expected that the reduction of the size of nano silica particles can improve the dispersion stability and prolong the useful life of the slurry.

A Study of the Physical Properties of Slurry and Mineral Hydrate Insulation Mixed with Polypropylene Fiber (폴리프로필렌 섬유 혼입 슬러리와 미네랄 하이드레이트 단열소재의 물리적 특성에 관한 연구)

  • La, Yun-Ho;Park, Jae-Wan;Chu, Yong-Sik
    • Journal of the Korean Ceramic Society
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    • v.52 no.1
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    • pp.13-18
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    • 2015
  • The fabrication method used for mineral hydrate is similar to that of ALC (autoclaved lightweight concrete), but the fabrication of normal slurry with a considerable amount of a foaming agent is difficult due to material separation and collapse of the slurry. Therefore, the development of fabrication methods for normal slurry is necessary. The final product, mineral hydrate insulation, has excellent thermal properties but poor strength characteristic given the many pores. In this study, in order to fabricate normal slurry, the viscosity and foaming time of the slurry were controlled. The mixing ratio of the starting material and the polypropylene fiber was controlled to improve the strength. Mineral hydrate with polypropylene fiber showed a higher strength than that without this type of fiber. Specifically, the compressive strength of mineral hydrate with 2% polypropylene fiber added to it was more than 40% higher than that without the fiber.

The effect of chemical kinetics of slurry components on Cu CMP (화학반응속도가 Cu CMP에 미치는 영향)

  • Jung, Won-Duck;Chang, One-Moon;Park, Sung-Min;Jeong, Hae-Do
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.11a
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    • pp.372-373
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    • 2006
  • Chemical kinetics affects Cu CMP results (removal rate, Non uniformity etc.) Because Cu is removed by chemical action. Key factors in chemical kinetics are process temperature and concentration of slurry components. In this study, Hydrogen peroxide and citric acid were selected as a oxidant and a complexing agent and Slurry were made by mixing this components. In order to study effects of Chemical Kinetics, X-ray photoelectron spectroscopy (XPS) were performed on Cu sample after etching test as concentration of citric acid and slurry temperature. Finally Cu CMP was performed as same conditions.

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Polymer Base Bored Pile in Bangkok Subsoils

  • Teparaksa, Wanchai
    • Proceedings of the Korean Geotechical Society Conference
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    • 2008.10a
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    • pp.407-426
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    • 2008
  • The bentonite slurry has been used as the stabilize suspension for wet process bored pile construction in Thailand. The bentonite suspension has benefit on filtration in the sand layer, but it creates thick cake film along pile shaft and loose sedimentation at pile toe. The base grouting technique was widely used to rectify the soft base or loose sedimentation problem of bored pile. The base grouting technique was not increased only end bearing capacity, but was also more increase in skin friction capacity of the bored piles. The comprehensive researches on base grouting was carried out by installing PVC casing inside the shaft to allow the drilling through the pile base in order to collect the soil sample below the pile tip. The polymer based slurry recently was used to replace the bentonite slurry to overcome the thick cake film along pile shaft as well as loose sedimentation at pile toe. The extent research on polymer slurry by physical model was performed to verify the real behavior of polymer. The appropriate mixing ratio of polymer was proposed. The design skin friction coefficient, $\beta$ and end bearing coefficient, Nq, for sand layer base on fully instrumented tested pile were proposed. The application on remedial of the lose capacity bored pile with large displacement in Bangladesh was proposed and discussed.

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