• 제목/요약/키워드: Size-distribution

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세라믹스의 파괴강도에 관한 확률론적 해석 (A Probabilistic Analysis on Fracture Strength of Ceramics)

  • 김선진
    • 한국해양공학회지
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    • 제10권2호
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    • pp.61-68
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    • 1996
  • Weibull distribution function is applied very successfully to the strength of brittle materials such as ceramics and the weakest link model is applied to explain the ovents. This paper deals with the effect of specimen size on the strength of ceramics. The values of tensile strength were calculated by the Monte-Calro simuation. The tensile strength obtained was plotted on Weibull probabillity papers and represented by the 3-parameter Weibull distribution. The strength distribution function was compared with the theoretical weibull distribution. As a result, it was found that the Weibull shape parameter was changed due to the size and there was a possibility of a false indication as if the weakest link model holds good. We should be very careful when we apply the Weibull statistics to estimate the strength of products.

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원통형 조사창에서의 양끝내포선 길이분포를 이용한 절리크기분포 추정 연구 (Estimation of Joint Size Distribution Using a Contained Trace Length Distribution in a Cylindrical Window)

  • 서가현;송재준
    • 터널과지하공간
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    • 제26권3호
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    • pp.201-211
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    • 2016
  • 본 연구에서는 3차원 원통형 조사창에서의 양끝내포선 길이 분포를 이용하여 절리 직경 분포 추정을 수행하였다. 추정 결과의 수치적인 오차를 줄이기 위하여, 보조변수를 도입한 개선된 방안을 제시하였다. 몬테-카를로 시뮬레이션으로 검증한 결과, 보조변수의 변화에 따라 추정 분포의 진동이 줄어들어 오차가 크게 감소한 것을 확인하였다. 또한 절리 직경의 최적 분포 및 적정한 보조변수 값을 찾기 위한 알고리즘을 제안하였다.

폴리에테르술폰 정밀여과막의 제조 및 특성 연구 (Preparation and Characteristics of Polyethersulfone Microfiltration Membranes)

  • 김노원
    • 멤브레인
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    • 제17권4호
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    • pp.329-337
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    • 2007
  • 본 연구에서는 p-toluenesulfonic acid (TSA)와 polyvinylpyrrolidone (PVP)를 함유한 polyethersulfone (PES) 고분자 용액을 이용하여 PES 멤브레인 내에 최소 공경을 갖는 내부 분리층을 만드는 방법에 관한 새로운 방법을 제시하고자 한다. 팽윤제로 사용된 PVP와 응고제로 사용된 TSA를 함유한 평막형 PES 멤브레인의 제조 및 구조적인 특성 조사가 수행되었으며, 상업용 막에 대등할 만한 투과 성능과 좁은 pore size distribution을 가지는 멤브레인을 제조할 수 있음을 확인하였다. 또한 PVP의 첨가는 멤브레인의 단면구조와 투과 성능에, TSA는 투과 성능보다는 pore size distribution에 영향을 준다는 것을 확인하였으며 이는 FE-SEM 결과와 TSA를 첨가한 멤브레인의 단면 사진에서 내부 최소 기공층의 두께가 두꺼워짐을 확인할 수 있었다.

제주도 해안가에서 측정된 에어로졸의 성분별 입경분포 특성 (Size Distribution of Ambient Aerosol Measured at a Coastal Site in Jeju Island)

  • 이기호;양희준;허철구
    • 한국환경과학회지
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    • 제12권10호
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    • pp.1043-1054
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    • 2003
  • During the period from April to September 2002, the size distributions of ambient aerosol were measured at the coastal site at Hamduk in Jeju Island. Na$\^$+/, K$\^$+/, Mg$\^$2+/, Ca$\^$2+/and Cl$\^$-/ exhibited mostly a bimodal coarse mode size distribution, while ammonium and sulfate were mainly in the fine size range, with maximum at around 0.54$\mu\textrm{m}$. The average molar concentration ratio of ammonium to sulfate for fine particles was equal to 2.0${\pm}$0.9. Nitrate was evenly found in both the coarse and fine modes. Elements like Al, Fe, Cu, Mg, Na, Ti, Sr and Mn were dominant in coarse particles, with the maximum at around 5.25$\mu\textrm{m}$. S and Pb were mainly in the submicrometer size range. Other elements with a fine and coarse modes were V, Ni, Cu, Ba and Mo. The patterns of the size distributions of trace elements measured at the downtown in Jeju City were very similar to those at the coastal site in Hamduk. However, the amplitude of size fractional concentrations at Jeju City was narrower than that at Hamduk. While the mass median diameters for the chemical species originated from the natural origin such as marine and crust were relatively large, those for ammonium, sulfate, S and Pb were very small.

Synthesis of scheelite-type nanocolloidal particles by pulsed laser ablation in liquid and their size distribution analysis

  • Lee, Jung-Il;Shim, Kwang Bo;Ryu, Jeong Ho
    • 한국결정성장학회지
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    • 제24권3호
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    • pp.111-119
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    • 2014
  • A novel pulsed laser ablation process in liquid was investigated to prepare scheelite-type ceramic [calcium tungstate ($CaWO_4$) and calcium molybdate ($CaMoO_4$)] nanocolloidal particles. The crystalline phase, particle morphology, particle size distribution, absorbance and optical band-gap were investigated. Stable colloidal suspensions consisting of well-dispersed $CaWO_4$ and $CaMoO_4$ nanoparticles with narrow size distribution could be obtained without any surfactant. Particle tracking analysis using optical microscope combined with image analysis was applied for a fast determination of particle size distribution in the prepared nanocolloidal suspensions. The mean nanoparticle size of $CaWO_4$ and $CaMoO_4$ colloidal nanoparticles were 16 nm and 30 nm, with the standard deviations of 2.1 and 5.2 nm, respectively. The optical absorption edges showed blue-shifted values about 60~70 nm than those of reported in bulk crystals. And also, the estimated optical energy band-gaps of $CaWO_4$ and $CaMoO_4$ colloidal particles were 5.2 and 4.7 eV. The observed band-gap widening and blue-shift of the optical absorbance could be ascribed to the quantum confinement effect due to the very small size of the $CaWO_4$ and $CaMoO_4$ nanocolloidal particles prepared by pulsed laser ablation in liquid.

Effects of the Size and Distribution of Preflocculated GCC on the Physical Properties of Paper

  • Lee, Kyong-Ho;Lee, Hak-Lae;Youn, Hye-Jung
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2006년도 PAN PACIFIC CONFERENCE vol.1
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    • pp.85-90
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    • 2006
  • Increasing the filler content of sheet improves the optical properties and printability of paper and provides an opportunity for saving production cost through fiber replacement with relatively low-priced filler. But increasing the filler content tends to decrease the strength of paper and filler retention. It also tends to deteriorate drainage on the paper machine. To overcome these problems, preflocculation technology of fillers may be employed. Many research efforts have been made on the properties of preflocculated filler, namely prefloc, whose size and size distribution were influenced by polymer type and shear level. But there is much to be investigated about the effect of the prefloc characteristics on the physical properties of paper. To evaluate the effect cationic polymers on the size and size distribution of preflocculated GCC and their shear stability, cationic PAM and cationic starch were used. The influence of the preflocculation on filler retention and its surface distribution, and the changes of physical and optical properties of handsheets affected by the characteristics of preflocs were examined. Filler distribution on sheet surface was also analyzed by EPMA. Results showed that cationic PAM formed large preflocs at low dosage. Cationic starch was required to add 15 times as much as cationic PAM to obtain the preflocs with similar size. But preflocs formed with cationic starch was superior in shear stability to those formed with cationic PAM. Filler preflocculation technology could provide an opportunity of increasing filler content significantly without loss in tensile strength. And increased filler contents could compensate brightness loss which often accompanies filler preflocculation. When excessively large preflocs were used, however, brightness loss rather than the improvement in tensile strength was predominant. Therefore it is of great importance to produce preflocs with proper size and shear stability for maximizing the improvement of physical properties of papers.

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[Retraction]Size measurement and characterization of ceria nanoparticles using asymmetrical flow field-flow fractionation (AsFlFFF)

  • Kim, Kihyun;Choi, Seong-Ho;Lee, Seungho;Kim, Woonjung
    • 분석과학
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    • 제32권5호
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    • pp.173-184
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    • 2019
  • As the size of semiconductors becomes smaller, it is necessary to perform high precision polishing of nanoscale. Ceria, which is generally used as an abrasive, is widely used because of its uniform quality, but its stability is not high because it has a high molecular weight and causes agglomeration and rapid precipitation. Such agglomeration and precipitation causes scratches in the polishing process. Therefore, it is important to accurately analyze the size distribution of ceria particles. In this study, a study was conducted to select dispersants useful for preventing coagulation and sedimentation of ceria. First, a dispersant was synthesized and a ceria slurry was prepared. The defoamer selection experiment was performed in order to remove the air bubbles which may occur in the production of ceria slurry. Dynamic light scattering (DLS) and asymmetrical flow field-flow fractionation (AsFlFFF) were used to determine the size distribution of ceria particles in the slurry. AsFlFFF is a technique for separating nanoparticles based on sequential elution of samples as in chromatography, and is a useful technique for determining the particle size distribution of nanoparticle samples. AsFlFFF was able to confirm the presence of a little quantities of large particles in the vicinity of 300 nm, which DLS can not detect, besides the main distribution in the range of 60-80 nm. AsFlFFF showed better accuracy and precision than DLS for particle size analysis of a little quantities of large particles such as ceria slurry treated in this study.

모래 입도분석을 위한 스마트폰 디지털 이미지 처리 방법 (Smartphone Digital Image Processing Method for Sand Particle Size Analysis)

  • 허주영;천세현
    • 한국해안·해양공학회논문집
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    • 제35권6호
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    • pp.164-172
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    • 2023
  • 백사장 모래의 입도분포는 해빈의 침식과 퇴적을 파악하는 데 중요한 정보를 제공한다. 모래의 입도분포 분석에 보편적으로 사용되는 체가름시험은 분석 시간이 길고 개별 입자의 형상과 색에 대한 정보를 얻을 수 없다는 한계점이 있다. 본 연구에서는 체가름시험법 보다 측정 과정이 간편하고 효율적인 스마트폰 디지털 이미지를 이용한 입도분포 분석 방법을 제안하였다. 이미지 분석 과정 중 이미지 기울기(Image Gradient) 계산을 통한 입자 경계 추출로 해상도가 상대적으로 낮은 스마트폰 디지털 이미지의 배경으로부터 입자를 효과적으로 검출하였다. 경상북도 4곳의 해수욕장에서 채취한 시료를 이용해 본 연구에서 제안한 경계 추출 이미지 분석법과 경계를 추출하지 않는 분석법을 각각 체가름시험 결과와 비교 검증하였을 때, 본 연구에서 제안한 방식은 D50에서 평균 8.21%의 평균 오차율을 보여 경계를 추출하지 않는 분석법 보다 65% 낮은 오차를 보였다. 따라서 스마트폰 디지털 이미지를 이용한 입도분포 분석은 간편하고 효율적이며 체가름시험에 준하는 정확성을 가짐을 확인하였다.

로그분포모형을 이용한 토양입도분포로부터의 불포화수리전도도 추정

  • 황상일
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2003년도 추계학술발표회
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    • pp.99-101
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    • 2003
  • Unsaturated hydraulic conductivity models have been widely used for the numerical modeling of water flow and contaminant transport in soils. In this study, a simple hydraulic conductivity model is developed by using information of particle-size distribution from the lognormal distribution model and its results are compared with those from the Kosugi-Mualem (KM) model. The accuracy of the proposed model is verified for observed data chosen from the international UNSODA database. Results showed that the proposed model produces adequate predictions of hydraulic conductivities. Performance of this model is generally better than the KM function.

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Measurements of Cloud Raindrop Particles Using the Ground Optical Instruments and Small Doppler Radar at Daegwallyeong Mountain Site

  • Oh, Sung-Nam;Jung, Jae-Won
    • 대한원격탐사학회지
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    • 제29권3호
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    • pp.293-306
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    • 2013
  • Hydrometeor type and Drop Size Distribution (DSD) in cloud are the fundamental properties that may help explain the rain formation processes and determine the parameters of radar meteorology. This study presents a preliminary analysis of hydrometeor types and DSD data of cloud measured with a PARSIVEL (PARticle SIze and VELocity) optical disdrometer at the site of Cloud Physics Observation System (CPOS, $37^{\circ}41^{\prime}N$, $128^{\circ}45^{\prime}E$, 843 m from sea level) in Daegwallyeong mountainside of Korea. The method has been validated by comparing the observed rainfall rates with the computed ones from the fitted distribution, using the physical data such as DSD, terminal velocity, and rain intensity which were measured by a Micro-Rain Radar (MRR) and a PARSIVEL optical disdrometer. The analysis period started in three cases: on rainy days with light rain (15.5 mm), moderate rain (76 mm), and heavy rain (121 mm), from March to November 2007, respectively.