• Title/Summary/Keyword: Size Distribution

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A Probabilistic Analysis on Fracture Strength of Ceramics (세라믹스의 파괴강도에 관한 확률론적 해석)

  • 김선진
    • Journal of Ocean Engineering and Technology
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    • v.10 no.2
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    • pp.61-68
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    • 1996
  • Weibull distribution function is applied very successfully to the strength of brittle materials such as ceramics and the weakest link model is applied to explain the ovents. This paper deals with the effect of specimen size on the strength of ceramics. The values of tensile strength were calculated by the Monte-Calro simuation. The tensile strength obtained was plotted on Weibull probabillity papers and represented by the 3-parameter Weibull distribution. The strength distribution function was compared with the theoretical weibull distribution. As a result, it was found that the Weibull shape parameter was changed due to the size and there was a possibility of a false indication as if the weakest link model holds good. We should be very careful when we apply the Weibull statistics to estimate the strength of products.

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Estimation of Joint Size Distribution Using a Contained Trace Length Distribution in a Cylindrical Window (원통형 조사창에서의 양끝내포선 길이분포를 이용한 절리크기분포 추정 연구)

  • Suh, Ga Hyun;Song, Jae-Joon
    • Tunnel and Underground Space
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    • v.26 no.3
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    • pp.201-211
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    • 2016
  • A method for estimating rock joint size distribution using contained traces length distribution from 3D cylindrical window survey was suggested. To reduce the numerical error, an improved technique was applied. The accuracy was verified by referring to Monte-Carlo simulation and it was found that the error can be decreased with suitable gamma values.

Preparation and Characteristics of Polyethersulfone Microfiltration Membranes (폴리에테르술폰 정밀여과막의 제조 및 특성 연구)

  • Kim, No-Won
    • Membrane Journal
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    • v.17 no.4
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    • pp.329-337
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    • 2007
  • This is the research about a new method to make the internal separation layer with smallest pore size in polyethersulfone (PES) membrane by adding p-toluenesulfonic acid (TSA) and polyvinylpyrolidone (PVP) to polymeric PES solution. The preparation and morphological characterization of PES sheet membranes containing PVP as a hydrophilic swelling material and TSA as a demixing material were performed. As a result by microflow porometery, the PVP and TSA added PES membranes showed good permeabilities and narrow pore size distributions, comparable to those of the commercial membranes. The concentration of PVP affected the PES characteristics on air permeability and surface structure. The concentration of TSA influenced on pore size distribution but do not affect air permeability. The surface images of FE-SEM shows similar pore size when TSA added or not. However, the cross-section images of FE-SEM show that the TSA added PES membranes have a increase of internal layer thickness with smallest pore size.

Size Distribution of Ambient Aerosol Measured at a Coastal Site in Jeju Island (제주도 해안가에서 측정된 에어로졸의 성분별 입경분포 특성)

  • 이기호;양희준;허철구
    • Journal of Environmental Science International
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    • v.12 no.10
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    • pp.1043-1054
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    • 2003
  • During the period from April to September 2002, the size distributions of ambient aerosol were measured at the coastal site at Hamduk in Jeju Island. Na$\^$+/, K$\^$+/, Mg$\^$2+/, Ca$\^$2+/and Cl$\^$-/ exhibited mostly a bimodal coarse mode size distribution, while ammonium and sulfate were mainly in the fine size range, with maximum at around 0.54$\mu\textrm{m}$. The average molar concentration ratio of ammonium to sulfate for fine particles was equal to 2.0${\pm}$0.9. Nitrate was evenly found in both the coarse and fine modes. Elements like Al, Fe, Cu, Mg, Na, Ti, Sr and Mn were dominant in coarse particles, with the maximum at around 5.25$\mu\textrm{m}$. S and Pb were mainly in the submicrometer size range. Other elements with a fine and coarse modes were V, Ni, Cu, Ba and Mo. The patterns of the size distributions of trace elements measured at the downtown in Jeju City were very similar to those at the coastal site in Hamduk. However, the amplitude of size fractional concentrations at Jeju City was narrower than that at Hamduk. While the mass median diameters for the chemical species originated from the natural origin such as marine and crust were relatively large, those for ammonium, sulfate, S and Pb were very small.

Synthesis of scheelite-type nanocolloidal particles by pulsed laser ablation in liquid and their size distribution analysis

  • Lee, Jung-Il;Shim, Kwang Bo;Ryu, Jeong Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.24 no.3
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    • pp.111-119
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    • 2014
  • A novel pulsed laser ablation process in liquid was investigated to prepare scheelite-type ceramic [calcium tungstate ($CaWO_4$) and calcium molybdate ($CaMoO_4$)] nanocolloidal particles. The crystalline phase, particle morphology, particle size distribution, absorbance and optical band-gap were investigated. Stable colloidal suspensions consisting of well-dispersed $CaWO_4$ and $CaMoO_4$ nanoparticles with narrow size distribution could be obtained without any surfactant. Particle tracking analysis using optical microscope combined with image analysis was applied for a fast determination of particle size distribution in the prepared nanocolloidal suspensions. The mean nanoparticle size of $CaWO_4$ and $CaMoO_4$ colloidal nanoparticles were 16 nm and 30 nm, with the standard deviations of 2.1 and 5.2 nm, respectively. The optical absorption edges showed blue-shifted values about 60~70 nm than those of reported in bulk crystals. And also, the estimated optical energy band-gaps of $CaWO_4$ and $CaMoO_4$ colloidal particles were 5.2 and 4.7 eV. The observed band-gap widening and blue-shift of the optical absorbance could be ascribed to the quantum confinement effect due to the very small size of the $CaWO_4$ and $CaMoO_4$ nanocolloidal particles prepared by pulsed laser ablation in liquid.

Effects of the Size and Distribution of Preflocculated GCC on the Physical Properties of Paper

  • Lee, Kyong-Ho;Lee, Hak-Lae;Youn, Hye-Jung
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2006.06a
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    • pp.85-90
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    • 2006
  • Increasing the filler content of sheet improves the optical properties and printability of paper and provides an opportunity for saving production cost through fiber replacement with relatively low-priced filler. But increasing the filler content tends to decrease the strength of paper and filler retention. It also tends to deteriorate drainage on the paper machine. To overcome these problems, preflocculation technology of fillers may be employed. Many research efforts have been made on the properties of preflocculated filler, namely prefloc, whose size and size distribution were influenced by polymer type and shear level. But there is much to be investigated about the effect of the prefloc characteristics on the physical properties of paper. To evaluate the effect cationic polymers on the size and size distribution of preflocculated GCC and their shear stability, cationic PAM and cationic starch were used. The influence of the preflocculation on filler retention and its surface distribution, and the changes of physical and optical properties of handsheets affected by the characteristics of preflocs were examined. Filler distribution on sheet surface was also analyzed by EPMA. Results showed that cationic PAM formed large preflocs at low dosage. Cationic starch was required to add 15 times as much as cationic PAM to obtain the preflocs with similar size. But preflocs formed with cationic starch was superior in shear stability to those formed with cationic PAM. Filler preflocculation technology could provide an opportunity of increasing filler content significantly without loss in tensile strength. And increased filler contents could compensate brightness loss which often accompanies filler preflocculation. When excessively large preflocs were used, however, brightness loss rather than the improvement in tensile strength was predominant. Therefore it is of great importance to produce preflocs with proper size and shear stability for maximizing the improvement of physical properties of papers.

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[Retraction]Size measurement and characterization of ceria nanoparticles using asymmetrical flow field-flow fractionation (AsFlFFF)

  • Kim, Kihyun;Choi, Seong-Ho;Lee, Seungho;Kim, Woonjung
    • Analytical Science and Technology
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    • v.32 no.5
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    • pp.173-184
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    • 2019
  • As the size of semiconductors becomes smaller, it is necessary to perform high precision polishing of nanoscale. Ceria, which is generally used as an abrasive, is widely used because of its uniform quality, but its stability is not high because it has a high molecular weight and causes agglomeration and rapid precipitation. Such agglomeration and precipitation causes scratches in the polishing process. Therefore, it is important to accurately analyze the size distribution of ceria particles. In this study, a study was conducted to select dispersants useful for preventing coagulation and sedimentation of ceria. First, a dispersant was synthesized and a ceria slurry was prepared. The defoamer selection experiment was performed in order to remove the air bubbles which may occur in the production of ceria slurry. Dynamic light scattering (DLS) and asymmetrical flow field-flow fractionation (AsFlFFF) were used to determine the size distribution of ceria particles in the slurry. AsFlFFF is a technique for separating nanoparticles based on sequential elution of samples as in chromatography, and is a useful technique for determining the particle size distribution of nanoparticle samples. AsFlFFF was able to confirm the presence of a little quantities of large particles in the vicinity of 300 nm, which DLS can not detect, besides the main distribution in the range of 60-80 nm. AsFlFFF showed better accuracy and precision than DLS for particle size analysis of a little quantities of large particles such as ceria slurry treated in this study.

Smartphone Digital Image Processing Method for Sand Particle Size Analysis (모래 입도분석을 위한 스마트폰 디지털 이미지 처리 방법)

  • Ju-Yeong Hur;Se-Hyeon Cheon
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.35 no.6
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    • pp.164-172
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    • 2023
  • The grain size distribution of sand provides crucial information for understanding coastal erosion and sediment deposition. The commonly used sieve analysis for grain size distribution analysis has limitations such as time-consuming processes and the inability to obtain information about individual particle shapes and colors. In this study, we propose a grain size distribution analysis method using smartphone digital images, which is simpler and more efficient than the sieve analysis method. During the image analysis process, we effectively detect particles from relatively low-resolution smartphone digital images by extracting particle boundaries through image gradient calculation. Using samples collected from four beaches in Gyeongsangbuk-do, we compare and validate the proposed boundary extraction image analysis method with the analysis method that does not extract boundaries, against sieve analysis results. The proposed method shows an average error rate of 8.21% at D50, exhibiting a 65% lower error compared to the method without boundary extraction. Therefore, grain size distribution analysis using smartphone digital images is convenient, efficient, and demonstrated accuracy comparable to sieve analysis.

로그분포모형을 이용한 토양입도분포로부터의 불포화수리전도도 추정

  • 황상일
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2003.09a
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    • pp.99-101
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    • 2003
  • Unsaturated hydraulic conductivity models have been widely used for the numerical modeling of water flow and contaminant transport in soils. In this study, a simple hydraulic conductivity model is developed by using information of particle-size distribution from the lognormal distribution model and its results are compared with those from the Kosugi-Mualem (KM) model. The accuracy of the proposed model is verified for observed data chosen from the international UNSODA database. Results showed that the proposed model produces adequate predictions of hydraulic conductivities. Performance of this model is generally better than the KM function.

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Measurements of Cloud Raindrop Particles Using the Ground Optical Instruments and Small Doppler Radar at Daegwallyeong Mountain Site

  • Oh, Sung-Nam;Jung, Jae-Won
    • Korean Journal of Remote Sensing
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    • v.29 no.3
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    • pp.293-306
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    • 2013
  • Hydrometeor type and Drop Size Distribution (DSD) in cloud are the fundamental properties that may help explain the rain formation processes and determine the parameters of radar meteorology. This study presents a preliminary analysis of hydrometeor types and DSD data of cloud measured with a PARSIVEL (PARticle SIze and VELocity) optical disdrometer at the site of Cloud Physics Observation System (CPOS, $37^{\circ}41^{\prime}N$, $128^{\circ}45^{\prime}E$, 843 m from sea level) in Daegwallyeong mountainside of Korea. The method has been validated by comparing the observed rainfall rates with the computed ones from the fitted distribution, using the physical data such as DSD, terminal velocity, and rain intensity which were measured by a Micro-Rain Radar (MRR) and a PARSIVEL optical disdrometer. The analysis period started in three cases: on rainy days with light rain (15.5 mm), moderate rain (76 mm), and heavy rain (121 mm), from March to November 2007, respectively.