• Title/Summary/Keyword: Sintering resistance

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Physical, Mechanical Properties and Freezing and Thawing Resistance of Non-Cement Porous Vegetation Concrete Using Non-Sintering Inorganic Binder (비소성 무기결합재를 사용한 무시멘트 다공성 식생콘크리트의 물리·역학적 특성 및 동결융해저항성 평가)

  • Kim, Hwang Hee;Kim, Chun Soo;Jeon, Ji Hong;Park, Chan Gi
    • Journal of The Korean Society of Agricultural Engineers
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    • v.56 no.5
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    • pp.37-44
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    • 2014
  • The physical, mechanical and freezing and thawing properties of non cement porous vegetation concrete using non-sintering inorganic binder have been evaluated in this study. Four types of porous vegetation concrete according to the binder type is evaluated. The pH value, void ratio, compressive strength, repeated freezing and thawing properties were tested. The test results indicate that the physical, mechanical and repeated freezing and thawing properties of porous vegetation concrete using the non-sintering inorganic binder is increased or equivalent compared to the porous vegetation concrete using the blast furnace slag + cement and hwang-toh + cement binders. Also, Vegetation monitoring test results indicate the porous vegetation concrete using the non-sintering inorganic binder have increasing effects of vegetation growth.

Mechanical Properties and Sintering of Ultra Fine WC-Graphene-Al Composites (초미립 WC-Graphene-Al2O3 복합재료 소결 및 기계적 성질)

  • In-Jin Shon
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.4
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    • pp.206-214
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    • 2023
  • Tungsten carbide has many industrial applications due to its high electrical and thermal conductivity, high melting temperature, high hardness and good chemical stability. Because tungsten carbide is difficult to sinter, it is sintered with nickel or cobalt as a binder and is currently used in nozzles, cutting tools, and molds. Alumina is reported to be a viable binder for tungsten carbide due to its higher oxidation resistance and lower cost than nickel and cobalt. The ultrafine tungsten carbide-graphene-alumina composites were rapidly sintered in a high frequency induction heating active sintering unit. The microstructure and mechanical properties (fracture toughness and hardness) of the composites were investigated and analyzed by Vickers hardness tester and electron microscope. Since the high-frequency induction heating sintering method enables high-speed sintering, ultrafine composites can be prepared by preventing grain growth. In the tungsten carbide-graphene-alumina composites, the grain size of tungsten carbide increased with the amount of alumina participation. The hardness and fracture toughness of the tungsten carbide-5% graphene- x% alumina (x = 0, 5, 10,15) composites were 5.1, 8.6, 8.6, and 8.4 MPa-m1/2 and 2384, 2168, 2165, and 2102 kg/mm2, respectively. The fracture toughness increased without a significant decrease in hardness. Sinterability was improved by adding alumina to tungsten carbide-graphene.

Effect of lead-free frit and RuO2 on the electrical properties of thick film NTC thermistors for low temperature co-firing (저온 동시 소성용 후막 NTC 서미스터의 전기적 특성에 미치는 무연계 프릿트 및 RuO2의 영향)

  • Koo, Bon Keup
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.31 no.5
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    • pp.218-227
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    • 2021
  • A thick film NTC thermistor for low temperature co-firing was manufactured by printing and sintering a paste prepared using NTC powder of Mn1.5Ni0.4Co0.9Cu0.4O4 composition, lead free frit, and RuO2 on a 96 % alumina substrate. The effect of frit and RuO2 on the electrical properties of thick film NTC thermistor was studied. The resistance of the thick film NTC thermistor was higher than that of the bulk phase sintered at the same temperature, but it was found that the negative resistance temperature characteristic appeared more clearly and linearly in the resistance - temperature characteristic. On the other hand, the area resistance decreased as the sintering temperature increased, and the area resistance increased as the amount of frit added increased. The B constant of the thick film NTC thermistor was 3000 K or higher. Among them, it was found that the B constant of the thick film NTC thermistor made of paste with 5 wt% of frit added and sintered at 900℃ showed the highest B constant. Also, it can be seen that the area resistance decreased with the addition of RuO2, and the change in the area resistance decrease of the thick film NTC thermistor obtained by sintering the paste containing 5 wt% of RuO2 at 900℃ is the most obvious.

Processing and Properties of Engine Valve-shaped TiAl-Mn Intermetallics by Reactive Sintering (반응소결법에 의해 엔진밸브 형상으로 제조한 TiAl-Mn 금속간화합물의 특성)

  • 김영진
    • Journal of Powder Materials
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    • v.4 no.4
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    • pp.243-251
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    • 1997
  • Engine valve-shaped TiAl-Mn intermetallics containing 43.5 to 47.5at%Al (Mn/Al=0.036) are successively fabricated by reactive sintering the elemental powder mixtures near-net shaped by extrusion and die forging. A duplex structure consisted of lamellar grains and equiaxed $\gamma$ grains is developed for all compositions, and the areal fraction of the lamellar grains(or equiaxed $\gamma$ grains) decreases (or increases) with increasing Al content. As Al content increased, the elongation increases with accompanying decrease in yield strength and ultimate tensile strength at both room temperature and 80$0^{\circ}C$. This indicates that the suitable composition is Ti-45at%Al-1.6at%Mn in considering the balance of ambient and elevated tensile properties. The reactive-sintered Ti-45Al-1.6Mn alloy shows superior oxidation resistance not only to the plasma arc melted one but also to the heat resistance steel STR35(representative exhaust valve head material for automotive engine). The reactive-sintered Ti-45Al-1.6Mn alloy coated with an oxidizing scale exhibits a better wear resistance than induction hardened martensitic steel STR11(representative exhaust valve tip material for automotive engine).

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Evaluation of corrosion resistance of Co-Cr alloys fabricated with different metal laser sintering systems

  • Tuna, Suleyman Hakan;Karaca, Erhan;Aslan, Ismail;Pekkan, Gurel;Pekmez, Nuran Ozcicek
    • The Journal of Advanced Prosthodontics
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    • v.12 no.3
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    • pp.114-123
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    • 2020
  • PURPOSE. The aim of this study was to evaluate the corrosion resistance of the specimens produced by five different commercial metal laser sintering (MLS) systems with their recommended Co-Cr alloy powders. MATERIALS AND METHODS. The MLS machines and the alloy powders used were, ProX 100-ST2724G (St-Pro), Mysint 100-EOS SP2 (SP2-Mys), EOSINT 270-EOS SP2 (SP2-EOS), SLM 100-Starbond CoS (SB-SLM), and MLab Cusing-Remanium® Star (RS-MLab), respectively. Eight specimens from each group were prepared. Open circuit potential (Eocp) and electrochemical impedance spectroscopy (EIS) measurements of polished surfaces of the specimens were conducted in a three-electrode cell using a potentiostat-galvanostat in Fusayama-Meyer artificial saliva (AS). Specimens from each group were immersed in AS and de-ionized water for seven days. Eocp, charge transfer resistance (Rct) values, and released ions (㎍/㎠ × 7d) in different solutions were determined. The specimen surfaces were observed with SEM/EDS. Results were analyzed statistically. RESULTS. Eocp values have shifted to potentials that are more positive over time. Steady-state Eocp values were from high to low as follows, SB-SLM, SP2-Mys, SP2-EOS, RS-MLab, and ST-Pro, respectively. After 60 mins, RS-MLab specimens had the highest Rct value, followed by SP2-Mys, SB-SLM, SP2-EOS, and ST-Pro. In all groups, ion release was higher in AS than that in de-ionized water. CONCLUSION. There were small differences among the corrosion resistances of the Co-Cr alloy specimens produced with MLS systems; meanwhile, the corrosion resistances were quite high for all specimens.

A Study on the Properties of Traditional Korean Roof Tile by Using Nano Alumino Silicate (전통한식기와의 나노알루미노실리케이트 첨가에 따른 성능연구)

  • Kim, Soon-Ho
    • Journal of the Korea Institute of Building Construction
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    • v.20 no.5
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    • pp.425-432
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    • 2020
  • The appearance of Korean traditional roof tiles is beautiful and excellent in water resistance, fire resistance and durability, but a high sintering temperature of 1,200℃ or higher is required. Therefore, due to the economical and heavy weight problem, the current trend is to use different roof finishing materials than Korean traditional roof tiles. By adding nanoaluminosilicate to clay and kaolin, which are the materials of the clay roof tiles, the sintering temperature is sintered at a low temperature of 1,000℃ or less, and the optimal mixing and material process is designed to satisfy the characteristics required as a Korean traditional roof tile. The results of this study again demonstrate the superiority of Korean traditional tiles with roof finishing materials using nanoaluminate. The properties of Korean traditional roof tiles that satisfy the criteria of KS F 3510 by applying fire resistance of natural minerals and nanoparticle technology to flexural strength of 2800N, Bulk specific gravity of 2.0g/㎤ and absorption rate of less than 10.0%, through which and researched materials development.

Fabrication and Properties of Ti-HA Composites Produced by Pulsed Current Activated Sintering for Biomaterials (통전가압활성소결에 의한 생체재료용 Ti-HA복합재료 제조 및 특성)

  • Woo, Kee Do;Kang, Duck Soo;Kwon, Eui Pyo;Moon, Min Seok;Shon, In Jin;Liu, Zhiguang
    • Korean Journal of Metals and Materials
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    • v.47 no.8
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    • pp.508-515
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    • 2009
  • Ti-6Al-4V biomaterial is widely used as a bone alternative. However, Ti-6Al-4V ELI alloy suffers from numerous problems such as a high elastic modulus and high toxicity. Therefore, non-toxic biomaterials with low elastic moduli need to be developed. Ti-HA(hydroxyapatite) composites were fabricated in the present work by pulsed current activated sintering (PCAS) at $1000^{\circ}C$ under 60 MPa using mixed Ti and HA powders. The effects of HA content on the physical and mechanical properties of the sintered Ti-HA composites have been investigated. X-ray diffraction(XRD) analysis of the Ti-HA composites, including Ti-40 wt%HA in particular, revealed new phases, $Ti_{2}O$, CaO, $CaTiO_3$, and TixPy, formed by chemical reactions between Ti and HA during sintering. The hardness of the Ti-HA composites decreased with an increase in HA content. The corrosion resistance of these composites was observed to be an excellent candidate as a commercial Ti-6Al-4 V ELI alloy. A Ti-5 wt%HA composite fabricated by PCAS is recommended as a new biomaterial, because it offers good corrosion resistance, compressive strength, wear resistance, and biocompatibility, and a low Young's modulus.