• Title/Summary/Keyword: Single domain

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In Situ Observation of Domain Structure of $NaNbO_3$ Using Polarizing Microscope (편광 현미경을 이용한 Sodium Niobate 단결정의 분역 구조 관찰)

  • 정선태
    • Journal of the Korean Ceramic Society
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    • v.34 no.12
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    • pp.1235-1239
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    • 1997
  • Sodium niobate single crystals were grown by high temperature solution growth with Na2O/B2O3 flux. The phase transitions and domain structures of sodium niobate were observed using transmission polarizing microscope from room temperature to $650^{\circ}C$. There was imperfect extinction region within as-grown crystals and this area could be removed by heat treatment. The area existed within crystal till 3$65^{\circ}C$, in which temperature the space group of sodium niobate is changed from Pbma to Pmnm. The phase transition from Pbma to Pmnm happened abruptly with changing domain structure. At 48$0^{\circ}C$, 52$0^{\circ}C$ and 572$^{\circ}C$, the colors and walls of domains were changed. All domains disappeared and the space group of sodium niobate was changed from P4/mbm to Pm3m at 64$0^{\circ}C$. When sodium niobate changed from high temperature phase to low temperature phase, the memory effect of domain structure was not observed.

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The orientations of ferroelastic domain in single Crystal, $CsPbCl_3$ ($CsPbCl_3$ 결정의 강탄성 domain의 orientations)

  • 신은정;정희태;김형국;정세영
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.1
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    • pp.117-125
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    • 1997
  • Ferroelastic $CsPbCl_3$ crystals were grown by the Czochralski method and Bridgman method. From XRD, DTA and the dielectric measurements, we investigated the structure and confirmed the phase transition temperatures of it. Using the polarizing microscope, we observed the ferroelastic domains and the temperature dependence of the domains. For the orientation states, we obtained the consistent result with the theoretical investigation by the crystallographical consideration. For Aizu species m3mF2/m(p) 12 orientation states are represented crystallographically.

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An Effective Experimental Optimization Method for Wireless Power Transfer System Design Using Frequency Domain Measurement

  • Jeong, Sangyeong;Kim, Mina;Jung, Jee-Hoon;Kim, Jingook
    • Journal of electromagnetic engineering and science
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    • v.17 no.4
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    • pp.208-220
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    • 2017
  • This paper proposes an experimental optimization method for a wireless power transfer (WPT) system. The power transfer characteristics of a WPT system with arbitrary loads and various types of coupling and compensation networks can be extracted by frequency domain measurements. The various performance parameters of the WPT system, such as input real/imaginary/apparent power, power factor, efficiency, output power and voltage gain, can be accurately extracted in a frequency domain by a single passive measurement. Subsequently, the design parameters can be efficiently tuned by separating the overall design steps into two parts. The extracted performance parameters of the WPT system were validated with time-domain experiments.

Observation of Domain Structure and Polarization Switching in (001)-oriented Pb(Mg1/3Nb2/3)O3-x%PbTiO3 Single Crystals by Scanning Force Microscope (주사 힘 현미경에 의한 (001) Pb(Mg1/3Nb2/3)O3-x%PbTiO3 단결정의 도메인 구조 및 분극 스위칭 관찰)

  • Lee, Eun-Gu
    • Journal of the Korean Ceramic Society
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    • v.47 no.4
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    • pp.333-337
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    • 2010
  • Domain structure and polarization switching in (001)-oriented $Pb(Mg_{1/3}Nb_{2/3})O_3-x%PbTiO_3$ (PMN-x%PT) crystals for x=20 and 35at% have been investigated in-situ by scanning force microscope (SFM) in a piezoresponse mode under a step DC electrical voltage. In the initial annealed condition, polar nano domains (PND) and domain striations oriented along {110} were observed in x=20 and x=35, respectively. For x=20, domain switching occurs by heterogeneous nucleation, where nucleation is not confined in the vicinity of domain boundaries, but rather can occur throughout the crystal volume. However, for x=35, domain switching tends to be preferentially initiated near pre-existing twin boundaries. With increasing the applying voltage, the nuclei density increased and assembled into {110} striations, indicating a stress-accommodated domain growth process. At higher voltage, nucleation occurs heterogeneously throughout the crystal volume.

The Improved Antigen-binding Activity of Biosimilar Remicade ScFv Antibodies by Fusion of the Leucine Zipper Domain (Leucine zipper도메인의 융합에 의한 바이오시밀러 레미케이드 Single-chain Fv 항체의 항원 결합력 개선)

  • Kim, Jin-Kyoo;Kim, Tae Hwan
    • Journal of Life Science
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    • v.30 no.11
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    • pp.1012-1020
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    • 2020
  • Remicade is a therapeutic biosimilar natural antibody in which the mouse variable domain has been linked to the human constant domain. It is a chimeric monoclonal antibody specific to tumor necrosis factor-alpha (TNF-α) and has been developed for the treatment of rheumatoid arthritis. To investigate the biological activity of the Remicade antibody, we carried out a bioinformatics study using a protein data bank to characterize the TNF-α antigen binding mechanism of the Remicade natural antibody. Because the production of the Remicade antibody is often limited by genetic instability of the natural antibody-producing cell, we generated a Remicade single-chain variable domain fragment antibody (Remicade) in which a heavy chain variable domain (VH) is joined with a light chain variable domain (VL) by a polypeptide linker. Furthermore, Remicade was fused to a leucine zipper (RemicadeScZip) for higher production and higher antigen-binding activity than Remicade. The Remicade and Remicade ScZip were expressed in Escherichia coli and purified by a Ni+-NTA-agarose column. As expected, the purified proteins had migrated as 28.80 kDa and 33.96 kDa in sodium dodecyl sulfate-polyacrylamide electrophoresis. The TNF-α antigen binding activity of Remicade was not observed by ELISA and western blot. In contrast, RemicadeScZip showed antigen-binding activity. Additional bio-layer interferometry analysis confirmed the antigen-binding activity of RemicadeScZip, suggesting that the leucine zipper stabilized the folding of RemicadeScZip in a denatured condition and improved the TNF-α antigenbinding activity.

Numerical and Experimental Analyses of the Aerodynamic Characteristics of a Counter Rotating Axial Fan (엇회전식 축류홴의 공력 특성에 관한 전산 해석 및 실험)

  • Cho, Jin-Soo;Won, Yu-Phil;Lee, Moon-Cheol
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.3
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    • pp.325-337
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    • 2000
  • A study was done on the numerical and experimental analyses of the aerodynamic characteristics of a counter rotating axial fan. The numerical analysis uses the frequency domain panel method developed for the aerodynamic analysis of interacting rotating systems, which is based on the unsteady lifting surface panel method. Each stage of interaction involves the solution of an isolated rotor, the interaction being done through the Fourier transform of the induced velocity field. Numerical results showed good agreements with other experimental data for single and counter rotating propeller systems. And they were compared with the experimental results of the counter rotating axial fan studied in the present paper. The performance test was carried out based on the Korean Standard (KS B 6311). It was focused on the relative efficiency increase of a counter rotating system for a single rotating one, and effects of the axial distance between the front and rear rotors on overall fan performances were investigated. As a result, it was shown that the counter rotating axial fan has the efficiency 14% higher than the single rotating one at peak efficiency points.

A Study on Performance Enhancement of Selection Combined Hybrid Sequential Deconvolution and SC-FDE for Single Carrier System (선택적 결합 기법을 활용하여 순차적 역컨벌루션과 단일반송파 수신기를 하이브리드하게 사용한 단일반송파 시스템 성능 향상에 관한 연구)

  • Jung, Hyeok-Koo
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.37 no.5A
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    • pp.305-310
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    • 2012
  • This paper proposes a selection combined hybrid sequential deconvolution and single carrier modulation with a zero forcing frequency domain equalizer for single carrier transmission system in order to enhance performance. Selection combining method is an algorithm of antenna space diversities, the receiver can choose the best channel environment only with the increase of the number of antennas, but a baseband structure is the same as the traditional receiver architecture. Simulation results show that the proposed algorithm has a better performance rather than the traditional single carrier transmission with a frequency domain equalizer.

Dielectric Properties and Phase Transformation of Poled <001>-Oriented Pb(Mg1/3Nb2/3)O3-PbTiO3 Single Crystals (분극된 <001> 방위 Pb(Mg1/3Nb2/3)O3-PbTiO3 단결정의 유전 특성 및 상전이)

  • Lee, Eun-Gu;Lee, Jae-Gab
    • Korean Journal of Materials Research
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    • v.22 no.7
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    • pp.342-345
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    • 2012
  • The dielectric properties and phase transformation of poled <001>-oriented $Pb(Mg_{1/3}Nb_{2/3})O_3-x%PbTiO_3$(PMN-x%PT) single crystals with compositions of x = 20, 30, and 35 mole% are investigated for orientations both parallel and perpendicular to the [001] poling direction. An electric-field-induced monoclinic phase was observed for the initial poled PMN-30PT and PMN-35PT samples by means of high-resolution synchrotron x-ray diffraction. The monoclinic phase appears from $-25^{\circ}C$ to $100^{\circ}C$ and from $-25^{\circ}C$ to $80^{\circ}C$ for the PMN-30PT and PMN-35PT samples, respectively. The dielectric constant (${\varepsilon}$)-temperature (T) characteristics above the Curie temperature were found to be described by the equation$(1/{\varepsilon}-1/{\varepsilon}_m)^{1/n}=(T-T_m)/C$, where ${\varepsilon}_m$ is the maximum dielectric constant and $T_m$ is the temperature giving ${\varepsilon}_m$, and n and C are constants that change with the composition. The value of n was found to be 1.82 and 1.38 for 20PT and 35PT, respectively. The results of mesh scans and the temperature-dependence of the dielectric constant demonstrate that the initial monoclinic phase changes to a single domain tetragonal phase and a to paraelectric cubic phase. In the ferroelectric tetragonal phase with a single domain state, the dielectric constant measured perpendicular to the poling direction was dramatically higher than that measured in the parallel direction. A large dielectric constant implies easier polarization rotation away from the polar axis. This enhancement is believed to be related to dielectric softening close to the morphotropic phase boundary.