• 제목/요약/키워드: Silver powder

검색결과 174건 처리시간 0.027초

졸-겔법을 이용한 은 담지 하이드록시아파타이트의 제조 (Preparation of Silver-doped Hydroxyapatite Using Sol-gel Method)

  • 문병배;김호건
    • 한국분말재료학회지
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    • 제12권6호
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    • pp.428-432
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    • 2005
  • In the present study, silver-doped antibacterial hydroxyapatites were successfully prepared by the sol-gel method. For the starting solution, the molar ratio of $Ca(NO_3)_2{\cdot}4H_2O, P(OC_2H_5)_3,\;C_2H_5OH,\;and\;H_O$ was set to 0.075:0.045:20:0.135; $AgNO_3$ was added to a ratio of Ag to total cation concentration of $0.5-12 mol\%$. The prepared sol was dried at $100^{\circ}C$ for 48h and heat-treated at $1000^{\circ}C$ for 2h to obtain particles in the 200-500nm size range. The product from the synthesis of silver-doped hydroxyapatite was investigated through X-ray diffraction experiments and scanning electron microscopy. The product showed high antibacterial properties, with a disinfection ratio of Staphylococcus aureus (ATCC 6538) and Escherichia coli (ATCC 25922) over $99.9^{\circ}C$ as calculated from an antimicrobial effects evaluation by the shake flask method.

탄소나노튜브 캐소드의 전계방출 특성에 미치는 CNT 페이스트용 나노입자 은분말의 영향 (Effect of Nano-Sized Silver Powders in CNT Paste on Field Emission Characteristics of Carbon Nanotube Cathode)

  • 안영제;이지언;신헌철;조영래
    • 한국재료학회지
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    • 제18권1호
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    • pp.12-17
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    • 2008
  • Carbon nanotube (CNT) cathodes were fabricated using nano-sized silver (Ag) powders as a bonding material between the CNTs and cathode electrodes. The effects of the powder size on the sintering behavior, the current density and emission image for CNT cathodes were investigated. As the diameter of the Ag powders decreases to 10 nm, the sintering temperature of the CNT cathode was lowered primarily due to the higher specific surface area of the Ag powders. In this study, it was demonstrated that nano-sized Ag powders can be feasibly used as a bonding material for a screen-printed CNT cathode, yielding a high current density and a uniform emission image.

티오요소와 염산 혼합 용액에서 사이클론 전해에 의한 은(Ag) 회수 (Recovery of Silver Using Cyclone Type Electrolytic Cell from Thiourea-hydrochloric Acid Mixed Solutions)

  • 조연철;소홍일;이주은;안재우;류호진
    • 자원리싸이클링
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    • 제26권4호
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    • pp.62-70
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    • 2017
  • 티오요소와 염산 혼합 용액 중 은(Ag)을 금속으로 회수하기 위해 사이클론 전해법을 이용하였다. 유속, 전류밀도, 은 농도, 티오요소 농도, 염산 농도를 주요 변수로 하여 은의 전해회수 거동을 살펴보았다. 유속, 전류밀도와 염산 농도가 증가할수록 은의 회수속도가 증가하였으며, 은 농도가 증가함에 따라 은의 회수 속도는 감소하였고, 티오요소 농도는 은 회수율과 전류효율에는 큰 영향이 없었다. 유속 12 L/min., 전류밀도 $0.75A/dm^2$, 1 g/L Ag, 0.5 M Thiourea, 0.1 M HCl에서 실험하였을 경우 99% 이상의 은 회수율을 보였다. 대부분의 실험 조건에서 은(Ag)은 분말 형태로 회수되었다.

절연체 종류에 따른 후막 전계 발광소자의 광학 및 전기적 특성 (Electrical and Optical Property of Powder Electroluminescent device at Dielectric variety)

  • 오주열;이종찬;박대희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1999년도 하계학술대회 논문집 D
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    • pp.1800-1802
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    • 1999
  • Electroluminescence is occurred when phosphor is located in electric field. In this paper, we made powder electroluminescent device (PELD) with structured ITO film/phosphor/Insulator/silver paste. The transparent electrode was ITO film and green(2704-01) and orange(2702-02) and blue-green(2703-01) were used as phosphor. The insulator was $BaTiO_3$ and $Y_2O_3$, back electrode was silver paste. To investigate electrical and optical properties of PELDs, EL spectrum, Brightness, Transferred charge density using Sawyer-Towers circuit was measured.

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Surface Morphology, Microstructure and Mechanical Properties of Thin Ag Films

  • Shugurov, Artur;Panin, Alexey;Chun, Hui-Gon;Oskomov, Konstantin
    • 한국분말재료학회지
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    • 제10권3호
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    • pp.190-194
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    • 2003
  • Thin Ag films deposited onto $SiO_2/Si$ substrates by DC magnetron sputtering and thereafter annealed ,it temperatures 100-50$0^{\circ}C$ are investigated by scanning tunneling and atomic forte microscopy. It is shown that the film surface topography and microstructure are considerably changed as a result of annealing. To provide a quantitative estimation of the surface topography changes of Ag films the surface fractal dimension was calculated. Elasticity and hardness of the films are studied by a nanoindentation technique. The films are found to have value of elastic modulus close to that of bulk silver while their hardness and yield stress are essentially higher.

후막 EL 소자의 광학 및 이동전하밀도 특성 (Transferred charge density and Optical Property on Powder Electroluminescent device)

  • 오주열;이종찬;박대희
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 춘계학술대회 논문집
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    • pp.286-290
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    • 1999
  • Electroluminescence is occurred when phosphor is located in electric field. In this paper, we made powder electroluminescent device (PELD) with structured ITO film/Phosphor/Insulator/Silver paste. The transparent electrode was ITO film and green(2704-01), orange(2702-02) and blue-green(2703-01) were used as phosphor. The insulator was BaTiO$_3$ and $Y_2$O$_3$, back electrode was silver paste. To investigate electrical and optical properties of PELDs, EL spectrum, Brightness, Transferred charge density using Sawyer-Tower\`s circuit was measured.

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유전체 종류에 따른 후막 전계발광(EL) 소자의 특성 (Properties of Powder Electroluminescent Device with $Y_2O_3 and BaTiO_3$)

  • 이종찬;박춘배;박대희
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 추계학술대회 논문집
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    • pp.582-585
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    • 1999
  • Electroluminescence is occurred when phosphor is located in electric field. In this paper, we made powder electroluminescent device (PELD) with structured ITO film/Phosphor/Insulator/Silver paste. The transparent electrode was ITO film and green(2704-01) and orange(2702-02) and blue-preen(2703-01) were used as phosphor. The insulator was BaTiO$_3$ and $Y_2$O$_3$, bark electrode was silver paste. To investigate electrical and optical properties of PELDs, EL spectrum, Brightness . Transferred charge density using Sawyer-Towers circuit was measured.

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Gel filtration에 의한 한방사선 인삼단백 분획의 정제 (Further Purification of Radioprotective Ginseng Protein Fraction by Gel Filtration)

  • 김춘미;박경애
    • Journal of Ginseng Research
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    • 제13권2호
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    • pp.254-259
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    • 1989
  • A radioprotective ginseng protein fraction was obtained from Korean white ginseng powder by the following isolation and purification procedures: Tris-HCI buffer extraction, 70% ammonium sulfate fractionation, CM-rellulosr column chromatography, heat inactivation and Sephadex G-75 column chromatography. This fraction was further purified by Sepharose 4B and Sephadex G-150 column chromatographies. Three fractions obtained were subjected to Native-PAGE and SDS-PAGE using gradient gels and the silver staining method. Molecular weights of the native proteins and their subunits were estimated.

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Solid Contents 에 따른 Ag Paste 의 특성 변화 (Characterization of Ag Pastes with solid contents variation)

  • 조현민;유명재;이우성;양형국;박종철
    • 한국마이크로전자및패키징학회:학술대회논문집
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    • 한국마이크로전자및패키징학회 2002년도 추계기술심포지움논문집
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    • pp.169-172
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    • 2002
  • Silver pastes for inner conductor in the Low Temperature Co-fired Ceramics (LTCC) are composed of silver powder, binder, solvent and additives. The composition of the chemicals have influence on rheology, printability, shrinkage rate, etc. In this study, commercial Ag pastes and Ag pastes made in KETI were investigated to find the relationship between characteristics of Ag paste and solid contents. Ag pastes with 68~90 wt% Solid Contents were tested. Substrate/paste matching property and conductivity of the conductor lines showed large dependence on solid contents of Ag paste.

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초음파화학 반응에 의한 Ag 도핑 광촉매용 나노 TiO2 분말의 합성 (Synthesis of Nano-Scale Photocatalyic TiO2 Powder Doped with Ag by Sonochemistry Reaction)

  • 조성훈;이수완
    • 한국재료학회지
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    • 제19권3호
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    • pp.169-173
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    • 2009
  • In chemistry, the study of sonochemistry is concerned with understanding the effect of sonic waves and wave properties on chemical systems. In the area of chemical kinetics, it has been observed that ultrasound can greatly enhance chemical reactivity in a number of systems by as much as a million-fold. Nano-technology is a super microscopic technology in which structures of 100 nanometers or smaller can be investigated. This technology has been used to develop $TiO_2$ materials and $TiO_2$ devices of that size. Thus far, electrochemistry methods and photochemistry methods have generally been used to create $TiO_2$ nano-size particles. However, these methods are complicated and create pollutants as a by-product. In the present study, nano-scale silver particles (5 nm) were prepared in a sonochemistry method. Sonochemistry deals with mechanical energy that is provided by the collapse of cavitation bubbles that form in solutions during exposure to ultrasound. $TiO_2$ powders 25 nm in size doped with Ag were formed using an ultrasonic sound technique. The experimental results showed the high possibility of removing pollution through the action of a photocatalyst. This powder synthesis technique can be considered as an environmentally friendly powder-forming processing owing to its energy saving characteristics.