• Title/Summary/Keyword: Silicone resin

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Effect of rinsing time on the accuracy of interim crowns fabricated by digital light processing: An in vitro study

  • Lee, Beom-Il;You, Seung-Gyu;You, Seung-Min;Kang, Seen-Young;Kim, Ji-Hwan
    • The Journal of Advanced Prosthodontics
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    • v.13 no.1
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    • pp.24-35
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    • 2021
  • PURPOSE. This study was to evaluate the effect of rinsing time on the accuracy of interim crowns fabricated by digital light processing. MATERIALS AND METHODS. The maxillary right first molar master die was duplicated using a silicone material, while a study die was produced using epoxy resin. Scans of the epoxy resin die were used in combination with CAD software to design a maxillary right first molar interim crown. Based on this design, 24 interim crowns were fabricated with digital light processing. This study examined the trueness and precision of products that were processed with one of the three different postprocessing rinsing times (1 min, 5 min, and 10 min). Trueness was measured by superimposing reference data with scanned data from external, intaglio, and marginal surfaces. Precision was measured by superimposing the scan data within the group. The trueness and precision data were analyzed using Kruskal-Wallis, nonparametric, and post-hoc tests, and were compared using a Mann-Whitney U test with Bonferroni correction (α=.05). RESULTS. The trueness of the external and intaglio surfaces of crowns varied significantly among the different rinsing times (P=.004, P=.003), but there was no statistically significant difference in terms of trueness measurements of the marginal surfaces (P=.605). In terms of precision, statistically significant differences were found among the external, intaglio, and marginal surfaces (P=.001). CONCLUSION. Interim crowns rinsed for 10 minutes showed high accuracy.

Comparative accuracy of new implant impression technique using abutments as impression copings with an angulated implant model (경사지게 식립된 임플랜트 모형에서 지대주를 인상용 코핑으로 이용한 새로운 인상법의 정확성 비교 연구)

  • Lee, Hyeok-Jae;Kim, Chang-Whe;Lim, Young-Jun;Kim, Myung-Joo
    • The Journal of Korean Academy of Prosthodontics
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    • v.46 no.2
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    • pp.201-208
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    • 2008
  • Statement of problem: A new implant impression technique which use abutments as impression coping, and use resin cement as a splinting material was described. Accuracy of this technique was compared with conventional closed tray and resin splinted open tray technique for a $15^{\circ}$ angled 3-implant model Material and methods: A dental stone master model with 3 linearly positioned implant analogue and a reference framework which was passively fitted to it were fabricated. The center analogue was perpendicular to the plane of model and the outer analogues had a $15^{\circ}$angulation forward or backward. 10 closed tray impressions, 10 resin splinted open tray impressions, 10 abutment-resin framework cementation impressions and 10 abutment-metal framework cementation impressions were made with additional silicone material and poured with dental stone. A light microscope with image processing was used to record the vertical gap dimension between reference framework and analogue of duplicated cast made with each 4 impression techniques. Statistical analysis used one-way ANOVA with post-hoc tests Tukey test of .05 level of significance Results: Significant difference in the vertical gap dimension was found between closed tray technique; 74.3 (${\pm}33.4$)${\mu}m$ and resin splinted open tray technique, and two other new technique. (P<.05) Abutment-metal framework cementation technique;42.5 (${\pm}11.9$)${\mu}m$ was significantly different from resin splinted open tray technique. (P<.05) Abutmentresin framework cementation technique;51.0 (${\pm}14.1$)${\mu}m$ did not differ significantly from resin splinted open tray technique;50.3 (${\pm}16.9$)${\mu}m$. (P>.05) Conclusion: Within limitations of this study, the accuracy of implant level impressions of resin splinted open tray technique was superior to that of closed tray technique. A new technique using abutment and metal framework cementation was more accurate than resin splinted open tray technique.

Comparison of shear bond strength between various temporary prostheses resin blocks fabricated by subtractive and additive manufacturing methods bonded to self-curing reline resin (절삭 및 적층 가공법으로 제작한 임시 보철물 레진 블록과 재이 장용 자가중합 레진의 전단결합강도 비교)

  • Hyo-Min Ryu;Jin-Han Lee
    • The Journal of Korean Academy of Prosthodontics
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    • v.61 no.3
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    • pp.189-197
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    • 2023
  • Purpose. This study aimed to compare and evaluate the shear bond strength between various temporary prostheses resin blocks fabricated by subtractive and additive manufacturing methods bonded to self-curing reline resin. Materials and methods. The experimental groups were divided into 4 groups according to the manufacturing methods of the resin block specimens and each specimen was fabricated by subtractive manufacturing (SM), additive manufacturing stereolithography apparatus manufacturing (AMS), additive manufacturing digital light processing manufacturing (AMD) and conventional self-curing (CON). To bond the resin block specimens and self-curing resin, the reline resin was injected and polymerized into the same location of each resin block using a silicone mold. The shear bond strength was measured using a universal testing machine, and the surface of the adhesive interface was examined by scanning electron microscopy. To compare between groups, one-way ANOVA was done followed by Tukey post hoc test (α = 0.05). Results. The shear bond strength showed higher values in the order of CON, SM, AMS, and AMD group. There were significant differences between CON and AMS groups, as well as between CON and AMD groups. but there were no significant differences between CON and SM groups (P > .05). There were significant differences between SM and AMD groups, but there were no significant differences between SM and AMS groups. The AMS group was significantly different from the AMD group (P < .001). The most frequent failure mode was mixed failures in CON and AMS groups, and adhesive failures in SM and AMD groups. Conclusion. The shear bond strength of SM group showed lower but not significant bond strength compared to the CON group. The additive manufacturing method groups (AMS and AMD) showed significantly lower bond strength than the CON group, with the AMD group the lowest. There was also a significant difference between the AMD and SM group.

Effects of primers on the microtensile bond strength of resin cements to cobalt-chromium alloy (레진 시멘트와 코발트 크롬 합금의 미세인장결합강도에 다양한 프라이머들이 미치는 영향)

  • Jung, Hong-Taek;Campana, Shiela A.;Park, Jin-Hong;Shin, Joo-Hee;Lee, Jeong-Yol
    • The Journal of Korean Academy of Prosthodontics
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    • v.57 no.2
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    • pp.95-101
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    • 2019
  • Purpose: The aim of this study is to evaluate the effects of various primers on the microtensile bond strength (${\mu}TBS$) of resin cements to cobalt-chromium (Co-Cr) dental casting alloy. Materials and methods: Four adhesive primers (Universal primer, Metal primer II, Alloy primer, and Metal/Zirconia primer) and two resin cements (Panavia F2.0, G-CEM LinkAce) were tested. One hundred fifty Co-Cr beams were prepared from Co-Cr ingots via casting ($6mm\;ength{\times}1mm\;width{\times}1mm\;thick$). The metal beams were randomly divided into ten groups according to the adhesive primers and resin cements used; the no-primer groups served as the control (n = 15). After sandblasting with aluminum oxide ($125{\mu}m$ grain), the metal and resin cements were bonded together using a silicone mold. Prior to testing, all metal-resin beams were examined under stereomicroscope, and subjected to the ${\mu}TBS$ test. The mean value of each group was analyzed via one-way ANOVA with Tukey's test as post hoc (${\alpha}=.05$) using SPSS software. Results: The mean ${\mu}TBS$ of all groups was ranged from 20 to 28 MPa. There is no statistically significant difference between groups (P > .05). Mixed failure, which is the combination of adhesive and cohesive failures, is the most prevalent failure mode in both the Panavia F2.0 and G-Cem LinkAce groups. Conclusion: The ${\mu}TBS$ of all tested groups are relatively high; however, the primers used in this study result in no favorable effect in the ${\mu}TBS$ of Panavia F2.0 and G-Cem LinkAce resin cement to Co-Cr alloy.

Ultrasonic Spray Nozzle System with Piezoelectric Device for Chemicals Dispersion (압전체를 이용한 약품 분사용 초음파 분사 노즐 시스템)

  • 고재석;김용현;김형수;조순행;최승철
    • Journal of the Microelectronics and Packaging Society
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    • v.10 no.4
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    • pp.65-71
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    • 2003
  • A new type of ultrasonic spray nozzle was fabricated employing a piezoelectric device. The spray nozzle was designed to disperse chemicals in a water treatment mixing tank. The piezoelectric properties in ultrasonic spray nozzles were optimized to improve the dispersion of chemicals. The piezoelectrics were packaged in an aluminum case with silicone resin for the aqueous solution proof packaging. Chemicals were dispersed with high efficiency and the chemicals consumption was reduced by the ultrasonic fine particle spraying. The concentration of Escherichia coli in mixing tank was decreased remarkably using ultrasonic spray nozzle dispersion compared to the conventional methods.

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The Characteristics of Dielectric Breakdown for Epoxy Resin irradiated Electron Beam (전자선 조사된 에폭시 수지의 절연파괴 특성)

  • Hong, Nung-Pyo;Cho, Dong-Chan;Park, Heung-Kyu;So, Byung-Mun;Kim, Wang-Kon;Hong, Jin-Woong
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.430-432
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    • 1995
  • In this paper, the electron beam with 1[Mrad], 2[Mrad], 4[Mrad], 8[Mrad] and 24[Mrad] is irradiated for specimen experiments on physical properties which is investigated by FTIR, and dielectric breakdown among the electrical characteristics of specimen are carried out. For the dielectric breakdown experiment, external 60 [Hz] AC voltage is applied to specimen with the rising voltage of 3[kV/cm] until dielectric breakdown occured. We made a breakdown experiment under the temperature condition of 50[$^{\circ}C$], 100[$^{\circ}C$], 150[$^{\circ}C$] in the silicone oils of dynamic viscosity of 100[cSt].

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Development of Multi-functional Mulch Papers and Evaluation of Their Performance(Part 3) -Defoaming Treatment during Trial Production of Mulch Papers and Their Influence on Wet End System- (다기능성 멀칭지의 개발 및 적용성 평가(제3보) -시제품 생상시 공정 백수의 거품제거 처리 및 그 영향에 관하여-)

  • 이학래;이진희
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.3
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    • pp.25-31
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    • 2000
  • It is required to use substantial amount of wet strength resin for producing multi-functional mulch papers since these paper products shold maintain its strength properties when they exposed to outdoor weather for several months. While producing mulch papers it is usual to observe significant amount of foam at white water silo. Thus it is imperative to use defoaming or antifoaming agents. In this study diverse defoaming and antifoaming agents have been tested for their effective-ness in eliminating foams that produced. It was shown that combined use of a silicone type defoamer and a fatty acid type anti-foaming agent was msot effective in eliminating foams. These chemicals were used in trial production of mulch papers and their influence on paper-making wet end system was examined including one pass retention cationic demand con-ductivity pH etc. It was found that the defoaming agents were very effective for removing foams in trial production. Tensile strengths of the mulch papers produced were significantly greater than commericial mulch papers produced in Japan.

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Clinical gap changes after porcelain firing cycles of zirconia fixed dentures

  • Bugurman, Bugurman Burcu;Turker, Sebnem Begum
    • The Journal of Advanced Prosthodontics
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    • v.6 no.3
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    • pp.177-184
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    • 2014
  • PURPOSE. The aim of this study was to measure the changes on the marginal and internal adaptation of zirconia based anterior fixed partial dentures after the porcelain firing process. MATERIALS AND METHODS. A total of 34 anterior fixed partial dentures using LAVA CAD/CAM system (3M ESPE, Germany) were applied. Two silicone replicas were obtained: one is obtained before porcelain firing process (initial) and the other is obtained after porcelain firing process (final), followed by the examination under a binocular stereomicroscope. Kruskal Wallis and Wilcoxon Signed Ranks tests were used for the statistical analysis (P<.05). RESULTS. No statistically significant difference was found between initial and final marginal gap values (P>.05). At the internal gap measurements, final marginal area values ($59.54{\mu}m$) were significantly lower than the initial marginal area values ($68.68{\mu}m$)(P<.05). The highest and the lowest internal gap values were observed at the incisal/occlusal area and at the marginal area, respectively. In addition, lower internal gap values were obtained for canines than for central incisors, lateral incisors and premolars at the incisal area (P<.05). CONCLUSION. The firing cycles did not affect the marginal gap of Lava CAD/CAM system, but it is controversial for the internal gap.

FRACTURE STRENGTH OF ZIRCONIA MONOLITHIC CROWNS (지르코니아 단일구조 전부도재관의 파절강도)

  • Jeong Hee-Chan
    • The Journal of Korean Academy of Prosthodontics
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    • v.44 no.2
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    • pp.157-164
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    • 2006
  • Purpose: The purpose of this study was to compare the fracture strength of the zirconia monolithic all-ceramic crowns according to the thickness(0.5 mm, 0.8 mm, 1.1 mm) and IPS Empress II ceramic crown of 1.5 mm thickness. Material and method: Eight crowns for each of 3 zirconia crown groups were fabricated using CAD/CAM system(Kavo, Germany) and eight Empress II crowns were made from silicone mold and wax pattern. Each crown group was finished in accordance with the specific manufacturer s instruction. All crowns were luted to the metal dies using resin cement and mounted on the testing jig in a universal testing machine. The load was directed at the center of crown with perpendicular to the long axis of each specimen until catastrophic failure occurred. Analysis of variance and Tukey multiple comparison test(p<.05) were applied to the data. Results and Conclusion: 1. The fracture strength of the zirconia monolithic all-ceramic crown was higher thickness increased(p<.05). 2 The fracture strength of 1.1 mm thickness zirconia monolithic all-ceramic crown was higher than the fracture strength of 1.5 mm thickness IPS Empress II crown(p<.05). 3. The fracture strength of 0.5 mm thickness zirconia monolithic all-ceramic crown exceeded maximum occlusal forces.

Detergency of Particulate Soil of PET Fabric Finished with Hydrophilic and Hydrophobic Chemicals (친수 및 소수처리 PET직물의 고형오구의 세척성)

  • Kang, In-Sook
    • Journal of the Korean Society of Clothing and Textiles
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    • v.36 no.11
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    • pp.1237-1245
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    • 2012
  • The effect of hydrophilicity and hydrophobicity of PET fabric on the detergency of particulate soil were investigated as functions of the concentration of hydrophilic and hydrophobic chemicals, surfactant concentration, ionic strength, adhesion and removal time, and pH. The detergency of the particulate soil was determined by the adhesion of particles to and their removal from fabric, the PET fabric and ${\alpha}-Fe_2O_3$ were used as textile materials and for the model of particulate soil, respectively. The hydrophilic and hydrophobic finish for PET fabric was treated with a polyester, silicone and fluorine organic compound of resin respectively. The adhesion of particulate soil to fabric treated with hydrophobic chemicals were slightly higher but its removal from fabric treated with hydrophobic chemicals was largely higher than fabric treated with a hydrophilic chemical regardless of solution conditions such as the concentration of hydrophilic and hydrophobic chemicals, surfactant concentration, ionic strength, adhesion and removal time, and pH. Therefore, hydrophobic treatment for fabric had a more positive effect than the hydrophilic treatment on the detergency of particulate soil.