• 제목/요약/키워드: Silica particle

검색결과 501건 처리시간 0.043초

Effects of SiC Particle Size and Inorganic Binder on Heat Insulation of Fumed Silica-based Heat Insulation Plates

  • Jo, Hye Youn;Oh, Su Jung;Kim, Mi Na;Lim, Hyung Mi;Lee, Seung-Ho
    • 한국세라믹학회지
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    • 제53권4호
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    • pp.386-392
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    • 2016
  • Heat insulation plates of fumed silica were prepared by mixing fumed silica, SiC powder and chopped glass fiber by a high speed mixer followed by pressing of the mixture powder in a stainless steel mold of $100{\times}100mm$. Composition of the plates, particle size of SiC, and type of inorganic binder were varied for observation of their contribution to heat insulation of the plate. The plate was installed on the upper portion of an electric furnace the inside temperature of which was maintained at $400^{\circ}C$ and $600^{\circ}C$, for investigation of heat transfer through the plate from inside of the electric furnace to outside atmosphere. Surface temperatures were measured in real time using a thermographic camera. The particle size of SiC was varied in the range of $1.3{\sim}17.5{\mu}m$ and the insulation was found to be most excellent when SiC of $2.2{\mu}m$ was incorporated. When the size of SiC was smaller or larger than $2.2{\mu}m$, the heat insulation effect was decreased. Inorganic binders of alkali silicate and phosphate were tested and the phosphate was found to maintain the heat insulation property while increasing mechanical properties.

슬러리 공급 시스템을 이용한 화학적 기계적 연마 공정에서의 POU 필터의 성능 평가 (Evaluation of Point-Of-Use (POU) Filters Performance in Chemical Mechanical Polishing Slurry Supply System)

  • 장선재;김호중;진홍이;남미연;아툴 쿨르카르니;김태성
    • 한국입자에어로졸학회지
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    • 제9권4호
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    • pp.261-269
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    • 2013
  • The chemical mechanical polishing (CMP) process is widely used in semiconductor manufacturing process for planarization of various materials and structures. Point-of-use (POU) filters are used in most of the CMP processes in order to reduce the unwanted micro-scratches which may result in defects. The performance of the POU filter is depends on type and size of the abrasives used during cleaning process. For this reason, there is a need to evaluate POU filters for their filtration efficiency (FE) with different types of abrasives. In this study, we developed filter test system to evaluate the FE of POU using ceria and silica abrasives (slurry). The POU filter is roll type capsule filter with retention size of 0.2 ${\mu}m$. Two POU filters of different make are evaluated for FE. We observed that both POU filters show similar filtration efficiency for silica and ceria slurry. Results reveal that the ceria slurry and the colloidal silica particle are removed not only by mechanical way but also hydrodynamic and electrostatic interaction way.

흡착식 냉동기의 열 및 물질전달에 관한 실험적 연구 (An Experimental Study on the Heat and Mass Transfer of Adsorption Chiller)

  • 권오경;윤재호;주영주;김용찬;김종하
    • 설비공학논문집
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    • 제17권8호
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    • pp.746-753
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    • 2005
  • Adsorption chillers have been receiving considerable attentions as they are energy-saving and environmentally benign systems. In order to evaluate adsorption rates, experiments were performed in the batch type adsorption apparatus. Three types of silica gels were investigated under an assortment of experimental conditions that are representatives of the actual operating environments in the adsorber of adsorption chillers. Experimental results revealed the effects of silica gel particle size, bed temperature, and fin pitch of fin tube on the adsorption rate. The $0.25\~1.18mm$ particle size of silica gel with high adsorption rate was selected as a suitable adsorbent. The measured adsorption rate became bigger with decreasing particle size. From the comparison of adsorption rate, it is found that the fin tube has about $21\%$ higher value than that of the bare tube. The effect of heat and mass flux is found to be more significant in the fin tube than in the bare tube.

실리카 분말을 이용한 나노 충격완화 장치의 설계에서 작동 유체 영향과 복원 시간에 대한 연구 (Effect of Water Volume and Relaxation Time in the Design of Nano Shock Absorbing Damper Using Silica Particle)

  • 문병영;김병수
    • 한국세라믹학회지
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    • 제40권3호
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    • pp.286-292
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    • 2003
  • 본 연구에서는 나노기술을 이용하여 에너지 감쇄 기능을 활용한 감쇄기 개발에 대한 기초적인 연구를 하였다. 기계 구조물에 사용되는 기존의 유체 감쇄기를 대체할 수 있는 무기재료를 이용한 새로운 감쇄기에 대한 기초연구를 수행하여 감쇄기 설계와 실용화에 적용하고자 하였다. 완충역할을 하는 입자로는 미로구조를 가지는 실리카겔을 사용하였고, 입자에 관련한 작동 유체로는 물을 사용하여 실험적으로 그 효과를 검증하였다. 콜로이드 감쇄기를 구현하기 위해서는 형성된 실리카겔 입자의 표면을 유기 실리콘 매질을 이용한 소수화 코팅 처리를 하였다. 콜로이드 감쇄기의 에너지 감쇄량과 효율을 작동 유체에 대하여 각각 구하여 유효한 감쇄 효과를 입증하여 설계에 반영할 수 있게 되었다. 또한 압축해제에 걸리는 시간을 조사하여 기존의 유압 감쇄기와 비교한 결과 본 논문에서 제안된 감쇄기의 기능이 우수함이 입증되었다.

PTMSP-Silica-PEI 복합막에 의한 수소-질소 혼합기체 분리 (Separation of Hydrogen-Nitrogen Gas Mixture by PTMSP-Silica-PEI Composite Membranes)

  • 이현경;최윤정
    • 멤브레인
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    • 제14권4호
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    • pp.304-311
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    • 2004
  • PTMSP-PEI 복합막과 PTMSP-Silica-PEI 복합막을 제조하고, 막의 특성을 FT-IR, GPC, SEM 등을 사용하여 조사하였다. PTMSP-Silica-PEI 복합막은 silica의 함량이 23∼60 wt%로 증가하면서 입자의 크기는 점차 작아지고 입자의 분포는 균일하게 되었다. PTMSP-PEI 복합막과 PTMSP-Silica-PEI 복합막에 의한 $H_2$/$N_2$ 혼합기체분리는 $25^{\circ}C$, $\Delta$P 5 psi∼30 psi 범위에서 조사되었다. PTMSP-PEI 복합막과 PTMSP-Silica-PEI 복합막들의 수소에 대한 분리인자($\alpha$, $\beta$, (equation omitted)) 값은 투과셀의 압력이 증가할수록 그리고 silica의 함량이 증가할수록 증가하였다. $25^{\circ}C$, $\Delta$P 30 psi에서 PTMSP-PEI 복합막의 수소에 대한 $\alpha$, $\beta$, (equation omitted) 값은 2.28, 1.58, 1.44이고 silica 60 wt%인 PTMSP-Silica-PEI 복합막의 수소에 대한 $\alpha$, $\beta$, (equation omitted) 값은 3.34, 1.95, 1.72 이었다.

FHD 공정에 의한 저손실 실리카 슬랩 도파로 형성 (Fabrication of Low Loss Silica Slab Waveguide by Flame Hydrolysis Deposition)

  • 심재기;김태홍;신장욱;박상호;김덕준;성희경
    • 한국세라믹학회지
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    • 제37권6호
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    • pp.524-529
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    • 2000
  • Silica slab wavegudie was fabricated on Si substrates by FHD for planar optical passive devices. The slab waveguide consists of lower clad and core layers, where core layer index is controlled by GeO2 addition. Doping of GeO2 in silica is difficult because of the low deposition density due to nonspherical particle generation in FHD process. Silica core particles deposited at various conditions such as flame temperature and substrate scanning were analyzed by SEM and TEM. As the flame temperature increased, the surface roughness of the core layer was decreased up to 3.6 nm after consolidation. Index difference and thickness of core of slab waveguide were 0.3%, 8$\mu\textrm{m}$ respectively. Measured optical loss at TE mode was <0.04 dB/cm at 1.3$\mu\textrm{m}$ and <0.06 dB/cm at 1.55$\mu\textrm{m}$.

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실리카가 첨가된 연소합성 TiO2 나노입자의 열처리에 따른 상변환 특성 (Effect of Silica Addition on Phase Transformation Characteristics of Heat-Treated Combustion-Synthesized TiO2 Nanoparticles)

  • 김민수;이교우
    • 대한기계학회논문집B
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    • 제33권3호
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    • pp.186-193
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    • 2009
  • In this article, the effect of silica addition on the phase transformation characteristics of $TiO_2$ nanoparticles synthesized by using an $O_2$-enriched coflow, hydrogen, diffusion flame was investigated. TTIP(titanium tetra-isopropoxide) and TEOS(tetraethyl-orthosilicate) were used as precursors for $TiO_2$ and $SiO_2$ nanoparticles, respectively. Based on the results from TEM and XRD analysis, it is believed that the silica addition on the flame synthesis of $TiO_2$ nanoparticles reduces the particle size distribution and raises the temperature of the phase transition from anatase to rutile. But the reduced sizes of the synthesized particles due to the silica addition made the sintering and phase transformation of particles more easily.

STUDIES FOR THE CHARACTER OF THE POROUS SILICA CONTAINING THE NANO-SIZED TIO$_2$, PARTICLE IN THE PORE.

  • Jhun, Hyun-pyo;Kong, Woo-sik;Lee, Kyoung-chul
    • 대한화장품학회지
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    • 제24권3호
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    • pp.59-64
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    • 1998
  • In order to lower porosity of the porous silica, titanium alkoxide solution was filled in the pore of silica in the heating-vacuum condition. The specific surface area of modified samples was decreased effectively from 900 m$^2$/g to 100 m$^2$/g. (The aggregation phenomena in modified samples were improved fairly.) Samples were heated at 600 , and then the titanium alkoxide in the pore was decomposed completely to titanium oxide from TGA-DTA measurement. From SEM result, it was evident that titanium oxide did not coat the surface of the silica. The modified samples were analyzed using SEM, DTA-TGA, BET, and UV-visible spectrometer.

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태양전지의 반사방지막을 위한 Silica 코팅의 트라이볼로지 및 광학적 특성 평가 (Tribological and Optical Characteristics of Silica Coating for Anti-reflection Coating of Solar Cell)

  • 김해진;김대은
    • 정보저장시스템학회논문집
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    • 제6권2호
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    • pp.68-73
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    • 2010
  • The interest in acquiring high efficiency solar cells has been steadily increasing due to various advantages such as low-cost installation, pollution free and everlasting energy generation. In order to raise the cell efficiency, there has been a lot of effort to develop effective anti-reflection coatings. In this work, the main objective was to investigate the effects of particle size and annealing temperature of silica anti-reflection coatings to maximize the cell efficiency as well as reliability. It was shown that the light transmittance could be increased by a few percent over a certain range of wavelength using the silica coating. Also, the tribological properties of the coating could be improved through the annealing process, which led to better reliability of the coating.