• Journal of Technologic Dentistry
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• v.38 no.4
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• pp.263-272
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• 2016

Purpose: The purpose of this study is to measure and compare a degree of setting expansion of dental stone by time depending on the mixing methods and mixing ratios of dental stone, to compare the surface state of each specimen with the use of an optical camera with microscope, and thereby to provide a fundamental material for making dental prostheses. Methods: The test on setting expansion of dental stone is based on ISO 6873. With two different mixing ratios and three kinds of stone mixing methods, test groups were created, and a total of six types of specimens (N=30) were made. Based on the specimens, the setting expansion rate of each one was measured in each time slot of 24 hours, and the surface of the set stone was measured. Results: According to the analysis on setting expansion rate of stone, the setting expansion of the specimen that was created in the way of vacuum mixing at normal mixing ratio was 0.1944% at 120 minutes; the setting expansion of the specimen that was created in the way of vacuum mixing at the mixing ratio which was 40% higher than normal mixing ratio was 0.195% at 120 minutes; the setting expansion of the specimen that was created in the way of mixing with hands at normal mixing ratio and then removing bubbles in vacuum mixer was 0.196% at 120 minutes. Conclusion: The setting expansion rate of each dental stone specimen was significantly different with the lapse of time up to 24 hours(p<.001).

• The Journal of Korean Academy of Prosthodontics
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• v.37 no.6
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• pp.730-740
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• 1999

The purpose of this study was to investigate setting and thermal expansion of dental soldering investments. In order to compare expansion rates and to investigate the effect of water/powder ratio on expansion, setting and thermal expansion of low dental soldering investments were measured under three different water/powder ratio conditions. standard, 20% decreased and 20% increased. Setting expansion of investments was measured by use of dialgauge method. Each measurement was started two minutes later from the beginning of spatulation and recorded every one minute for one hour. Thermal expansion of cylindrical test specimens, 10mm diameter, 50mm length, was recorded in a thermodilatometer at heating rate of $10^{\circ}C$ per minute from $25^{\circ}C\;to\;700^{\circ}C$. The results of this study were obtained as follows: 1. Setting expansion rates under the standard water/powder ratio condition were 0.198% in Speed-E, 0.090% in Deguvest, 0.080% in CM and Hi-temp. Setting expansion of Speed-E was significantly different from those of CM, Deguvest and Hi-temp, and setting expansion of Deguvest was significantly different from those of CM and Hi-temp(p<.05). 2. Under the decreased water/powder ratio condition, there was significant increase in setting expansion of 4 dental soldering investments (p<.05). 3. There were no significant differences in setting expansions of investments except Hi-temp between standard and increased water/powder ratio condition(p<.05). 4. Thermal expansion rates under the standard water/powder ratio condition were 1.923% in Deguvest, 1.629% in Speed-E, 1.619% in Hi-temp and 1.580% in CM. No significant differences in thermal expansions under the standard water/powder ratio condition existed only between Speed-I and Hi-temp(p<.05) 5. Under the decreased water/powder ratio condition, there was significant increase in thermal expansion of CM and Deguvest but decrease in thermal expansion of Speed-E (p<.05). 6. Under the increased water/powder ratio condition, there was significant decrease in thermal expansion of CM, Deguvest and Speed-I but decrease in thermal expansion of Hi-temp(p<.05).

• Journal of Korea Foundry Society
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• v.5 no.2
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• pp.85-96
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• 1985

In order to investigate the effect of particle size and distribution of silica sand on the characteristics of investment, W/P ratio, setting time, temperature change during setting, setting expansion, thermal expansion and compressive strength of the investments were measured. In this experiment, magnesia clinker and mono ammonium phosphate were used as binder, and particle size and distribution of silica sand were classified for convinence into 10 categories. The main results obtained from this investigation were summerized as follows. 1. W/P ratio decreased with increase of particle size and evenness in distribution of sand grain. 2. Setting time decreased with increase of evenness in distribution of sand grain, and temperature during setting increased with evenness in distribution of sand grain. 3. Setting expansion decreased with increase of particle size, while it increased with evenness in distribution of sand grain. 4. Thermal expansion decreased with increase of particle size. 5. Compressive strength increased with increase of particle size and evenness in distribution of sand grain. From above results, G.F.N. 250 sand which contains 30% of 50-100 mesh could be recommended for investment casting.

• Journal of the korean academy of Pediatric Dentistry
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• v.38 no.3
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• pp.229-236
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• 2011

ProRoot MTA(Dentsply Tulsa, U.S.A) which has similar component with Portland cement has setting expansion character and long setting time. Excessive expansion can cause fracture at the apical portion of the root and decreasing of volume stability. And the long setting time makes additional visits for crown restoration and slow setting process of this material can change physical properties itself. In this study, among requirements of root canal filling material(KS P ISO 6876) which is revised at 2008, we investigated the setting time and setting expansion. Objects are recently developed OrthoMTA(BioMTA, Korea), conventional ProRoot white MTA(Dentsply Tulsa, U.S.A) and White portland cement(Union, Korea). The results in setting expansion, OrthoMTA was $0.08{\pm}0.02%$, ProRoot white MTA and White portland cement were each $0.28{\pm}0.06$, $0.80{\pm}0.25%$(p<0.05). The results in setting time, OrthoMTA, ProRoot white MTA, White portland cement were each $307.78{\pm}3.83$ min, $150.44{\pm}2.35$ min, $235.33{\pm}9.07$ min(p<0.05).

• Journal of Korea Foundry Society
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• v.5 no.2
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• pp.97-108
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• 1985

In order to investigate the effect of magnesia clinker on the characteristics of the investments, temperature change during setting, setting time, compressive strength and thermal expansion of the investments were measured, and x-ray analyses were also performed. The investments were prepared in accordance with variation of the content and the particle size of magnesia clinker respectively. From this experiment, the results were summarized as follows; 1. Temperature of the investments during setting rapidly increased with increase of MgO contents and decrease of the particle size of magnesia clinker. 2. Setting time decreased with increase of MgO contents and decrease of the particle size of magnesia clinker. 3. Compressive strength increased with increase of MgO contents and decrease of the particle size of magnesia clinker. 4. Thermal expansion decreased with increase of MgO contents and decrease of the particle size of magnesia clinker. From the above results, the investment which contains 8% of MgO (270-325mesh) could be recommended for phosphate investment castings.

• Journal of Korean Institute of Industrial Engineers
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• v.11 no.2
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• pp.141-154
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• 1985

The capacity expansion problem has been defined. Existing literatures on capacity expansion problems have been reviewed and unified under a structure of problem domain. The problem domain has been defined by three relavent coordinates; function or objective of the project, consideration of resource allocation, and consideration of project sequencing. Long range planning is of vital importance in setting up ultimately efficient capital investment plans to meet immediate demand increase. Simplified expansion sequencing example problems have been introduced and solved to help understanding of a solution scheme.

• Journal of the Korea Concrete Institute
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• v.24 no.4
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• pp.491-498
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• 2012

This study examines setting shrinkage, coefficient of thermal expansion, and elastic modulus of unsaturated polyester( UP)-methyl methacrylate(MMA) polymer concrete, which is generally used for repair of portland cement concrete pavement and manufacturing of precast products. In this study, a series of laboratory test were conducted with variables such as UP-MMA ratio, shrinkage reducing agent (SRA) content, and test temperature. The results showed that the setting shrinkage ranged from 29.2 to $82.6{\times}10^{-4}$, which was significantly affected by test temperature. Moreover, the findings revealed that the coefficient of thermal expansion, elastic modulus and ultimate strain of UP-MMA based polymer concrete ranged from 21.6 to $31.2{\times}10^{-6}/^{\circ}C$, 2.8 to $3.3{\times}10^4$ MPa, and 0.00381 to 0.00418, respectively. The results of this study will be used as important data for design and application of UP-MMA based polymer concrete.

• The Journal of Korean Academy of Prosthodontics
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• v.28 no.1
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• pp.137-163
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• 1990

The properties of a investment material can be described by the consistency at the slurry state, the setting time, the compressive strength and the thermal expansion during the casting. In this study the effect of the production parameters which are included the ratio of quartz and cristobalite, the content of binder, the water powder ratio and the content and concentration of additives on the Properties of the gypsum-bonded investments has been investigated with help of the consistency test, the vicat needle test, the compressive strength test, the thermal expansion test, x-ray diffraction and DTA thermal differential test. The experimental results showed that the constitution of a investment with W/P ratio of 0.34, 30% of gypsum, 0.8% aluminium sulfate, 2% magnesium sulfate, 0.6% sodium phosphate was adapted for the properties of the KDA Spec. No. 13 type I investment. The important experimental results are summarized as follows. 1. The consistency of the investment decreased with increasing amount of aluminium sulfate and decreasing amount of sodium phosphate. An addition of magnesium sulfate up to 2% an increase of the consistency was shown. But 3% magnesium sulfate in investment showed a decrease of the consistency. The consistency did not vary significantly with a variation of the content of gypsum and cristobalite and the W/P ratio. 2. Aluminium sulfate and the magnesium sulfate promoted the hardening and the aluminium phosphate delayed the hardening. The setting time increased with amount of gypsum. The effect of the matrix on the setting time was insignificant. With the W/P ratio of 0.34 the setting time was 14 min. 3. The compressive strength decreased with the amount of aluminium sulfate up to 0.25% and increased with the amount of aluminium sulfate greater than 3%. The compressive strength decreased as decreasing the amount of magnesium sulfate and gypsum and as increasing the W/P ratio. The effect of the refractory on the compressive strength was also not significant. With the W/P ratio of 0.34 the compressive strength was $34Kg/mm^2$. 4. The 1st thermal expansion was found at the temperature near and the steady state or the contraction stage was found at the temperature between $250^{\circ}C$ and $500^{\circ}C$. After this stage the 2nd thermal expansion took place at the temperature near $500^{\circ}C$. The amount of thermal expansion increased with decreasing the content of magnesium sulfate, aluminium sulfate and gypsum and the W/P ratio. And the amount of thermal expansion increased as the content of sodium phosphate and cristobalite. With the W/P ratio of 0.34 the amount of total expansion was 1.2%.

• The Journal of Korean Academy of Prosthodontics
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• v.29 no.1
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• pp.139-165
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• 1991

The properties of a investment material can be described by the consistency at the slurry state, the setting time, the compressive strength and the thermal expansion during the casting. In this study the effect of the production parameters which are included the ratio of quartz and cristobalite, the content of binder, the water powder ratio and the content and concentration of additives on the properties of the gypsum-bonded investments has been investigated with help of the consistency test, the vicat needle test, the compressive strength test, the thermal expansion test, x-ray diffraction and DTA thermal differential test. The experimental results showed that the constitution of a investment with W/P ratio of 0.34, 30% of gypsum, 0.8% aluminium sulfate, 2% magnesium sulfate, 0.6% sodium phosphate was adapted for the properties of the KDA Spec. No. 13 type I investment. The important experimental results are summarized as follows. 1. The consistency of the investment decreased with increasing amount of aluminium sulfate and decreasing amount of sodium phosphate. An addition of magnesium sulfate up to 2% an increase of the consistency was shown. But 3% magnesium sulfate in investment showed a decrease of consistency. The consistency did not vary significantly with a variation of the content of gypsum and cristobalite and the W/P ratio. 2. Aluminium sulfata and the magnesium sulfate promoted the hardening and the aluminium phoshpate delayed the hardening. The setting time increased with amount of gypsum. The effect of the matrix on the setting time was insignificant. With the W/P ratio of 0.34 the setting time was 14 min. 3. The compressive strength decreased with the amount of aluminium sulfate up to 0.25% and increased with the amount of aluminium sulfate greater than 3%. The compressive strength decreased as decreasing the amount of magnesium sulfate and gypsum and as increasing the W/P ratio. The effect fo the refractory on the compressive strength was also not significant. With the W/P ratio of 0.34 the compressive strength was $34Kg/mm^2$. 4. The 1st thermal expansion was found at the temperature near $250^{\circ}C$ and the steady state or the contraction stage was found at the temperature between $250^{\circ}C$ and $500^{\circ}C$. After this stage the 2nd thermal expansion took place at the temperature near $500^{\circ}C$. The amount of thermal expansion increased with decreasing the content of magnesium sulfate, aluminium sulfate and gypsum and the W/P ratio. And the amount of thermal expansion increased as the content of sodium phosphate ad cristobalite. With the W/P ratio of 0.34 the amount of total expansion was 1.2%.

• Structural Engineering and Mechanics
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• v.49 no.6
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• pp.763-773
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• 2014

The recently developed Ultra High Performance Concrete (UHPC) displays outstanding compressive strength and ductility but is also subjected to very large autogenous shrinkage. In addition, the use of forms and reinforcement to confine this autogenous shrinkage increases the risk of shrinkage cracking. Accordingly, this study adopts a combination of shrinkage reducing admixture and expansive admixture as a solution to reduce the shrinkage of UHPC and estimates its appropriateness by evaluating the compressive and flexural strengths as well as the autogenous shrinkage according to the age. Moreover, the coefficient of thermal expansion known to experience sudden variations at early age is measured in order to evaluate exactly the autogenous shrinkage and the thermal expansion is compensated considering these measurements. The experimental results show that the compressive and flexural strengths decreased slightly at early age when mixing 7.5% of expansive admixture and 1% of shrinkage reducing admixture but that this decrease becomes insignificant after 7 days. The use of expansive admixture tended to premature the setting of UHPC and the start of sudden increase of autogenous shrinkage. Finally, the combined use of shrinkage reducing admixture and expansive admixture appeared to reduce effectively the autogenous shrinkage by about 47% at 15 days.