• 제목/요약/키워드: Semi-solid

검색결과 480건 처리시간 0.024초

반응고 재료에서 점성을 고려한 고상입자의 거동예측을 위한 수치모사 해석 (Dynamic Simulation of Solid Particle Considering Change by Viscosity in Rheology Material)

  • 권기영;강충길
    • 소성∙가공
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    • 제18권1호
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    • pp.26-38
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    • 2009
  • It was reported that the semi-solid forming process has many advantages over the conventional forming process, such as a long die life, good mechanical properties and energy savings. It is very important, however, to control liquid segregation to gain mechanical property improvement of materials. During forming process, rheology material has complex characteristics, thixotropic behavior. Also, difference of velocity between solid and liquid in the semi-solid state material makes a liquid segregation and specific stress variation. Therefore, it is difficult for a numerical simulation of the rheology process to be performed. General plastic or fluid dynamic analysis is not suitable for the behavior of rheology material. The behavior and stress of solid particle in the rheology material during forging process is affected by viscosity, temperature and solid fraction. In this study, compression experiments of aluminum alloy were performed under each other tool shape which is rectangle shape(square array), rectangle shape(hexagonal array), and free shape tool. In addition, the dynamics behavior compare with Okano equation to power law model which is viscosity equation.

Solid-state Synthesis of $Mg_2X$ (X=Si, Ge, Sn and Pb) via Bulk Mechanical Alloying

  • Aizawa, Tatsuhiko;Song, Renbo
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.831-832
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    • 2006
  • Solid-state processing via the bulk mechanical alloying enables us to directly fabricate $Mg_2X$ semi-conductive material performs. Precise control of chemical composition leads to investigation on the dilution and enrichment of X in $Mg_2X$. Two types of solid-state reactivity are introduced: e.g. synthesis of $Mg_2Si$ from elemental mixture Mg-Si is nucleation-controlled process while synthesis of $Mg_2Sn$ from Mg-Sn, diffusion-controlled process. Thermoelectricity of these $Mg_2X$ is evaluated for discussion on the validity and effectiveness of this new PM route as a reliable tool for fabrication of thermoelectric compounds.

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초고압을 이용한 반고형 사과 이유식 개발 및 품질평가 (Development of Semi-Solid Apple Baby Food using High Pressure Processing and Quality Evaluation)

  • 조형용;조은경;김병철;신해헌
    • 한국식품영양학회지
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    • 제24권4호
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    • pp.777-785
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    • 2011
  • 비열처리가공기술 중 하나로 새롭게 주목받고 있는 초고압처리를 반고형 형태의 친환경 유기농 이유식 제조에 적용하여 완제품 형태로 제조 후 냉장 조건으로 저장하여 저장기간에 따른 제품 안전성을 조사하였다. 가열 처리를 하지 않고 550 MPa 압력에서 3분 동안 초고압 처리하여 냉장 상태로 15일 동안 저장한 결과, 일반세균과 대장균 모두 검출되지 않아 미생물학적 안전성을 확인할 수 있었으며, 초고압 처리를 하지 않은 대조군에서 일반세균이 $2.54{\times}10^3$, $7.85{\times}10^2$ CFU/g 수준으로 검출되었던 것과 비교했을 때 초고압 처리를 하는 것이 제품의 신선도를 살리고 제품의 안전성을 유지하기 위해 적합한 처리법이라고 판단되어진다. 초고압 처리를 통한 물성 변화는 처리 전 대조구와 점도, 스푼풀 현상을 비교하였을 때 큰 차이가 나타나지 않는 것으로 나타났고, 그 결과 사과의 신선한 상태를 유지하고 미생물학적 안전성 역시 유지하면서 냉장상태로 약 2주간 저장이 가능한 친환경 반고형 이유식을 제조할 수 있었다.

캐비티 공진기를 이용한 반고체 상태 물질의 복소 비유전율 측정 방법 (Method for Measurement of Complex Relative Permittivity of Semi-Solid Materials Using Novel Cavity Resonator Design)

  • 박래승;장지현;박병덕;김준환;박상복;정용식;천창율
    • 한국전자파학회논문지
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    • 제25권8호
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    • pp.872-878
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    • 2014
  • 본 논문은 새로운 캐비티 공진기 구조를 이용한 반고체 상태 물질의 복소 비유전율 측정 방법을 제안하고 있다. 윗면에 개구면이 존재하고, Ground 판이 분리되어 있는 구조를 이용하여 반고체 상태 물질도 캐비티 내부에 위치할 수 있도록 했다. 공진주파수의 변화와 Critical-Points Method를 이용해 실험적으로 증류수와 0.9 % 식염수의 복소 비유전율을 측정하였으며, 측정값을 Cole-Cole Equation을 통해 이론값과 비교했다.

반용융 성형된 반응고 A356 합금의 인장 특성 (Tensile Properties of Thixoformed Semi-solid A356 Alloy)

  • 유영빈;송팔용;김상식;이재현;이명호
    • 한국재료학회지
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    • 제10권1호
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    • pp.69-76
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    • 2000
  • 반응고 금속의 반응용 성형법은 그 우수한 성형성으로 생산공정에 있어 주조나 단조와 같은 일반 성형법에 비해 많은 장점을 가지고 있는 반면, 정밀한 공정 변수 제어가 요구되므로 실용화에 있어 크게 제한 받고 있다. 본 연구에서는 반응고 금속인 A356합금을 사용하여 밀폐형 가압 성형 전후의 기계적 특성의 변화를 관찰하여, 가압 성형시의 정확한 공정 변수 제어가 이루어지지 않았을 경우에 일어날 수 있는 기계적 특성의 감소 원인이 가압 성형에 의한 미세조직의 응집과 조대화에 있음을 미세조직과 파단면 관찰을 통하여 규명하였다. 또한 가압 성형 후 본 연구에서 \`반응고 열처리\`라 명명한 후 처리 공정을 적용하여 인장 특성을 향상시킬수 있었다.

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단호박을 이용한 반고형 이유식의 제조 (Preparation of Semi-solid Infant Foods Using Sweet-pumpkin)

  • 박현경;임성경;손경희;김현정
    • 한국식품영양과학회지
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    • 제30권6호
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    • pp.1108-1114
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    • 2001
  • 호박을 이용한 반고형 이유식을 제조하기 위하여 단호박과 늙은호박을 각각 마쇄하거나, 찌거나, 데친 후 각각을 체에 내리고 가열하여 puree를 만들고, 이들의 수분함량, 점도, 색도, $\beta$-carotene 함량, riboflavin 함량, ascorbic acid 함량을 측정하고, 관능검사를 실시하였다. 단호박퓨레가 호박퓨레보다 수분 함량이 적었고, 점도, Hunter L, a, b 색도, $\beta$-carotene 함량, riboflavin 함량은 높았다. 관능검사를 실시하여 단맛과 전체적인 선호도가 높은 찐 단호박 퓨레를 이유식의 주원료로 선택하였다. 변성전분의 혼합비율이 증가할수록 호화개시온도는 낮아지고 최고점도는 증가하였다. 찐 단호박 퓨레에 변성전분, 쌀가루, 유제품을 혼합하여 제조한 이유식은 살균과정에서 색도의 변화는 적었으나 점도가 증가하였는데 변성전분 3%를 혼합한 이유식은 점도가 안정하였다. 전체적인 선호도가 찐 단호박퓨레 40%, 쌀가루 7%와 전지분유 3%, 물 50%를 혼합한 단호박 이유식이 가장 높았다.

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폴리오르소에스텔을 이용한 나록손의 반고형 이식제제의 방출, 생체적합성 및 약물동력학적 연구 (Release, Biocompatibility and Pharmacokinetics of Semi-solid Naloxone Implants of Poly(ortho ester))

  • 임상희;박주애;김길수
    • Journal of Pharmaceutical Investigation
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    • 제29권1호
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    • pp.21-27
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    • 1999
  • Semi-solid poly(ortho esters) (POE) were prepared to provide bioerodible carriers for sustained drug delivery systems of naloxone (NLX) in the treatment of narcotic addiction. As the POE have viscous behavior at room temperature, a significant advantage of this polymer is that it can be injected without any surgical intervention. The POE was synthesized by a transesterification reaction between 1,2,6-hexanetriol and trimethyl orthoacetate, and the structure of the polymer was confirmed by IR. The in vitro release of the drug from POE was studied. The release rate of NLX decreased with increasing intrinsic viscosities of the polymer. In vivo biocompatibility studies were carried out in rats with NLX loaded POE. Histopathological analysis showed that NLX implants are well-tolerated by rats when used subcutaneously. Pharmacokinetic studies of POE-NLX implants of two different viscosities were carried out in rabbits. In all cases, plasma concentrations of NLX were maintained over 1 ng/ml for at least 168 hours, but initial burst effect was observed. Mean residence time(MRT) was found to depend on the viscosity of the polymer.

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폴리오르소에스터를 이용한 니페디핀의 반고형 이식제제의 제조 및 평가 (Preparation and Evaluation of Semi-Solid Nifedipine Implants of Poly(ortho esters))

  • 이새별;박주애;이승진;김길수
    • Journal of Pharmaceutical Investigation
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    • 제29권2호
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    • pp.93-98
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    • 1999
  • Semi-solid poly(ortho esters) (POE) were prepared to provide bioerodible carriers for sustained drug delivery systems of nifedipine in the treatment of cardiovascular disease. As the POE has viscous behavior at room temperature, a significant advantage of this polymer is that it can be injected without any surgical intervention. The POE was synthesized by a transesterification reaction between 1,2,6-hexanetriol and trimethyl orthoacetate and the nifedipine release from POE was studied in vitro. The release rate of nifedipine decreased with increasing the amount of nifedipine and the diethanolamine dispersed in the polymer. But the excess amounts, above 3%, of diethanolamine retarded the release of nifedipine. In vivo biocompatibility studies were carried out in rats with nifedipine loaded POE. Histopathological analysis showed that nifedipine loaded POE implants were well-tolerated by rats when used subcutaneously. In case of the rats implanted POE containing diethanolamine, tissue necrosis and inflammation were occured. Pharmacokinetic studies of nifedipine loaded POE implants were carried out in rabbits. In all cases, plasma concentrations of nifedipine were maintained over 15 ng/ml for at least 360 hours and biological half $life(t_{1/2})$ and mean residence time(MRT) were increased by addition of diethanolamine.

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The Theoretical Study of the Measuring Thermal Diffusivity of Semi-Infinite Solid Using the Photothermal Displacement

  • Jeon, PiIsoo;Lee, Kwangjai;Yoo, Jaisuk;Park, Youngmoo;Lee, Jonghwa
    • Journal of Mechanical Science and Technology
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    • 제18권10호
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    • pp.1712-1721
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    • 2004
  • A method of measuring the thermal diffusivity of semi-infinite solid material at room temperature using photothermal displacement is proposed. In previous works, within the constant thickness of material, the thermal diffusivity was determined by the magnitude and phase of deformation gradient as the relative position between the pump and probe beams. In this study, however, a complete theoretical treatment of the photothermal displacement technique has been performed for thermal diffusivity measurement in semi-infinite solid materials. The influence of parameters, such as, radius and modulation frequency of the pump beam and the thermal diffusivity, was studied. We propose a simple analysis method based on the zero -crossing position of real part of deformation gradient and the minimum position of phase as the relative position between two beams. It is independent of parameters such as power of pump beam, absorption coefficient, reflectivity, Poisson's ratio, and thermal expansion coefficient.