• 대한기계학회논문집B
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• 제24권1호
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• pp.21-28
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• 2000

Although commercial PIV systems have been widely used for the non-intrusive velocity field measurement of fluid flows, they are still under development and have considerable room for improvement. In this study, a single-frame double-exposure PIV system using a high-resolution CCD camera was developed. A pulsed Nd:Yag laser and high-resolution CCD camera were synchronized by a home-made control circuit. In order to resolve the directional ambiguity problem encountered in the single-frame PIV technique, the second particle image was genuinely shifted in the CCD sensor array during the time interval dt. The velocity vector field was determined by calculating the displacement vector at each interrogation window using cross-correlation with 50% overlapping. In order to check the effect of spatial resolution of CCD camera on the accuracy of PIV velocity field measurement, the developed PIV system with three different resolution modes of the CCD camera (512 ${\times}$ 512, lK ${\times}$ IK, 2K ${\times}$ 2K) was applied to a turbulent flow which simulate the Zn plating process of a steel strip. The experimental model consists of a snout and a moving belt. Aluminum flakes about $1{\mu}m$ diameter were used as scattering particles for the liquid flow in the zinc pot and the gas flow above the zinc surface was seeded with atomized olive oil with an average diameter of 1-$3{\mu}m$. Velocity field measurements were carried out at the strip speed $V_s$=1.0 m/s. The 2K ${\times}$ 2K high-resolution PIV technique was significantly superior compared to the smaller pixel resolution PIV system. For the cases of 512 ${\times}$ 512 and 1K ${\times}$ 1K pixel resolution PIV system, it was difficult to get accurate flow structure of viscous flow near the wall and small vortex structure in the region of large velocity gradient.

• 대한기계학회논문집
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• 제17권5호
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• pp.1106-1114
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• 1993

본 연구에서는우수한 섬유강화 고분자복합판의 제조 및 개량을 섬유구조의 분리. 배향의 관점에서 연구한다. 유리섬유매트는 유리섬유를 50mm의 길이로 균일하 게 절단하여 공기중에서 분산시켜 6~7mm두께로 만들고,이 유리섬유매트를 바늘의 종류와 스트레칭 횟수에 따라 니들펀칭하여 유리섬유의 매트구조를 변화시킨다. 유리 섬유의 매트구조 별로 모재와 적층시킨 다음 열압축프레스를 사용하여 1차로 시이트를 제작하고, 이 제작된 시이트를 가열로로 가열하여 2차 고온압축 프레스성형한다. 이 때 섬유와 모재의 분리 및 배향의 상관관계를 나타내는 상관계수를 구하고, 이 계수에 미치는 매트 구조의 영향에 대한 실험결과를 보고한다.

• 폴리머
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• 제27권4호
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• pp.370-376
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• 2003

나노입자의 제조 방법인 개선된 자발적 용매 확산 방법을 이용하여 폴리(DL-락타이드-co-글리콜라이드) 나노입자를 제조하였다. 고분자 용액은 물에 잘 혼합되는 유기 용매인 에탄올과 아세톤의 이종 혼합 용매를 사용하여 제조하였다. 유화제 및 안정제는 우수한 생체적합성을 갖는 PEG-PPG 블록 공중합체를 사용하였다. 최적의 나노입자 제조 조건을 얻기 위하여 나노입자 형성에 영향을 주는 인자들인 안정제의 종류 및 농도, 교반 방법, 물/오일 상의 비, 고분자의 농도 등을 고려하였다. 나노입자 제조 후, 입자의 크기 및 분산도는 광산란 입도 분석기를 이용하여 평가하였다. 제조된 나노입자는 50~200 nm의 크기와 단분산 형태의 크기분포를 보였다. 또한, 유기상과 수용액상에서 이종 혼합 용매와 고분자의 농도에 대한 적당한 조건을 조절함으로써 PLGA 나노입자의 높은 수율과 우수한 물리적 특성을 얻을 수 있었다.

• 대한토목학회논문집
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• 제8권1호
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• pp.113-125
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• 1988

우리 나라의 하천종합개발계획(河川綜合開發計劃) 수립의 기준이 되는 계획홍수량(計劃洪水量) 결정수단으로 활용되어 왔던 홍수량공식(洪水量公式) 들을 조사하였다. 이들 가운데 11종(種)의 홍수량(洪水量) 공식(公式)을 선정하여 유역규모(流域規模)에 따른 계획비홍수량(計劃比洪水量)을 계산 비교하였다. 강우조건과 유역조건이 가능한 범위까지 같은 경우가 될 수 있게 하여 검토한 바 같은 유역에서 극치들의 변동폭이 400%나 되는 편차를 가지며 이런 범위안에서 각공식 별로 서로 많은 차이를 보여 주게 됨을 알 수 있었다. 지금 쓰이고 있는 홍수량(洪水量) 산정의 절차는 무척 복잡하고 많은 노력(努力)을 거쳐서 어렵게 결정하고 있으나 성과(成果)는 사용된 수문자료(水文資料)의 기간(期間)이나 정도(精度)에 좌우되어 공학적(工學的)인 판단(判斷)의 타당성이 결여된 경우가 많았음을 경험하였다. 따라서 보다 단순하면서 합리적(合理的)인 수단의 개발을 기왕의 홍수량(洪水量) 공식(公式) 비교에서 얻을 수 있었다.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 춘계학술대회 논문집
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• pp.1155-1158
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• 2005

Micro-stereolithography is a newly proposed technology as a means that can fabricate a 3D micro structure of free form. It makes a 3D micro-structure by dividing the shape into many slices of relevant thickness along horizontal surfaces, hardening each layer of slice with a focused laser beam, and stacking them up to a desired shape. However, we do not anticipate the electric conductivity of the final product at the existing micro-stereolithography. The reason is that this technology uses polymer to make the product. Thus the new suspension which was mixed conventional photopolymer with metal powder was developed in this study. The developed suspensions were based on SL5180 which is commercialized resin and IMS03 that is made in our laboratory. And Triton X-100 was added at the suspension for getting the scattering effect and stabilizing effect. The layer recoating device was developed to be flat the mixed high viscosity suspension. A 3D micro structure was manufactured by using recoating system and micro-stereolithography system. The fabricated product was sintered to get the electric conductivity. After sintering, a pure copper product was made. In this study, new process was developed by making metal micro structure having an electric conductivity. This technology broadened the realm of the micro-stereolithography technology. And it will be applied to make the 3D micro structure of free form which has a high hardness and an electric conductivity in the near future.

• 한국진공학회지
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• 제21권3호
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• pp.171-177
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• 2012

본 연구에서는 Mn을 첨가시킨 $LiNbO_3$ 단 결정을 기술하는 스핀 해밀토니언으로 계의 고유치를 구하고, 이를 이용하여 자기 감수성을 온도 의존성으로 조사하였다. 선형응답이론에 기초한 Argyres-Sigel의 투영연산자 방법을 이용하여 계의 자체 에너지함수를 유효한 항까지 계산하였다. 초 미세구조 효과를 고려한 온도 의존성의 역 자기 감수성은 온도의 증가에 따라 그 효과가 더욱 크게 나타나는 것으로 조사되었다. 자체에너지 함수의 실수 부분인 선 너비는 온도의 증가에 따라 감소하는데 이는 온도의 증가로 인해 $Nb^{5+}$와 $Li^+$ 이온들이 산소 층과 다른 인접한 산소 층 쪽으로 이동하기 때문인 것으로 보인다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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• pp.263-263
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• 2013

This work examines the dynamic properties of ice surfaces in vacuum for the temperature range of 140~180 K, which extends over the onset temperatures for ice sublimation and the phase transition from amorphous to crystallization ice. In particular, the study focuses on the transport processes of excess protons and chloride ions in ice and their segregative behavior to the ice surface. These phenomena were studied by conducting experiments with a relatively thick (~100 BL) ice film constructed with a bottom $H_2O$ layer and an upper $D_2O$ layer, with excess hydronium and chloride ions trapped at the $H_2O$/$D_2O$ interface as they were generated by the ionization of hydrogen chloride. The migration of protons, chloride ions, and water molecules to the ice film surface and their H/D exchange reactions were measured as a function of temperature using the methods of low energy sputtering (LES) and Cs+ reactive ion scattering (RIS). Temperature programmed desorption (TPD) experiments monitored the desorption of water and hydrogen chloride from the surface. Our observations indicated that both hydronium and chloride ions migrated from the interfacial layer to segregate to the surface at high temperature. Hydrogen chloride gas desorbs via recombination reaction of hydronium and chloride ions floating on the surface. Surface segregation of these species is driven by thermodynamic potential gradient present near the ice surface, whereas in the bulk, their transport is facilitated by thermal diffusion process. The finding suggests that chlorine activation reactions of hydrogen chloride for polar stratospheric ice particles occur at the surface of ice within a depth of at most a few molecular layers, rather than in the bulk phase.

• 한국대기환경학회지
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• 제33권4호
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• pp.361-369
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• 2017

In this study, the characteristics of the dust emission according to the presence or absence of operation of the gas stove were analyzed by particle size analysis and density estimation while the mackerel was cooked while the fan was placed on the gas stove used in the home. The experiment was carried out using 20 mackerel of normal size at home. Commercially available canola oil was used as edible oil. In order to understand the characteristics such as particle size distribution of fine dust, light scattering measurement method which can be measured at intervals of several seconds was used. Particles generated by combustion of gas stove, particles formed by heating cooking oil, and particles generated by heating mackerel fish meat are judged to be nano size particles smaller than $1{\mu}m$. Therefore, it is necessary to use precise measurement method rather than the measurement method using the filter which is currently being measured in the measurement of the particles discharged from the fuel combustion or food cooking in the future. Analyzing the particle size and density of the dust emitted from the cooking stove is expected to contribute technically to the reduction of dust emissions from the cooking process of gas and fuel facilities at home and commercial facilities.

• 한국재료학회지
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• 제23권8호
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• pp.447-452
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• 2013

Recently, products that a have 3-dimensional(3D) micro structure have been in wide use. To fabricate these 3D micro structures, several methods, such as stereo lithography, reflow process, and diffuser lithography, have been used. However, these methods are either very complicated, have limitations in terms of patterns dimensions or need expensive components. To overcome these limitations, we fabricated various 3D micro structures in one step using a pair of diffusers that diffract the incident beam of UV light at wide angles. In the experiment, we used positive photoresist to coat the Si substrate. A pair of diffusers(ground glass diffuser, opal glass diffuser) with Gaussian and Lambertian scattering was placed above the photomask in the passage of UV light in the photolithography equipment. The incident rays of UV light diffracted twice at wider angles while passing through the diffusers. After exposure, the photoresist was developed fabricating the desired 3D micro structure. These micro structures were analyzed using FE-SEM and 3D-profiler data. As a result, this dual diffuser lithography(DDL) technique enabled us to fabricate various microstructures with different dimensions by just changing the combination of diffusers, making this technology an efficient alternative to other complex techniques.

• 폴리머
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• 제37권3호
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• pp.332-341
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• 2013

H-shaped amphiphilic pentablock copolymers $(PSt)_2-b-PCL-b-PEO-b-PCL-b-(PSt)_2$ was synthesized via chemoenzymatic method by combining enzyme-catalyzed ring-opening polymerization (eROP) of ${\varepsilon}$-caprolactone (${\varepsilon}$-CL) and atom transfer radical polymerization (ATRP) of styrene. By this process, we obtained copolymers with controlled molecular weight and low polydispersity. The structure and composition of the obtained copolymers were characterized by nuclear magnetic resonance (NMR), gel permeation chromatography (GPC) and infrared spectroscopy analysis (IR). The crystallization behavior of the copolymers was analyzed by differential scanning calorimetry (DSC) and X-ray diffraction (XRD). The crystallization behavior of the H-shaped block copolymers demonstrated a PCL dominate crystallization. The self-assembly behavior of the copolymers was investigated in aqueous media. The hydrodynamic diameters of the copolymer micelles in aqueous solution were measured by dynamic light scattering (DLS). The morphology of the copolymer micelles was observed by atomic force microscopy (AFM) and transmission electron microscopy (TEM). The hydrodynamic diameters of spherical micelles declined gradually with the increase of the hydrophobic chain lengths of the copolymers. The critical micelle concentration (CMC) values were determined from fluorescence emission, and it was found that the CMCs decreased with an increase of PSt hydrophobic block lengths.