• 분석과학
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• 제10권3호
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• pp.209-215
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• 1997

2차 전지의 양극(anode)으로 사용되는 Li-AGICs를 혼합가압법에 의하여 Li의 함유량에 따라 합성하였다. 이들 합성된 화합물을 X-선회절법, UV/VIS 분광학적 분석법 및 DSC 열분석법을 이용하여 특성화하였다. X-선회절분석 결과에 의하면 리튬의 함유량이 증가함에 따라 낮은 stage가 관찰되었으나, 각각의 화합물들은 혼재된 stage를 가지고 있음이 나타났다. $Li_{30wt%}$-AGIC의 경우 지배적으로 1 stage의 구조가 나타났지만 순수한 1 stage의 화합물은 얻을 수가 없었는데, 이것은 인조 흑연의 구조적 특성 때문에 예상할 수 있다. UV/VIS 분광학적 특성에 의하면 Li-AGIC의 흡수 spectra가 활성적으로 나타나지는 않았지만, $Li_{30wt%}$-AGIC의 경우 뚜렷한 $R(%)_{min}$의 형성과 함께 특징적인 흡수영역을 나타내고 있다. DSC에 의한 열역학적 결과로부터 화합물에 대하여 엔탈피의 변화량(${\Delta}H$)과 엔트로피의 변화량(${\Delta}S$)을 구하였다. 이들로부터 Li-AGIC의 발열반응과 흡열반응의 결과들은 인조 흑연 사이에 존재하던 리튬이 열에 의해 deintercalation이 일어날 때의 열적 안정성과 관련이 있음을 알 수 있다. 또한 열적 변이가 일어나는 동안 $Li_{30wt%}$-AGIC의 구조 변화에 대하여 토론하였다.

• Journal of the Korean Wood Science and Technology
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• 제34권5호
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• pp.59-66
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• 2006

The thermal properties of wood flour, Hwangto, and maleated polyethylene (MAPE) reinforced HDPE composites were investigated in this study. The thermal behavior of reinforced wood polymer composites was characterized by means of thermogravimetric (TGA) and differential scanning calorimetric (DSC) analyses. Hwangto and MAPE were used as an inorganic filler and a coupling agent, respectively. According to TGA analysis, the increase of wood flour level increased the thermal degradation of composites in the early stage, but decreased in the late stage. On the other hand, Hwangto reinforced composites showed the higher thermal stability than virgin HDPE, from the determination of differential peak temperature ($DT_p$). Decomposition temperature of wood flour and/or Hwangto reinforced composites increased with increase of heating rate. From DSC analysis, melting temperature of reinforced composites little bit increased with the addition of wood flour or Hwangto. As the loading of wood flour or Hwangto to HDPE increased, overall enthalpy decreased. It showed that wood flour and Hwangto absorbed more heat energy for melting the reinforced composites. Hwangto reinforced composites required more heat energy than wood flour reinforced composites and virgin HDPE. Coupling agent gave no significant effect on the thermal properties of composites. Thermal analyses indicate that composites with Hwangto are more thermally stable than those without Hwangto.

• 폴리머
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• 제35권3호
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• pp.196-202
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• 2011

비즈페놀 A 에폭시 수지와 폴리옥시프로필렌 디아민 경화제계의 경화 반응속도를 시차주사열량계을 이용하여 승온 및 등온 경화조건에서 조사하였다. 승온실험에서는 Ozawa와 Kissinger법을 이용하여 다양한 가열속도에서 얻어진 발열피크의 이동으로부터 활성화 에너지를 구하였다. 또한 등온실험에서 얻어진 데이터는 자촉매 효과를 고려한 Kamal의 속도모델로 분석하였으며, 그 결과 경화반응 초기의 속도우세 구간에서 실험데이터와 잘 맞았다. 반응 후기의 확산우세 구간에서는 확산효과를 적용하여 경화의 전체과정을 기술하였다. 또한 동역학분석을 이용하여 경화 후 저장 탄성률과 가교점간의 평균분자량을 측정하였다.

• Nuclear Engineering and Technology
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• 제54권6호
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• pp.1935-1946
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• 2022

The investigations of the coated-particles of nuclear fuel samples are carried out in three stages: front-end, irradiation in the reactor core, and post-irradiation examination. The front-end stage is the initial analysis of the failures rates of produced samples before they are placed in the reactor core. The purpose of the verification is to prepare the particles for an experiment that will determine the degree of damage to the coated particles at each stage. Before starting experiments with the samples, they must be properly prepared. Polishing the samples in order to uncover the inner layers is an important, initial experimental step. The authors of this paper used a novel way to prepare samples for testing - by applying an ion polisher. Mechanical polishing used frequently for sample preparations generates additional mechanical damages in the studied fuel particle, thus directly affecting the experimental results. The polishing methods were compared for three different coated particles using diagnostic methods such as Raman spectroscopy, scanning electron microscopy, and confocal laser scanning microscopy. Based on the obtained results, it was concluded that the ion polishing method is better because the level of interference with the structures of the individual layers of the tested samples is much lower than with the mechanical method. The same technique is used for the fuel particles undergone ion implantation simulating radiation damage that can occur in the reactor core.

• 한국정보과학회논문지:정보통신
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• 제35권6호
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• pp.474-481
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• 2008

스캐닝 웜은 자기 스스로 복제가 가능하며 네트워크를 통해서 짧은 시간 안에 아주 넓은 범위에 걸쳐 전파되므로 네트워크의 부하를 증가시켜 심각한 네트워크 혼잡현상을 일으킨다. 따라서 실시간으로 스캐닝 웜을 탐지하기 위해 많은 연구가 진행되고 있으나 대부분의 연구가 패킷 헤더 정보를 이용하는 방법에 중점을 두고 있으며, 이 방법은 네트워크의 모든 패킷을 검사해야 하므로 비효율적이며 탐지시간이 오래 걸린다는 단점이 있다. 따라서 본 논문에서는 네트워크 트래픽량, 트래픽량의 미분값, 트래픽량의 평균 미분값, 트래픽량의 평균 미분값과 평균 트래픽량의 곱에 대한 variance를 통해 스캐닝 웜을 탐지하는 기법을 제안한다. 실제 네트워크에서 측정한 정상 트래픽과 시뮬레이터로 생성한 웜 트래픽에 대해 성능을 분석한 결과, 기존의 탐지기법으로는 탐지되지 않는 코드레드와 슬래머를 제안한 탐지기법으로 탐지할 수 있었다. 또한 탐지속도를 측정한 결과 웜 발생초기에 모두 탐지가 되었는데, 슬래머는 발생 후 4초만에 탐지되었으며, 코드레드와 위티는 발생한지 11초만에 탐지되었다.

• Applied Microscopy
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• 제20권2호
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• pp.117-126
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• 1990

Structural changes of the vitelline envelopes during oogenesis of a polychaete, Nectoneanthes oxypoda, were examined with a scanning electron micrscope. Oocytes grow in the same coelomic fluid to the final stage, but the surface appears to change in the structure during oogenesis. Projections, which were identified to be microvilli, change in shape, number and size. Short microvilli, which cover the surface of oocyte of $33{\mu}m$ diameter densely, grow in length, reaching a maximum at the stage of $73{\mu}m$. The number of microvilli increases with the stages of oogenesis, reaching a plateau at the stage of $82{\mu}m$. The observations suggest that control of material transport including yolk precursor proteins may be correlated with the structural changes in the microvilli.

• 한국공작기계학회논문집
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• 제16권3호
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• pp.23-30
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• 2007

Nano-stages are used in many ultra-precision systems, such as scanning probe microscope(SPM), optical fiber aligners, ultra-precision cutting, measuring systems, and optical systems. It is difficult to find the solutions because the performances and characteristics of nano-scale motion stage are determined by various factors. To understand effects of nano-scale motion stage, three types of hinge structures were designed and manufactured. Each hinge structures were designed following with the results of simulation. And from the result of experiments, hysteresis, displacement, and accuracy were compared with each hinge structures.

• 대한암한의학회지
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• 제15권1호
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• pp.111-117
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• 2010

Background & Objectives: Colorectal Cancer is 10% of all cancer incidence and the motality from colorectal cancer is nearly 450,000 a year. Since chemopreventive agents from Herbal medicine is hot issue recently, to prove antitumor effecicacy of Rhus vernifciflua STOKES decoction (Chijong-dan), clinical study was carried out. Here we report one patient with colorectal cancer of stage IV. The patient had a colorectal cancer (Stage IV, T4N2M1), lymph node metastases and underwent chemotherapy. Methods: The patient visited Hana oriental medicine Clinic in 2009 and was treated using Chijong-dan for 1 year at Hana Oriental Clinic. Results: Chijongdan showed no side effect during its treatment and tumor size was retarded based on CT scanning. Overall, this case report suggests that Rhus vernifciflua STOKES decoction can be a potent cancer preventive agents for colorectal cancer but it is still required to verify the scientific and clinical evidences for Rhus vernifciflua STOKES decoction (Chijong-dan).

• International Journal of Contents
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• 제11권4호
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• pp.56-69
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• 2015

This paper proposes an efficient image encryption scheme based on quintuple encryption using two chaotic maps. The encryption process is realized with quintuple encryption by calling the encrypt(E) and decrypt(D) functions five times with five different keys in the form EDEEE. The decryption process is accomplished in the reverse direction by invoking the encrypt and decrypt functions in the form DDDED. The keys for the quintuple encryption/decryption processes are generated by using a Tent map. The chaotic values for the encrypt/decrypt operations are generated by using a Gumowski-Mira map. The encrypt function E is composed of three stages: permutation, pixel value rotation and diffusion. The permutation stage scrambles all the rows and columns to chaotically generated positions. This stage reduces the correlation radically among the neighboring pixels. The pixel value rotation stage circularly rotates all the pixels either left or right, and the amount of rotation is based on chaotic values. The last stage performs the diffusion four times by scanning the image in four different directions: Horizontally, Vertically, Principal diagonally and Secondary diagonally. Each of the four diffusion steps performs the diffusion in two directions (forward and backward) with two previously diffused pixels and two chaotic values. This stage ensures the resistance against the differential attacks. The security and performance of the proposed method is investigated thoroughly by using key space, statistical, differential, entropy and performance analysis. The experimental results confirm that the proposed scheme is computationally fast with security intact.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2006년도 춘계학술대회 논문집
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• pp.665-666
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• 2006

In precision laser microfabrication, focusing is essential to acquire good machining precision and uniform machining quality. If it does not perform, laser machining cannot be realized. So, confocal scanning method with high depth resolution is used for focus detection technique. This paper is concerned with a procedure for design, analysis and performance test of an autofocus fine actuating stage, which is composed of flexure-hinge type lever mechanism and piezoelectric actuator. Through series of analytical design, the stage is simplified as a rigid bodies(lever and main body) and springs(flexure hinges). The simplified model was applied to determine the dimension of flexure hinges and lever. After structural analysis confirmed design requirement, an actual stage was made and verified through an experiment on the static and dynamic characteristics(maximum stroke and 1st natural frequency). The fabricated stage was satisfied with the design requirement.