• 한국진공학회:학술대회논문집
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• 한국진공학회 2010년도 제39회 하계학술대회 초록집
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• pp.209-209
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• 2010

금(Au) 또는 은(Ag) 금속 나노입자의 모양, 크기, 분포 상태를 조절하여 가시광선과 적외선, 자외선 영역에서 강한 표면 플라즈몬 효과을 이용할 수 있는데, 최근 이러한 금속 나노입자의 표면플라즈몬 효과를 이용하여 태양광 소자의 성능을 향상시키는 연구가 매우 활발하게 이루어지고 있다. 그 중, 높은 효율과 낮은 제작비용 그리고 간단한 공정과정의 장점을 갖고 있어서 크게 주목 받고 있는 염료감응태양전지에서도 금(Au) 또는 은(Ag) 금속 나노입자을 이용하기 위한 많은 연구가 진행되고 있다. 그 예로, Au가 코팅된 $TiO_2$ 기반의 염료감응태양전지구조를 제작하여, 입사된 빛이 표면플라즈몬 효과를 통해, Au에서 여기된 전자들이 Au/$TiO_2$ 사에의 schottky 장벽을 통과하여 $TiO_2$의 전도대 전자들의 밀도가 증가하여, charge carrier generating rate을 높여 소자의 광변환 효율의 향상을 증명하였다. 이에 본 연구에서는, $TiO_2$보다 높은 전자 이동도(mobility)와 직선통로(direct path way)의 장점을 갖고 있는 ZnO nanorod에서의 charge carrier generating rate을 높일 수 있도록, 비교적 가격이 저렴한 Ag nanoparticle을 코팅하였다. ZnO nanorod 제작은 낮은 온도에서 간단하게 성장시킬 수 있는 hydrothermal 방법을 이용하였다. 기판위에 RF magnetron 스퍼터를 이용하여 AZO seed layer를 증착한 후, zinc nitrate $Zn(NO_3)_2{\cdot}6H_2O$과 hexamethylentetramines (HMT)으로 혼합된 용액을 사용해 ZnO nanorods를 성장시켰다. 이 후, Ag를 형성할 수 있도록 열증기증착법을 이용하여 코팅하였다. Ag의 증착시간에 따른 ZnO nanorods에서의 코팅된 구조와 형태를 관찰하기 위해 field emission scanning electron microscopy (FE-SEM)을 이용하여 측정하였으며, 결정성을 조사하기 위해 X-ray diffraction (XRD)을 이용하여 분석하였다. 또한 입사된 빛에 의해, 여기된 ZnO 전도대 전자들이 다시 재결합을 통해 방출되는 photoluminescence 양을 scanning PL 장비를 통해 측정하여 Ag가 코팅된 ZnO nanorod의 광특성을 분석하였다.

• Current Optics and Photonics
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• 제2권5호
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• pp.474-481
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• 2018

We propose a polarization phase-shifting technique to investigate the thickness of $Ta_2O_5$ thin films deposited on BK7 substrates, using a modified Sagnac interferometer. Incident light is split by a polarizing beam splitter into two orthogonal linearly polarized beams traveling in opposite directions, and a quarter-wave plate is inserted into the common path to create an unbalanced phase condition. The linearly polarized light beams are transformed into two circularly polarized beams by transmission through a quarter-wave plate placed at the output of the interferometer. The proposed setup, therefore, yields rotating polarized light that can be used to extract a relative phase via the self-reference system. A thin-film sample inserted into the cyclic path modifies the output signal, in terms of the phase retardation. This technique utilizes three phase-shifted intensities to evaluate the phase retardation via simple signal processing, without manual adjustment of the output polarizer, which subsequently allows the thin film's thickness to be determined. Experimental results show that the thicknesses obtained from the proposed setup are in good agreement with those acquired by a field-emission scanning electron microscope and a spectroscopic ellipsometer. Thus, the proposed interferometric arrangement can be utilized reliably for non-contact thickness measurements of transparent thin films and characterization of optical devices.

• Journal of Ceramic Processing Research
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• 제20권5호
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• pp.484-489
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• 2019

VO2 is an attractive candidate as a transition metal oxide switching material as a selection device for reduction of sneak-path current. We demonstrate deposition of nanoscale VO2 thin films via thermal atomic layer deposition (ALD) with H2O reactant. Using this method, we demonstrate VO2 thin films with high-quality characteristics, including crystallinity, reproducibility using X-ray diffraction, and X-ray photoelectron spectroscopy measurement. We also present a method that can increase uniformity and thin film quality by splitting the pulse cycle into two using scanning electron microscope measurement. We demonstrate an ON / OFF ratio of about 40, which is caused by metal insulator transition (MIT) of VO2 thin film. ALD-deposited VO2 films with high film uniformity can be applied to next-generation nonvolatile memory devices with high density due to their metal-insulator transition characteristic with high current density, fast switching speed, and high ON / OFF ratio.

• Nuclear Engineering and Technology
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• 제54권10호
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• pp.3795-3802
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• 2022

NaI(Tl) scintillation materials are considered to be one of many materials that are used exclusively for γ-ray detection and spectroscopy. The gamma-ray spectrometer is not an easy-to-use device, and the accuracy of the numerical values must be carefully checked based on the rules of the calibration technique. Therefore, accurate information about the detection system and its effectiveness is of greater importance. The purpose of this study is to estimate, using an analytical-numerical formula (ANF), the purely geometric solid angle, geometric efficiency, and total efficiency of a cylindrical NaI(Tl) γ-ray detector with a side-through hole. This type of detector is ideal for scanning fuel rods and pipelines, as well as for performing radio-immunoassays. The study included the calculation of the complex solid angle, in combination with the use of various points like gamma sources, located axially and non-axially inside the through detector side hole, which can be applied in a hypothetical method for calibrating the facility. An extended γ-ray energy range, the detector, source dimensions, "source-to-detector" geometry inside the side-through hole, path lengths of γ-quanta photons crossing the facility, besides the photon average path length inside the detector medium itself, were studied and considered. This study is very important for an expanded future article where the radioactive point source can be replaced by a volume source located inside the side-trough hole of the detector, or by a radioactive pipeline passing through the well. The results provide a good and useful approach to a new generation of detectors that can be used for low-level radiation that needs to be measured efficiently.

• Restorative Dentistry and Endodontics
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• 제48권1호
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• pp.4.1-4.10
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• 2023

Objectives: This study aimed to compare the torsional and cyclic fatigue resistance of ProGlider (PG), WaveOne Gold Glider (WGG), and TruNatomy Glider (TNG). Materials and Methods: A total of 15 instruments of each glide path system (n = 15) were used for each test. A custom-made device simulating an angle of 90° and a radius of 5 millimeters was used to assess cyclic fatigue resistance, with calculation of number of cycles to failure. Torsional fatigue resistance was assessed by maximum torque and angle of rotation. Fractured instruments were examined by scanning electron microscopy (SEM). Data were analyzed with Shapiro-Wilk and Kruskal-Wallis tests, and the significance level was set at 5%. Results: The WGG group showed greater cyclic fatigue resistance than the PG and TNG groups (p < 0.05). In the torsional fatigue test, the TNG group showed a higher angle of rotation, followed by the PG and WGG groups (p < 0.05). The TNG group was superior to the PG group in torsional resistance (p < 0.05). SEM analysis revealed ductile morphology, typical of the 2 fracture modes: cyclic fatigue and torsional fatigue. Conclusions: Reciprocating WGG instruments showed greater cyclic fatigue resistance, while TNG instruments were better in torsional fatigue resistance. The significance of these findings lies in the identification of the instruments' clinical applicability to guide the choice of the most appropriate instrument and enable the clinician to provide a more predictable glide path preparation.

• 대한기계학회논문집A
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• 제21권1호
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• pp.104-111
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• 1997

Accounting for the additional damages come out from non-proportional loading path effect, material damage according to crystal structure dependence was studied. Microscopic observations of damaged material by SEM(Scanning Electron Microscope) showed crystal structure dependence. Biaxial in-phase loaded specimens showed the slips of same direction, which pararell each other, but biaxial 90.deg. out-of-phase loaded specimens showed multiply crossed slips. S. H. Doong and D. F. Socie reported that wavy/planar or planar slip material showed the increase in the cyclic hardening level during non-proportional cycling. From these results, the additional hardening and non-proportional loading effects were related with slip mechanism, and the slip mechanism was related with crystal structure. In the present study, a damage mechanism which accounts for the non-proportional loading effect from crystal structure dependence was considered and applied to A17075-T651.

• 제어로봇시스템학회논문지
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• 제21권6호
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• pp.497-502
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• 2015

One of the goals in the field of mobile robotics is the development of personal service robots for the elderly which behave in populated environments. In this paper, we describe a security robot system and ongoing research results that minimize the risk of the elderly and the infirm to access an area to enter restricted areas with high potential for falls, such as stairs, steps, and wet floors. The proposed robot system surveys a potential falling area with an equipped laser scanner sensor. When it detects walking in elderly or infirm patients who in restricted areas, the robot calculates the velocity vector, plans its own path to forestall the patient in order to prevent them from heading to the restricted area and starts to move along the estimated trajectory. The walking human is assumed to be a point-object and projected onto a scanning plane to form a geometrical constraint equation that provides position data of the human based on the kinematics of the mobile robot. While moving, the robot continues these processes in order to adapt to the changing situation. After arriving at an opposite position to the human's walking direction, the robot advises them to change course. The simulation and experimental results of estimating and tracking of the human in the wrong direction with the mobile robot are presented.

• Corrosion Science and Technology
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• 제12권5호
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• pp.227-232
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• 2013

A number of components installed in the secondary system of nuclear power plants are exposed to aging mechanisms such as FAC (Flow-Accelerated Corrosion), Cavitation, Flashing, and LDIE (Liquid Droplet Impingement Erosion). Those aging mechanisms can lead to thinning of the components. In April 2013, one (1) inch small bore piping branched from the main steam line experienced leakage resulting from wall thinning in a 1,000 MWe Korean PWR nuclear power plant. During the normal operation, extracted steam from the main steam line goes to condenser through the small bore piping. The leak occurred in the downstream of an orifice. A control valve with vertical flow path was placed on in front of the orifice. This paper deals with UT (Ultrasonic Test) thickness data, SEM images, and numerical simulation results in order to analyze the extent of damage and the cause of leakage in the small bore piping. As a result, it is concluded that the main cause of the small bore pipe wall thinning is liquid droplet impingement erosion. Moreover, it is observed that the leak occurred at the reattachment point of the vortex flow in the downstream side of the orifice.

• 열처리공학회지
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• 제22권1호
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• pp.3-7
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• 2009

Variation in oxidation behavior with heat treatment temperature is investigated for a Ni-Ti alloy using X-ray diffraction, DSC (differential scanning calorimetry) and Auger electron spectroscopy. And the effect of oxidation on transformation behavior and superelasticity is characterized. A cold-worked 50.6Ni-Ti alloy is oxidized at 300-$700^{\circ}C$ for 1 hr in the air atmosphere. With an increase in heating temperature, the structure of $TiO_2$ changes from amorphous (300 and $400^{\circ}C$) to anatase ($500^{\circ}C$), and to rutile ($700^{\circ}C$). Activation energy of oxidation for NiTi is measured to be 51 Kcal/mol when heating temperature is $500^{\circ}C$ or above. Since Ti reacts preferably with oxygen, Ni content increases between matrix and oxide, forming $Ni_{3}Ti$ compounds. The resultant of oxidation decreases significantly $M_s$ and $A_s$ temperature in the specimen oxidized at $900^{\circ}C$ with $B_2{\rightarrow}M$ transformation path. An extra is found on cooling between two peaks in the specimen with $B_2{\rightarrow}R{\rightarrow}M$ one which is oxidized at $900^{\circ}C$ and aged at $500^{\circ}C$. Oxidation deteriorates superelasticity due to formation of Ni-rich compound.

• 한국전자파학회지:전자파기술
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• 제4권2호
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• pp.34-40
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• 1993

Mobile 시스템을 위한 마이크로스트립 안테나는 공진 주파수가0.88GHz되게 섣계하였다. 마이크로스 트럽 어레이 안테나를 Tchebyscheff 다항식을 이용하여 구형 마이크보스트립 패치 크기에 의존하도록 상대적 전류 분포닫 1:4.69:1되게 설계하고 주 부엽 차를 20dB의 이펀치로 설계하였다. 설계된 마이크 로스트립 어레이 패치 안테나는 반사 손실, V.S.W.R, 방사 패턴, 벤드폭등 여라 특성을 측정하였고 이론치와 서로 일치함을 확인하였다 또한 빔 스케닝블 위해 상대적 전류 분포에 따른 패치 어레이 안테나의 위상 변환 과정을 제시했다.