• Transactions of Materials Processing
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• v.30 no.4
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• pp.195-200
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• 2021

In this study, we investigated the dominant processing variables that would influence the microstructural development of AA6061 deformed by differential speed rolling (DSR) at ambient temperature. For this purpose, we carried out a series of DSR on the samples to investigate the effects of roll speed ratio, sample rotation, and number of operation under specific rotation. Among these, the condition with a height reduction of 75% at a speed ratio of 1:4 through rotation along rolling direction (RR) displayed the pronounced results of more homogenous matrix-structure and superior mechanical properties than the others tested in this study. This was mainly due to the cross shearing of macro-shear pattern in segment where dynamic recrystallization took place with ease throughout the sample. Thus, an average microhardness value of 101 Hv was obtained in the present sample deformed by 4-pass DSR with RR where macro cross-shearing was effectively applied.

• Bulletin of the Korean Chemical Society
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• v.23 no.11
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• pp.1590-1594
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• 2002

Liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry (LC-APCI-MS) has been used for the determination of sulfonamides in meat. Five typical sulfonamides were selected as target compounds, and beef meat was selected as a matrix sample. As internal standards, sulfapyridine and isotope labeled sulfamethazine (${13}^C_6$-SMZ) were used. Compared to the results of recent reports, our result have shown improved precision to a RSD of 1.8% for the determination of sulfamethazine spiked with 75 ng/g level in meat.

• Journal of the Korean Statistical Society
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• v.24 no.1
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• pp.1-18
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• 1995

The generalized logit model of nominal type with random regressors is studied for bootstrapping. In particular, asymptotic normality and consistency of bootstrap model estimators are derived. It is shown that the bootstrap approximation to the distribution of the maximum likelihood estimators is valid for alsomt all sample sequences.

• Proceedings of the KIEE Conference
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• 1992.07b
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• pp.727-729
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• 1992

In this study, the piezoelectric composites with 1-3 connectivity have been studied. A piezoelectric ceramics PZT prepared by Flux method is used as a filler in a epoxy Eccogel polymer matrix. The piezoelectric coefficients were increased as PZT volume% increases, and resonance frequency was moved to lower frequency as the sample thickness increased. The acoustic matching impedance with water is lowered than single phase PZT ceramics.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.17 no.4
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• pp.363-373
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• 2019

Waste characterisation associated with nuclear site decommissioning relies on radiochemical analysis of a diverse range of sample types, requiring extensive validation of analytical techniques using matrix-matched materials. The absence of relevant reference materials has hindered robust method development and validation. The paper discusses how method validation in support of nuclear waste characterisation can be achieved without using reference materials. The key stages in an analytical procedure are evaluated and a multi-stage approach is proposed with the ultimate aim of determining an operational envelope for an analytical procedure.

• Proceedings of the KIEE Conference
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• 1989.11a
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• pp.176-179
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• 1989

Newton's OPF algorithm, for each iteration, solves with second order approximation of Lagraqngian function and sparse matrix technique. When load model is applied to this technique, load voltages have tendency to be fixed at lower limit. It makes the solution inadequte. In this paper, reference bus voltage specification technique suggested to make adequate load voltage. This method is verified useful 6-bus Ward-Hale sample system.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03b
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• pp.112-115
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• 1999

The effect of intermediate annealing on the texture evolution in I.f steel was investigated by using X-ray texture measurement. After The sample was cold rolled to 80% reduction intermediate annealing was introduced to preform ${\gamma}$-fiber orientation grains in deformed matrix. The annealing time was varied between 30 and 3600 sec, These samples were cold rolled to 90% reduction and full annealed. By intermediate annealing final full annealed samples had very homogeneous ${\gamma}$-fiber orientation resulting in good deep drawability.

• Journal of the Korean Statistical Society
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• v.24 no.2
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• pp.507-518
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• 1995

The ordinary least squares based estiamte $S^2$ of the disturbance variance is considered in the linear regression model when the disturbances follow the first-order moving-average process. It is shown that $S^2$ is weakly consistent estimate for the disturbance varaince without any restriction on the regressor matrix X. Also, simple exact bounds on the relative bias of $S^2$ are given in finite sample sizes.

• Proceedings of the KIEE Conference
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• 1997.07c
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• pp.1064-1066
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• 1997

This paper proposes an efficient algorithm of designing PSS and CSS. First, the stabilizer input variable is selected using the participation matrix. Secondly, the stabilizer constants are decided using first order eigenvalue sensitivity. The proposed method was validated to sample power system.

• Bulletin of the Korean Chemical Society
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• v.18 no.11
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• pp.1172-1175
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• 1997

Calcium isotopic ratios are precisely measured by removing isobaric interferences originated from water in the plasma. Liquid Ar cryogenic trap combined with membrane desolvator could eliminate backgrounds at m/z 42 and 44. Slow drift of ICP-MS is corrected by the frequent running of the standards. It is found necessary to separate Ca from the sample matrix using Ca oxalate precipitation technique. Currently, the RSD is 0.5-1.0% for 2 minutes of measurement but is expected to be improved if the measurement time is increased. The technique was applied to 42Ca enriched baby fecal samples and successfully determined 42Ca/44Ca ratio changes.