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http://dx.doi.org/10.5012/bkcs.2002.23.11.1590

Determination of Sulfonamides in Meat by Liquid Chromatography Coupled with Atmospheric Pressure Chemical Ionization Mass Spectrometry  

Kim, Dal-Ho
Choi, Jong-Oh
Kim, Jin-Seog
Lee, Dae-Woon
Publication Information
Bulletin of the Korean Chemical Society / v.23, no.11, 2002 , pp. 1590-1594 More about this Journal
Abstract
Liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry (LC-APCI-MS) has been used for the determination of sulfonamides in meat. Five typical sulfonamides were selected as target compounds, and beef meat was selected as a matrix sample. As internal standards, sulfapyridine and isotope labeled sulfamethazine (${13}^C_6$-SMZ) were used. Compared to the results of recent reports, our result have shown improved precision to a RSD of 1.8% for the determination of sulfamethazine spiked with 75 ng/g level in meat.
Keywords
Sulfonamides; Meat; LC-APCI-MS; IDMS; SPE;
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