• Title/Summary/Keyword: Sample matrix

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Effects of Mold on Properties of SiC-$ZrB_2$ Composites through SPS (SPS법에 의한 SiC-$ZrB_2$ 복합체의 특성에 미치는 몰드의 영향)

  • Shin, Yong-Deok;Lee, Jung-Hoon;Park, Jin-Hyoung;Ju, Jin-Young;Lee, Hee-Seung
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.1515-1516
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    • 2011
  • Conductive SiC-$ZrB_2$ composites were produced by subjection a 40:60(vol%) mixture of zirconium diborided ($ZrB_2$) powder and ${\beta}$-silicon carbide (SiC) matrix to spark plasma sintering (SPS) under argon atmosphere. Inner diameters of graphite mold were $15mm{\varphi}$ and $20mm{\varphi}$, respectively. The relative densities of $15mm{\varphi}$ and $20mm{\varphi}$ sample were 99.4% and 97.88%, respectively. Reactions between ${\beta}$-SiC and $ZrB_2$ were not observed via x-ray diffraction (hereafter, XRD) analysis. The result of FE-SEM of fracture face of $15mm{\varphi}$ sample was intergranular fracture and that of $20mm{\varphi}$ sample was transgranular fracture. Because the fracture strength of $15mm{\varphi}$ sample was much higher than that of $20mm{\varphi}$ sample. The electrical resistivity, $9.37{\times}10^{-4}{\Omega}{\cdot}cm$ of $15mm{\varphi}$ sample was higher than that, $6.17{\times}10^{-4}{\Omega}{\cdot}cm$ of $20mm{\varphi}$ sample because of densification. Although sintering condition of SPS is same. the properties of sintered SiC-$ZrB_2$ compacts were changed according to inner diameter of graphite mold.

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A Methodology for Expanding Sample OD Based on Probe Vehicle (프로브 차량 기반 표본 OD의 전수화 기법)

  • Baek, Seung-Kirl;Jeong, So-Young;Kim, Hyun-Myung;Choi, Kee-Choo
    • Journal of Korean Society of Transportation
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    • v.26 no.2
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    • pp.135-145
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    • 2008
  • As a fundamental input to the travel demand forecasting, OD has been always a concern in obtaining the accurate link traffic volume. Numerous methods were applied thus far without a complete success. Some existing OD estimation techniques generally extract regular samples and expand those sample into population. These methods, however, leaves some to be desired in terms of accuracy. To complement such problems, research on estimating OD using additional information such as link traffic volume as well as sample link use rate have been accomplished. In this paper, a new approach for estimating static origin-destination (OD) using probe vehicle has been proposed. More specifically, this paper tried to search an effective sample rate which varies over time and space. In a sample test network study, the traffic volume error rate of each link was set as objective function in solving the problem. As a key result the MAE (mean absolute error) between expanded OD and actual OD was identified as about 5.28%. The developed methodology could be applied with similar cases. Some limitations and future research agenda have also been discussed.

Microstructural Evolution of Cu-15 wt%Ag Composites Processed by Equal Channel Angular Pressing (등통로각압축공정을 이용하여 제조된 Cu-15 wt%Ag 복합재의 미세구조)

  • Lee, In Ho;Hong, Sun Ig;Lee, Kap Ho
    • Korean Journal of Metals and Materials
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    • v.50 no.12
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    • pp.931-937
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    • 2012
  • The microstructure of Cu-15 wt%Ag composites fabricated by equal channel angular pressing (ECAP) with intermediate heat treatment at $320^{\circ}C$ was investigated by transmission electron microscopy (TEM) observations. Ag precipitates with a thickness of 20-40 nm were observed in the eutectic region of the Cu-15 wt%Ag composite solution treated at $700^{\circ}C$ before ECAP. The Cu matrix and Ag precipitates had a cube on cube orientation relationship. ECAPed composites exhibited ultrafine-grained microstructures with the shape and distribution dependent on the processing routes. For route A in which the sample was pressed without rotation between each pass, the Cu and Ag grains were elongated along the shear direction and many micro-twins were observed in elongated Cu grains as well as in Ag filaments. The steps were observed on coherent twin boundaries in Cu grains. For route Bc in which the sample was rotated by 90 degrees after each pass, a subgrain structure with misorientation of 2-4 degree by fragmentation of the large Cu grains were observed. For route C in which the sample was rotated by 180 degrees after each pass, the microstructure was similar to that of the route A sample. However, the thickness of the elongated grains along the shear direction was wider than that of the route A sample and the twin density was lower than the route A sample. It was found that more microtwins were formed in ECAPed Cu-15 wt%Ag than in the drawn sample. Grain boundaries were observed in relatively thick and long Ag filaments in Cu-15 wt%Ag ECAPed by route C, indicating the multi-crystalline nature of Ag filaments.

Measuring Level of Difficulty of Fingerprint Database based on Sample Quality (영상 품질 기반의 지문 데이터베이스의 난이도 정량화)

  • Ryu, Ji-Eun;Jang, Ji-Hyeon;Kim, Hak-Il
    • Journal of the Korea Institute of Information Security & Cryptology
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    • v.18 no.5
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    • pp.59-69
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    • 2008
  • The purpose of this paper is to measure the level of difficulty of fingerprint database based on sample quality. This paper proposes distribution of a sample quality analyzer and a difference of sample quality analyzer to measure the level of difficulty. Experimental results demonstrate that there are stronger correlation between matching performance and level of difficulty based on difference of sample quality than other measure. Especially, level of difficulty based on OQ Block of MPQ co-occurrence matrix shows highest correlation with matching performance, and moreover it can predict the matching performance of unknown databases.

Analytical study on nickel content in ceramic, metal and plastic materials (세라믹, 금속 및 플라스틱 소재의 니켈 함유량 분석에 관한 연구)

  • Choi, Zel-Ho
    • Analytical Science and Technology
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    • v.24 no.6
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    • pp.443-450
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    • 2011
  • Quantitative analytical condition for nickel in ceramic, metal and plastic materials using complexation and solvent extraction followed by inductively coupled plasma-atomic emission spectrometry (ICP-AES) and atomic absorption spectrophotometry (AAS) was studied. Ceramic, metal and plastic samples were dissolved by acid digestion. Nickel was determined by ICP-AES and AAS after extraction of Ni $(DMG)_2$ in $CHCl_3$. Recovery efficiency of nickel was satisfactory, and most of matrix elements causing interference could be effectively eliminated by the separation. Nickel in the certified reference materials (BAM-376 and PACS-2) were quantitatively determined without influence of sample matrix.

Effect of Isothermal Aging on the Magnetic Properties of 1Cr-0.5Mo Steel

  • Kim, Min-Gi;Ryu, K.S.;Lee, Y.H.;Park, J.S.;Kim, C.G.
    • Journal of Magnetics
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    • v.16 no.3
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    • pp.225-228
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    • 2011
  • Magnetic properties and Rockwell hardness of 1Cr-0.5Mo steel have been investigated as a function of isothermal aging time. Our results showed that coercivity, hysteresis loss and Rockwell hardness in the aged samples decreased as aging time increased. This phenomenon was analyzed using optical microscopy and scanning electron microscopy. A significant diffusion of Cr and Mo atoms formed $M_2C$ and $M_7C$ carbides, lowering the matrix strength. $M_2C$ and $M_7C$ carbides partially segregated inside grains, diffused into grain boundaries, and finally resulted in a soft ferrite matrix and a hard grain boundary. The magnetic and mechanical softening of the matrix is likely to govern the properties of the sample more than the hardening of the grain boundary by carbide precipitations.

Mechanical Properties of Unidirectional Carbon-carbon Composites as a Function of Fiber Volume Content

  • Dhakate, S.R.;Mathur, R.B.;Dham, T.L.
    • Carbon letters
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    • v.3 no.3
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    • pp.127-132
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    • 2002
  • Unidirectional polymer composites were prepared using high-strength carbon fibers as reinforcement and phenolic resin as matrix precursor with keeping fiber volume fraction at 30, 40, 50 and 60% respectively. These composites were carbonized at $1000^{\circ}C$ and graphitised at $2600^{\circ}C$ in the inert atmosphere. The carbonized and graphitised composites were characterized for mechanical properties as well as microstructure. Microscopic studies were carried out of the polished surface of carbonized and graphitised composites after etching by chromic acid, to understand the effect of fiber volume fraction on oxidation at fiber-matrix interface. It is found that the flexural strength in polymer composites increases with fiber volume fraction and so does for the carbonised composites. However, the trend was found to be reversed in graphitised composites. In all the carbonized composites anisotropic region has been observed at fiber-matrix interface which transforms into columnar type microstructure upon graphitisation. The extension of strong and weak columnar type microstructure is function of fiber volume fraction. SEM microscopy of the etched surface of the sample reveal that composites containing 40% fiber volume has minimum oxidation at the interface, revealing a strong interfacial bonding.

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A Speech Homomorphic Encryption Scheme with Less Data Expansion in Cloud Computing

  • Shi, Canghong;Wang, Hongxia;Hu, Yi;Qian, Qing;Zhao, Hong
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.13 no.5
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    • pp.2588-2609
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    • 2019
  • Speech homomorphic encryption has become one of the key components in secure speech storing in the public cloud computing. The major problem of speech homomorphic encryption is the huge data expansion of speech cipher-text. To address the issue, this paper presents a speech homomorphic encryption scheme with less data expansion, which is a probabilistic statistics and addition homomorphic cryptosystem. In the proposed scheme, the original digital speech with some random numbers selected is firstly grouped to form a series of speech matrix. Then, a proposed matrix encryption method is employed to encrypt that speech matrix. After that, mutual information in sample speech cipher-texts is reduced to limit the data expansion. Performance analysis and experimental results show that the proposed scheme is addition homomorphic, and it not only resists statistical analysis attacks but also eliminates some signal characteristics of original speech. In addition, comparing with Paillier homomorphic cryptosystem, the proposed scheme has less data expansion and lower computational complexity. Furthermore, the time consumption of the proposed scheme is almost the same on the smartphone and the PC. Thus, the proposed scheme is extremely suitable for secure speech storing in public cloud computing.

Multivariate Process Capability Indices for Skewed Populations with Weighted Standard Deviations (가중표준편차를 이용한 비대칭 모집단에 대한 다변량 공정능력지수)

  • Jang, Young Soon;Bai, Do Sun
    • Journal of Korean Institute of Industrial Engineers
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    • v.29 no.2
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    • pp.114-125
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    • 2003
  • This paper proposes multivariate process capability indices (PCIs) for skewed populations using $T^2$rand modified process region approaches. The proposed methods are based on the multivariate version of a weighted standard deviation method which adjusts the variance-covariance matrix of quality characteristics and approximates the probability density function using several multivariate Journal distributions with the adjusted variance-covariance matrix. Performance of the proposed PCIs is investigated using Monte Carlo simulation, and finite sample properties of the estimators are studied by means of relative bias and mean square error.

Selective or Class-wide Mass Fingerprinting of Phosphatidylcholines and Cerebrosides from Lipid Mixtures by MALDI Mass Spectrometry

  • Lee, Gwangbin;Son, Jeongjin;Cha, Sangwon
    • Bulletin of the Korean Chemical Society
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    • v.34 no.7
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    • pp.2143-2147
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    • 2013
  • Matrix assisted laser desorption/ionization (MALDI) mass spectrometry (MS) is a very effective method for lipid mass fingerprinting. However, MALDI MS suffered from spectral complexities, differential ionization efficiencies, and poor reproducibility when analyzing complex lipid mixtures without prior separation steps. Here, we aimed to find optimal MALDI sample preparation methods which enable selective or class-wide mass fingerprinting of two totally different lipid classes. In order to achieve this, various matrices with additives were tested against the mixture of phosphatidylcholine (PC) and cerebrosides (Cers) which are abundant in animal brain tissues and also of great interests in disease biology. Our results showed that, from complex lipid mixtures, 2,4,6-trihydroxyacetophenone (THAP) with $NaNO_3$ was a useful MALDI matrix for the class-wide fingerprinting of PC and Cers. In contrast, THAP efficiently generated PC-focused profiles and graphene oxide (GO) with $NaNO_3$ provided Cer-only profiles with reduced spectral complexity.