• 제목/요약/키워드: SLS growth mechanism

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SLS(Solid-Liquid-Solid) 성장기구에 의한 탄화규소 나노튜브의 성장 (Growth of SiC Nanotube by SLS (Solid-Liquid-Solid) Growth Mechanism)

  • 노대호;김재수;변동진;양재웅;김나리
    • 한국재료학회지
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    • 제14권2호
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    • pp.83-89
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    • 2004
  • SiC nanotubes were synthesized by SLS growth mechanism using various metal catalysts. Synthesized nanotubes had mean diameters of 20~50 nm and several $\mu\textrm{m}$ length. The kind of catalysts affected microstructures of SiC nanotubes by different diffusion routes. These differences are attributed to catalysts' physical properties and relative activities to the graphite substrate. Fe acted as a good catalyst of SLS growth mechanism. But in case of Ni, SiC nanotubes grew slowly. Optical property was measured by photoluminescence measurement. Relatively broad peak was obtained and mean peak positioned at about 430 nm. This result was the same as other nanocrystalline SiC materials, but was different from the results of bulk SiC probably due to quantum confinement effect and defect in the grown SiC nanotube.

SLS 성장방법에 의한 SiC 나노와이어의 성장 (Growth of SiC nanowires by SLS growth mechanism)

  • 노대호;김재수;변동진;진정근;김나리;양재웅
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.116-116
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    • 2003
  • Most of all nano-structures, SiC had a high electrical conductivity and mechanical strengths ay high temperatures. So It was considered a useful materials for nanosized device materials and added materials for strength hardening. Much methods were developed for SiC nanowire and nanorods like CVD, carbothermal reduction, Laser ablation and CNT-confined reduction. These methods used the VLS (Vapor-Liquid-Solid) growth mechanism. In these experiments, SiC nanowire was grown by SLS (Sold-Liquid-Solid) growth mechanism used Graphite substrate, And we characterized its microstructure to compare with VLS growth mechanism.

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S-L-S 성장기구를 이용한 양질의 골드 나노선 합성 (Synthesis of Au Nanowires Using S-L-S Mechanism)

  • 노임준;김성현;신백균;조진우
    • 한국전기전자재료학회논문지
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    • 제25권11호
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    • pp.922-925
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    • 2012
  • Single crystalline Au nanowires were successfully synthesized in a tube-type furnace. The Au nanowires were grown by vapor phase synthesis technique using solid-liquid-solid (SLS) mechanism on substrates of corning glass and Si wafer. Prior to Au nanowire synthesis, Au thin film served as both catalyst and source for Au nanowire was prepared by sputtering process. Average length of the grown Au nanowires was approximately 1 ${\mu}m$ on both the corning glass and Si wafer substrates, while the diameter and the density of which were dependent on the thickness of the Au thin film. To induce a super-saturated states for the Au particle catalyst and Au molecules during the Au nanowire synthesis, thickness of the Au catalyst thin film was fixed to 10 nm or 20 nm. Additionally, synthesis of the Au nanowires was carried out without introducing carrier gas in the tube furnace, and synthesis temperature was varied to investigate the temperature effect on the resulting Au nanowire characteristics.

촉매의 휘발법에 의한 이산화규소 나노와이어의 성장 (Growth of SiO2 Nanowire by Catalyst Evaporation Method)

  • 노대호;김재수;변동진;이재훈;양재웅;김나리
    • 한국재료학회지
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    • 제15권3호
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    • pp.189-194
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    • 2005
  • [ $SiO_2$ ] nanowires were synthesized using the catalyst evaporation method. Grown nanowires had different shapes by kind of used metal catalyst. Mean diameters of grown $SiO_2$ nanowire were about 30 nm. The kind of catalysts affected microstructure of grown $SiO_2$ nanowire because of its typical growth reactions through the liquid state metal catalysts. Optical property were measured by photoluminescence spectroscopy. Relatively broad peak was obtained and mean peak positioned at 450 nm.