• Title/Summary/Keyword: SEM-EDS analysis

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Effect of polishing solution temperature and times by electro-polishing in dental casting Co-Cr-Mo alloy (치과 주조용 Co-Cr-Mo alloy에서 전해용액 온도와 전해시간에 따른 전해연마의 특성)

  • Jang, Jae-Young;Song, Jae-Sang;Nah, Jung-Sook
    • Journal of Technologic Dentistry
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    • v.34 no.2
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    • pp.145-153
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    • 2012
  • Purpose: The purpose of this study was to investigate to effect of the electro-polishing condition according to electrolyte temperature and current and polishing time on surface morphology and composition by scanning electron microscopy(SEM) and energy dispersive X-ray spectrometer(EDS) in dental casting Co-Cr-Mo alloys. Methods: 16 specimens were divided into 4 groups which have each 4 specimens. The size of specimens were 10mm wide and 5mm height. the electro-polishing of specimens are by polishing solution temperature and times in Co-Cr-Mo alloy by SEM and EDS analysis. Results: The results shows that most smooth surface is obtained when electro-polishing is performed at $49^{\circ}C$ for 30-40sec with electro gap of 10mm and 8 voltage. Conclusion: The morphologies of specimens after electro-polishing were scratch absent and significant between at $40^{\circ}C$ for 45sec and at $49^{\circ}C$ for 45sec.

Effects of Nb5+ Addition on Microstructure and Dielectric Properties of BaTiO3

  • Kim, Yeon Jung;Hyun, June Won
    • Applied Science and Convergence Technology
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    • v.26 no.5
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    • pp.143-147
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    • 2017
  • Structural studies on the addition characteristics of Nb ions to $BaTiO_3$ solid solutions were performed by XRD and SEM/EDS technique. The X-ray diffraction peaks of the (111), (200) and (002) planes of Nb-doped $BaTiO_3$ solid solutions with different mole% of Nb were analyzed. We also investigated the relationship between the dielectric and structural properties of Nb-doped $BaTiO_3$. The transition temperatures of $BaTiO_3$ solid solution doped with 0.5mole%Nb and 1.0 mole%Nb were ${\sim}116^{\circ}C$ and ${\sim}87^{\circ}C$, respectively, which were found to be shifted to very low temperature from the transition temperature of pure $BaTiO_3$ (about $125^{\circ}C$). As a result of analysis of 1/K versus T and ln[$(1/K)-(1/K_m)$ versus ($T-T_m$)] of the two compositions used in this experiment, the diffusivity slightly differs from that of pure $BaTiO_3$ at temperatures above Curie temperature. And this characteristic was analyzed by applying the modified Curie-Weiss law.

Salt Weathering Characteristics and Mechanism Interpretation of the Five-Storied Stone Pagoda in Tapri-ri, Uiseong (의성 탑리리 오층석탑의 염풍화 특성과 메커니즘 해석)

  • Lee, Mi Hey;Lee, Myeong Seong;Lee, Jae Man;Chun, Yu Gun
    • 보존과학연구
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    • s.33
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    • pp.57-67
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    • 2012
  • The Uiseong Tapriri Five-Storied stone pagoda has occurred exfoliation, granular disintegration and discoloration by physical and chemical weathering factors with the major deterioration occurring due to efflorescence by salt. According to the results of SEM-EDS and X-ray diffraction analysis, salts consists of gypsum, taranakite. Artificial salt weathering tests were carried out using the same type of rocks as those in the stone pagoda. The test results showed that efflorescence occurred on the surface of the rock, and that exfoliation and granular disintegration occurred inside the rock due to salt crystallization.

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Strength and Reaction Characteristic of the Hardened Blast Furnace Slag Paste using the Alkali Accelerator (알칼리 자극제를 사용한 고로슬래그 경화체의 반응 및 강도특성)

  • Kim, Yun-Mi;Park, Sun-Gyu;Lee, Sang-Soo;Song, Ha-Young
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2013.05a
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    • pp.313-314
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    • 2013
  • The study carried out the experiment with presenting as the fundamental data for developing non-cement by using red mud generated in blast furnace slag and bauxite generated in the process of manufacturing the pig iron process of manufacturing Al(OH)3/Al2O from as the binding material using the accelerator of NaOH. After fixing the thing and the NaOH adding the blast furnace slag and NaOH 10, 20, 30 (%) with 10, 20, 30 (%) substituted the red mud in the blast furnace slag and the experimental method carried out the experiment. And it measured the flexural strength and compressive strength and took a photograph EDS analysis and SEM. Consequently, the compressive strength was improved as the addition rate of the NaOH was high and the compressive strength according to the replacement ratio of the red mud was degraded. This is determined that film of the blast furnace slag is destroyed and it makes the hydration reaction condition and the intensity is revealed.

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The Analysis of Oxidization Characteristics according to the shapes of RCD contacts (RCD 접점형태에 따른 산화특성 분석)

  • Kim, Dong-Woo;Kim, Hyang-Kon;Gil, Hyoung-Jun;Han, Woon-Kim;Choi, Chung-Seog
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.07a
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    • pp.576-577
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    • 2005
  • In this paper, the oxidization characteristics were analyzed according to the shapes of Residual Current Protective Device(RCD) contacts. RCD is an electrical safety device specially designed to immediately switch the electricity off when electric leakage is detected at a level harmful to a person using electrical equipment. The shapes of RCD contacts are a little bit different according to the models. When RCD is turned on, stationary and moving contact do not fit together. So, it can cause the increase of contact resistance. To discover the deterioration characteristics of RCD contacts by switching repetition, the contacts were analyzed by stereo microscope, Scanning Electron Microscope(SEM) and Energy Dispersive X-ray Spectrometer(EDS).

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Study on Particulate Pollutant Reduction Characteristics of Vegetation Biofilters in Underground Subway Stations (지하역사내 식생바이오필터의 입자상 오염물질 저감특성 연구)

  • Kim, Tae Han;Oh, Ji Eun;Kim, Mi Ju
    • Journal of the Semiconductor & Display Technology
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    • v.21 no.4
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    • pp.99-105
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    • 2022
  • Public attention to the indoor environment of underground subway stations, which is a representative multi-use facility, has been increasing along with the increase in indoor activities. In underground stations, fine iron oxide, which affects the health of users, is generated because of the friction between wheels and rails. Among particulate pollutant reduction technologies, plants have been considered as a non-chemical air purification method, and their effects in reducing certain chemical species have been identified in previous studies. The present study aimed to derive the total quantitative and qualitative reduction effects of a bio-filter system comprising air purifying plants, installed in an underground subway station. The experiment proceeded in two ways. First, PM(particulate matter) reduction effect by vegetation biofilter was monitored with the IAQ(indoor air quality) station. In addition, chemical speciation analysis conducted on the samples collected from the experimental and control areas where plants and irrigation using SEM-EDS(scanning electron microscopy-energy dispersive X-ray spectroscopy). This study confirmed the effect of the vegetation bio-filter system in reducing the accumulation of particulate pollutants and transition and other metals that are harmful to the human body.

Characteristics of Individual Particles for PM2.5 Collected around Busan North Port (부산 북항 주변지역에서 포집된 PM2.5의 개별입자 특성)

  • Hyun, Sangmin;Cheon, Seong-Woo;Kim, Wonnyon;Kang, Nayeon;Park, Jeong-Ho
    • Journal of Environmental Science International
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    • v.31 no.9
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    • pp.781-791
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    • 2022
  • In order to investigate the characteristics of the effects of various emission sources such as ships around the Busan North Port area, PM2.5 samples were analyzed by SEM/EDS (scanning electron microscopy with energy dispersive x-ray spectrometer). In the port city Busan, the main emission source of PM2.5 is ships, and soot was observed as the main exhaust particles of a ship diesel engine. As a result of the individual particle analysis of PM2.5 at the sampling site, carbonaceous particles such as soot and water droplet-shaped, which are considered to be exhausted from ships, were constantly observed. And some spherical Fe-rich particles also appeared.

A Study on the Manufacturing of Lacquer Ware Objects of Nangnang(I) (낙랑칠기(樂浪漆器)의 칠기법(漆技法) 조사(調査)(I))

  • Kim, Kyoungsu;Yu, Heisun;Yi, Yonghee
    • Conservation Science in Museum
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    • v.4
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    • pp.79-88
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    • 2003
  • The lacquer ware objects of Nangnang were treated for conservation and seven of them were studied on the manufacturing technic. When we examined them using microscopes and an SEM-EDS analysis, the lacquer layer was proved to consist of two parts: the ground and the upper lacquer. The ground coating was made of several mixed materials such as powdered bone and minerals. Many forms of powdered bone were observed. We could find out that HgS, PbO and AgS were used as pigments. We could also find out a specific process and materials were used for those objects, although we could not say definitely what they were because the number of the sample was not big enough.