• Title/Summary/Keyword: SEM test

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Ultrasonic evaluation of small surface fatigue cracks initiating in residual stress zone (잔류응력 영역에서 발생한 작은 피로균열의 초음파 평가)

  • Kang Kae-Myung;Kim Jin-Yeon
    • Journal of the Korean Institute of Gas
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    • v.4 no.1 s.9
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    • pp.55-62
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    • 2000
  • A surface acoustic wave method for the evaluation of small fatigue crack initiated from a pit-type surface flaw is presented. In-situ ultrasonic experiments are performed for aluminum 2024-T3 alloy samples under the fatigue test. During the fatigue test, the surface acoustic wave reflection signal from the pit and crack is measured under different hold-stress levels. From the measured and predicted surface wave reflections the depths of fully and partially open cracks are determined and results are verified by comparing with SEM fractography The crack opening behavior of the fatigue crack is evaluated from the predicted effective crack depths. The method developed in this study can be applied to monitor and characterize crack initiation and propagation from pit-type surface flaws in the early stage of fatigue life.

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Apparent digestibility coefficients of animal feed ingredients for olive flounder (Paralichthys olivaceus)

  • Md Mostafizur Rahman;Kang-Woong Kim;Sang-Min Lee
    • Fisheries and Aquatic Sciences
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    • v.25 no.11
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    • pp.537-548
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    • 2022
  • Apparent digestibility coefficients (ADCs) of dry matter, crude protein, crude lipid, nitrogen-free extract, energy and essential amino acids in animal-based feed ingredients were determined for olive flounder (Paralichthys olivaceus). A reference diet (RF) was formulated to contain 1.0% chromic oxide (Cr2O3) as an inert indicator. Nine test diets were formulated to contain RF and one of the feed ingredients (pollock meal [PM], jack mackerel meal [JMM], anchovy meal [AM], cod meal [CM], sardine meal [SM], sand eel meal [SEM], tuna meal [TM], meat meal [MM] and squid liver meal [SLM]) at a 7:3 ratio in each diet designated as PM, JMM, AM, CM, SM, SEM, TM, MM and SLM, respectively. Olive flounder, averaging 150 ± 8.0 g, were stocked at a density of 25 fish per tank in 400-L fiberglass tanks attached with fecal collection columns. Feces were collected from triplicate groups of fish one time a day for four weeks. Dry matter and crude protein ADCs of CM and SEM were significantly higher than the other tested ingredients. Lipid ADCs of JMM, CM and SEM were significantly higher than the other test ingredients. Energy ADCs of CM and SEM were significantly higher than that of the other tested ingredients. The availability of amino acids in CM was generally higher than the other animal protein sources. PM exhibited the lowest amino acid availability among the treatments. Interestingly, MM exhibited significantly higher nutrient digestibility than several marine-based ingredients. However, CM and SEM are seeming to be highly digestible and effective to use in olive flounder diet compared to the other tested ingredients. Overall, the results of this study provide information about the bioavailability of nutrients and energy in animal feedstuffs to apply when formulating cost-effective practical feeds for olive flounder.

Engineering Properties of Volcanic Ash-Cement Soil Mixtures and Zeolite-Cement Soil Mixtures (화산재-시멘트 혼합토 및 제올라이트-시멘트 혼합토의 공학적 특성)

  • Lee, Chung-Won;Chang, Dong-Su;Park, Sung-Yong;Yeon, Kyu-Seok;Kim, Yong-Seong
    • Journal of The Korean Society of Agricultural Engineers
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    • v.55 no.2
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    • pp.65-75
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    • 2013
  • In this study, the engineering characteristics of volcanic ash-cement soil mixtures and zeolite-cement soil mixtures are investigated by using unconfined compression test, freezing-thawing test, SEM and XRD analysis. The samples were mixed with volcanic ash from Mt. Baekdusan or porous zeolite, and cement as the ratios of 3.5:1, 4.0:1, 4.5:1, 5.0:1 with and without metakaolin. It is confirmed that compressive strength degraded with increasing of the amount of volcanic ash or zeolite, and increased with addition of metakaolin as a binder. Moreover, test results suggested that the mixtures provided sufficient freezing-thawing resistance. In addition, ettringite as a product of cement hydration was detected by SEM and XRD, and that possibly contributes to the strength of the mixtures.

The Effect of Interpenetrating Polymer Network upon Tracking Resistance of Epoxy Composite Materials (에폭시 복합재료의 내트래킹성에 미치는 상호침입망목의 효과)

  • 김탁용;이덕진;손인환;김명호;김경환;김재환
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1996.11a
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    • pp.225-229
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    • 1996
  • In this study, in order to develop outdoor insulating materials, SIN(simultaneous interpenetrating polymer network) was introduced to Epoxy resin and the environment resistance was investigated. The single network structure specimen(E series) formed of Epoxy resin alone and simultaneous interpenetrating polymer network specimen (EM series) in which epoxy resin was taken as the first network and methyl methacrylate resin as the second network were manufactured. Ten kinds of specimens were manufacture by filler (SiO$_2$) content. SEM were utilized in order to confirm their network structure changes, and AC voltage dielectric strength was measured. Also, UV-test and tracking test were carried out investigate the environment resistance characteristic. Therefore the variations of network structure were happened as a result of SEM test, and it was confirmed that simultaneous interpenetrating polymer network specimens were more excellent than single network structure specimens.

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Degradation of Composite Insulator as Accelated Aging Test (가속열화 실험에 의한 고분자 애자의 분해)

  • 이용희;장동욱;박영국;박정남;강성화;임기조
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.144-147
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    • 2000
  • The effect of accelerated aging test on ethylene-propylene-diene monomer(EPDM) rubber used for outdoor insulation was studied by X-ray photoelectron spectroscopy(XPS), scanning electron microscope(SEM), FFT spectrum alalysis, and electrical pulse counts using PC by oscilloscope(300 MHz). In electrical alalysis, FFT spectrum analysis indicated arcing caused a significant increase in the third harmonic content of the leakage current of polluted insulator. Also, pulse counts increased as aging time. The surface oxygen and aluminum content were found to increase and that of carbon and nitrogen were found to decrease with time. The detailed XPS analysis indicated that the concentration of carbon in C-C decreased and concentration of highly oxidized carbons increased with time, which was due to the oxidation of EPDM rubber polymer SEM analysis indicated that crack and erosion of EPDM rubber occurred with time.

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A QUANTITATIVE ANALYSIS ABOUT MICROLEAKAGE OF ALL-IN-ONE ADHESIVES (올인원 접착제의 미세누출에 관한 정량적 분석)

  • Kang, Yong-Hee;Shin, Soo-Il;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.29 no.1
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    • pp.66-72
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    • 2004
  • All-in-one adhesives were recently developed for reducing the technique sensitivity and chair time, but lots of concerns were made on bondability, longevity, and microleakage. The object of this study was to evaluate microleakage and marginal quality of all-in-one adhesives using electrochemical method and SEM analysis quantitatively. After making Class V cavities, they were bulk filled with Heliomolar(#A1 after surface treatment with three adhesives: Adper Prompt (Group A), One up bond F (Group O), Xeno III (Group X) Electrical conductivity (microamphere, ${\mu}A$) was checked two times: before and after cavity filling. Percentage of leaky margin was estimated from SEM image (${\times}1,000$). The data were statistically analysed: ANOVA and Paired T test for electrical conductivity, Kruskal-Wallis and Mann-Whitney test for marginal quality, Spearman s rho test for checking of relationships between 2 methods. The result were as follows: 1. There was no difference in microleakage between adhesive systems and every specimen showed some of microleakage after filling. 2. Microleakage was reduced about 70% with composite resin filling. 3. Marginal quality was the best in group A. decreasing among groups in the following order: group O, followed by group X. There were significant differences between group A and group X (p=0.015), and between group 0 and group X (p=0.019). 4. There was no relationship between the microleakage measured by electrochemical method and marginal quality measured by SEM analysis. Within the results of this study, there was no difference in microleakage among groups by electrical conductivity. However, significant difference in marginal quality was seen among groups. It was believed that these dissimilar results might be induced because of their own characteristics. Analysis of microleakage needs various methods for accuracy.

Influence of the Chemical Treatment of Bamboo Fiber (BF) on Physical Properties of BF and PP/BF Composites (대나무 섬유(BF) 및 PP/BF 복합체의 물성에 미치는 BF의 화학적 처리의 영향)

  • Lee, Beom Hee;Jeong, Da Sol;Kim, Cheol Woo;Park, Seong Ho;Kim, Youn Cheol
    • Applied Chemistry for Engineering
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    • v.29 no.2
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    • pp.168-175
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    • 2018
  • In order to investigate the effect of the chemical treatment of bamboo fiber on physical properties of polypropylene (PP)/bamboo fiber (BF) composites, silane coupling agents such as ${\gamma}$-aminopropyltriethoxysilane (APS), ${\gamma}$-glycidoxypropyl-trimethoxysilane (GPS) and ${\gamma}$-mercaptopropyltrimethoxysilane (MRPS) were applied to BF and alkaline treated BF. Morphological properties of the chemically treated BF were confirmed by optical microscope and SEM measurements, and chemical structure changes were confirmed by FT-IR and EDS. TGA results showed that the thermal stability of silane treated BF increased. Based on the analysis of a universal testing machine and an Izod impact test, the flexural and impact properties of PP/silane treated BF composites showed higher values than those of PP/BF composites. The enhancement of interfacial adhesion properties of the PP/BF composite was checked from SEM images of the fracture of specimens after the tensile test.

Physical Properties of Environment-friendly Insulating Composite Materials Using Natural Cellulose as a Core Material (천연섬유질을 심재로 사용한 친환경 복합단열재의 물성)

  • Hwang, Eui-Hwan;Cho, Soung-Jun;Kim, Jin-Man
    • Korean Chemical Engineering Research
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    • v.49 no.1
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    • pp.120-127
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    • 2011
  • For the development of the environment-friendly insulating composite materials, natural cellulose (wood chip and sawdust) was used as a core material and activated Hwangtoh was used as a binder. Various specimens were prepared with the water/binder ratio and natural cellulose/binder ratio. The physical properties of these specimens were then investigated through compressive and flexural strength test, absorption test, hot water resistance test, thermal conductivity, measurement of pore distribution and observation of micro-structures using scanning electron microscope (SEM). Results showed that the absorption ratio increased with the increase of natural cellulose/binder ratio but decreased remarkably with the increase of polymer/binder ratio. The compressive and flexural strength development varied appreciably with the increase of water/binder ratio and natural cellulose/binder ratio. On the other hand, thermal conductivity decreased with the increase of natural cellulose/binder ratio and polymer/binder ratio. Through SEM, it was found that activated Hwangtoh that reacted with water formed a hydrate crystal leading to the compact structure and the total pore volume of the specimen using activated Hwangtoh was smaller than that of the non-activated Hwangtoh.

Test-retest Reliability of Sit-to-Stand and Gait Assessment Using the Wii Balance Board (Wii Balance Board를 이용한 Sit-to-Stand와 보행기능 측정의 검사-재검사 신뢰도)

  • Yang, Seong-rye;Oh, Yu-ri;Jeon, Ye-rim;Park, Dae-sung
    • Physical Therapy Korea
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    • v.23 no.3
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    • pp.40-47
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    • 2016
  • Background: Assessments of Sit-to-Stand (STS) and gait functions are essential procedures in evaluating level of independence for the patients after stroke. In a previous study, we developed the software to analyze center of pressure (COP) in standing position on Wii Balance Board (WBB). Objects: This purpose of this study is to measure test-retest reliability of ground reaction forces, COP and time using WBB on STS and gait in healthy adults. Methods: Fifteen healthy participants performed three trials of STS and gait on WBB. The time (s), vertical peak (%) and COP path-length (cm) were measured on both tasks. Additionally, counter (%), different peak (%), symmetry ratio, COP x-range and COP y-range were analyzed on STS, 1st peak (%), 2nd peak (%) of weight were analyzed on gait. Intra-class correlation coefficient (ICC), standard error measurement (SEM) and smallest real difference (SRD) were analyzed for test-retest reliability. Results: ICC of all variables except COP path-length appeared to .676~.946 on STS, and to .723~.901 on gait. SEM and SRD of all variables excepting COP path-length appeared .227~8.886, .033~24.575 on STS. SEM and SRD excepting COP path-length appeared about .019~3.933, .054~11.879 on gait. Conclusion: WBB is not only cheaper than force plate, but also easier to use clinically. WBB is considered as an adequate equipment for measuring changes of weight bearing during balance, STS and gait test which are normally used for functional assessment in patients with neurological problems and elderly. The further study is needed concurrent validity on neurological patients, elderly patients using force plate and WBB.

A Study on the Website Evaluation Method Using the SEM (구조방정식을 이용한 웹사이트의 인간공학적 평가 방법에 관한 연구)

  • Choe, Jae-Ho;Baek, In-Gi
    • Journal of the Ergonomics Society of Korea
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    • v.22 no.2
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    • pp.45-56
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    • 2003
  • The purpose of this study is to develop the model including multiple causal relationship between factors to evaluate overall user satisfaction and develop an objective method to quantify the impacts and scores of each qualitative factors on overall user satisfaction using Structural Equation Model(SEM) and also test the feasibility to construct a comprehensive website evaluation model including qualitative and quantitative factors. The SEM model used 2 qualitative factors of usability and esthetic factors for the evaluation factors of user satisfaction and select 4 attributes of each factors using factor analysis. 3 shopping mall sites were evaluated to construct the SEM model, and 155 subjects participated the website evaluation using the walk-through and face-to-face survey method. Analysis results showed that the SEM model was statistically significant for all the 3 websites evaluated. Both the usability and esthetic factors showed significant effects to user satisfaction of websites and have positive correlation. The user satisfaction was more effected by the usability factor than esthetic factors, and the simplification and harmonization were the most critical attributes of the usability and esthetic factors.