• Title/Summary/Keyword: SEM evaluation

검색결과 960건 처리시간 0.023초

Calcium Lactate Affects Shelf-life and Firmness of Kimchi

  • Kim, Soon-Dong;Kim, Mee-Hyang;Kim, Mee-Jung
    • 한국식품저장유통학회:학술대회논문집
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    • 한국식품저장유통학회 2003년도 춘계총회 및 제22차 학술발표회
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    • pp.136-136
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    • 2003
  • Calcium lactate has been known extending shelf-life of several lactic acid fermented foods through buffer action with lactic acid and binding of calcium and pectic polysaccharides in the tissue. But, the effects in kimchi during storage and distribution has not been observed. Calcium lactate is tasteless, nontoxic compounds commonly used in a number of food products. Recent observations have indicated the potential usefulness of calcium lactate as food additive which has anticariogenic-, antimicrobial-, anticalculus, anti- carcinogenic effects and enhancement of bone mineral density. In this work we determined the effects of calcium lactate(CaL)-treatment(0, 1, 2 and 3% against salted Chinese cabbage) on the pH, acidity, microbial counts, content of alcohol insoluble substance and calcium texture, color, scanning electron microscopic observation of kimchi tissue and sensory test during storage. pH of CaL treated kimchi were higher(3.78∼3.92) than that of control products(3.58). Total microbe(TM) of CaL treated kimchis were lower but ratio of lactic acid bacteria against TM was higher than those of control products, respectively. Calcium content of treated products were 3-5 times higher than control products. The hardness and crispy taste of treated products were remarkably higher than those of control products evaluated by SEM observation AIS analysis, sensory and textural analysis. Moreover, evaluation on the pH, acidity and sensory test showed the shelf-life of treated kimchi(CaL 2%) to be 25-30 days, which was 13-15 days longer than that of control products.

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블루베리 가루를 첨가한 쌀 파운드케이크의 품질 특성 (Quality Characteristics of Rice Pound Cake prepared with Blueberry Powder)

  • 이원갑;이정애
    • 동아시아식생활학회지
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    • 제23권5호
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    • pp.577-585
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    • 2013
  • This study investigated the physicochemical and sensory characteristics of rice pound cake prepared with various amounts of blueberry powder. The weight of rice pound cakes with additions of 2~8% blueberry powder increased from 418.58 to 420.50 g. The volume and specific loaf volume of rice pound cakes prepared by adding blueberry powder were lower than those of the control. The baking loss rate for the control was 7.72% and that of rice pound cakes prepared by adding blueberry powder decreased by 6.98~6.56%. The moisture contents of rice pound cakes added with blueberry powder were higher than the control. The pH levels for rice pound cakes prepared with blueberry powder ranged between 6.47 and 7.58 and that of the control was 8.11. The microstructural observation by scanning electron microscopy (SEM) showed well developed air cells of control. DPPH radical scavenging activity of the control group was 13.6%, whereas pound cakes prepared by adding blueberry powder ranged from 35.2~78.8%. The "a" value of redness was increased, but L and b value were decreased significantly by additions of blueberry powder. The full textural properties of rice pound cakes were being significantly increased by additions of blueberry powder. Sensory evaluation scores in terms of appearance, flavor, taste, texture and overall preference for pound cakes showed that 4~6% of substituted sample groups were higher than those of others. The results of this study suggest that additions of 4~6% blueberry powder was the best substitution ratio for rice pound cakes.

Nonlinear analysis of reinforced concrete beams strengthened with polymer composites

  • Pendhari, S.S.;Kant, T.;Desai, Y.M.
    • Structural Engineering and Mechanics
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    • 제24권1호
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    • pp.1-18
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    • 2006
  • Strengthening of existing old structures has traditionally been accomplished by using conventional materials and techniques, viz., externally bonded steel plates, steel or concrete jackets, etc. Alternatively, fibre reinforced polymer composite (FRPC) products started being used to overcome problems associated with conventional materials in the mid 1950s because of their favourable engineering properties. Effectiveness of FRPC materials has been demonstrated through extensive experimental research throughout the world in the last two decades. However there is a need to use refined analytical tools to simulate response of strengthened system. In this paper, an attempt has been made to develop a numerical model of strengthened reinforced concrete (RC) beams with FRPC laminates. Material models for RC beams strengthened with FRPC laminates are described and verified through a nonlinear finite element (FE) commercial code, with the help of available experimental data. Three dimensional (3D) FE analysis has been performed by assuming perfect bonding between concrete and FRPC laminate. A parametric study has also been performed to examine effects of various parameters like fibre type, stirrup's spacing, etc. on the strengthening system. Through numerical simulation, it has been shown that it is possible to predict accurately the flexural response of RC beams strengthened with FRPC laminates by selecting an appropriate material constitutive model. Comparisons are made between the available experimental results in literature and FE analysis results obtained by the present investigators using load-deflection and load-strain plots as well as ultimate load of the strengthened beams. Furthermore, evaluation of crack patterns from FE analysis and experimental failure modes are discussed at the end.

삼중수소 저장용기 이종용접부의 수소취화 거동 평가 (II) (Evaluations of Hydrogen Embrittlement Behaviours on Dissimilar Welding Part of SDS Bottles (II))

  • 조경원;최재하;장민혁;이영상;홍태환
    • 한국수소및신에너지학회논문집
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    • 제26권2호
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    • pp.120-126
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    • 2015
  • Recently, the ever-increasing use of fossil fuels for rapid industrial development and population significantly caused an environment pollution and global warming such as climate change. So research and development of sustainable and eco-friendly energy have been performed. Especially the interest in nuclear fusion fuel was significantly increased from the developed countries. The system of fusion energy production was tritium separation, storage and delivery, and purification. Republic of Korea is in charge of Storage and Delivery System (SDS) in the International Thermonuclear Experimental Reactor (ITER). Welding part of the SDS bottles for storing the tritium is known to be susceptible to hydrogen embrittlement. In this study, conducted a study for the relaxation of the stability and hydrogen embrittlement of the weld area. The hydrogen heat treatment was processed through the Pressure-Composition-Temperature (PCT) device according to the time variation. Also mechanical properties such as impact test and hardness test according to using the alkaline cleaning liquid for hydrogen embrittlement relief and the fracture was observed by scanning electron microscopy (SEM) after the mechanical properties evaluation.

삼중수소 저장용기 이종용접부의 수소취화 거동 평가 (I) (Evaluations of Hydrogen Embrittlement Behaviours on Dissimilar Welding Part of SDS Bottles (I))

  • 조경원;최재하;장민혁;이영상;홍태환
    • 한국수소및신에너지학회논문집
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    • 제26권2호
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    • pp.114-119
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    • 2015
  • Nowdays, fossil fuels have been used as an important resource in development of industry. But it is limited and caused climate change such as pollution and global warming. So nuclear fusion research is being issued with tritium to develop eco-friendly and sustainable energy. Republic of Korea is in charge of Storage and Delivery System (SDS) in the International Thermonuclear Experimental Reactor (ITER), weld present in the SDS bottles are easily exposed to the hydrogen embrittlement of special characteristics of the hydrogen in hydrogen atmosphere, When the hydrogen embrittlement is rapidly progresses, the cracking is generated in the weld zone. Due to this cracking, the risk of leakage of tritium into the atmosphere occurs. In this study, hydrogen heat treatment was processed through the Pressure-Composition-Temperature (PCT) device according to the time variation. Also mechanical properties such as rupture strength test, three point bend test and hardness test in accordance with the respective time have been conducted and the fracture was observed by scanning electron microscopy(SEM) after the mechanical properties evaluation.

유비쿼터스 서비스 평가를 위한 u-서비스 체험성의 분석 (The Analysis of U-service Experienceability for Ubiquitous Service Evaluation)

  • 김성후;박창호;김청택
    • 한국조사연구학회지:조사연구
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    • 제7권1호
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    • pp.1-28
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    • 2006
  • IT 산업의 발전과 더불어 사회 및 산업 환경에서 컴퓨터와 컴퓨터 망을 이용한 새로운 환경을 구축하고자 하는 유비쿼터스 혁명이 도래하고 있다. 특히 일반 사용자 측면에서 볼 때 유비쿼터스 환경이 제공하는 양방향적이고 능동적인 지원 서비스는, 기존의 일방향적 서비스와 질적으로 구별되는 새로운 서비스 패러다임이 될 것이며, 따라서 기존의 제품 사용성이나 서비스 체험 양상과는 다른 차원의 서비스 평가 문제를 불러일으킬 것이다. 본 연구는 유비쿼터스 서비스에 대한 여러 차원의 경험을 종합적으로 u-서비스 체험성이라 정의하고, 이 u-서비스 체험성을 평가하는 요인과 문항에 대한 타당화를 위하여, u-서비스에 대한 체험성 모형을 제안하고자 하였다. u-서비스 관련 시나리오와 미리 개발된 서비스 체험 평가문항들을 이용하여, u-서비스 체험성에 대한 요인분석을 실시하였다. 그 결과, 나-중심성, 주권성, 멋, 사용성, 신뢰성, 접속성 등의 6 개의 하위 요인으로 구조화된 유비쿼터스 서비스의 체험성 모형을 확인하였다.

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전기화학적 방법에 의한 주조 스테인리스강 CF8M $\sigma$상 열화평가 (Evaluation of the $\sigma$-Phase Degradation for Cast Stainless Steel CF8M by the Electrochemical Method)

  • 권재도;김중형;박중철;변장환;이우호
    • 대한기계학회논문집A
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    • 제23권11호
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    • pp.2014-2021
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    • 1999
  • The present investigation is concerned with the degradation characteristics of cast stainless steel(CF8M), exposed to the $\sigma$-phase degradation at $700^{\circ}C$. In the present paper, the degradation of CF8 M at $700^{\circ}C$ is evaluated by a non-destructive test, DL-EPR(double loop electrochemical potentiokinetic reactivation). The surface of specimens is observed by using scanning electron microscopy after DL-EPR test. Also. chromium contents of matrix, grain boundary and ferrite phase are analyzed by electron probe X-ray micro analyzer. Through the experiments, the following results are obtained 1) The degree of sensitization(DOS) of CF8M aged up to 15hr at $700^{\circ}C$ is increased with acing time while that is decreased with aging time from 15hr to 150hr. 2) The impact energy decreases with increase of $\sigma$-phase while DOS increases with $\sigma$-phase until aging time reaches to 15hr. After the aging time. 15hr, the $\sigma$-phase and the rate of impact energy with respect to aging time decreases. Therefore the degradation behavior of the CF8M can be evaluated by comparing SEM micrographs and the value of DOS.

탄소나노튜브로 강화된 에폭시 복합재료의 기계적 물성과 열팽창 계수 측정 (Measurement of Mechanical Property and Thermal Expansion Coefficient of Carbon-Nanotube-Reinforced Epoxy Composites)

  • 구민예;김정현;강희용;이교우
    • 대한기계학회논문집A
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    • 제37권5호
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    • pp.657-664
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    • 2013
  • 에폭시 수지에 다중벽 탄소나노튜브를 첨가하여 초음파 처리와 전단혼합 방법으로 분산시켜 다중벽 탄소나노튜브로 강화된 에폭시 복합재료를 제조하였으며, 에폭시 수지 내 다중벽 탄소나노튜브의 분산 적정성을 판단하고 기계적 및 열적 물성을 고찰하였다. 충전재 분산에 대한 평가를 위해 정성적인 방법으로 주사전자현미경(scanning electron microscope, SEM) 이미지를 사용하였고, 정량적인 판단을 위해 인장실험을 실시하였다. 또한, 열적 특성을 평가하기 위해 열팽창계수(coefficient of thermal expansion, CTE)를 측정하였다. 주사전자현미경 사진 및 인장 강도와 영률(Young's modulus)의 작은 편차를 통해서 다중벽 탄소나노튜브가 에폭시 수지 내에 적절히 분산되었음을 확인하였다. 충전재 함량에 따라 인장 강도와 영률이 증가함을 보였고 열팽창계수 측정에서는 열안정성 개선을 고찰하였다.

피로한도 이하에서 발생하는 압입축의 접촉손상 특성 (Characterization of Contact Surface Damage in a Press-fitted Shaft below the Fretting Fatigue Limit)

  • 이동형;권석진;함영삼;유원희
    • 한국정밀공학회지
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    • 제27권8호
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    • pp.42-47
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    • 2010
  • In this paper, the characteristics of contact surface damage due to fretting in a press-fitted shaft below the fretting fatigue limit are proposed by experimental methods. A series of fatigue tests and interrupted fatigue tests of small scale press-fitted specimen were carried out by using rotating bending fatigue test machine. Macroscopic and microscopic characteristics were examined using scanning electron microscope (SEM), optical microscope or profilometer. It is found that fretting fatigue cracks were initiated even under the fretting fatigue limit on the press-fitted shafts by fretting damage. The fatigue cracks of press-fitted shafts were initiated from the edge of contact surface and propagated inward in a semi-elliptical shape. Furthermore, the fretting wear rates at the contact edge are increased rapidly at the initial stage of total fatigue life. After steep increasing, the increase of wear rate is nearly constant under the load condition below the fretting fatigue limit. It is thus suggested that the fretting wear must be considered on the fatigue life evaluation because the fatigue crack nucleation and propagation process is strongly related to the evolution of surface profile by fretting wear in the press-fitted structures.

초음파 감쇠를 이용한 순 티타늄 판재의 용접부 특성 (Characteristics of Welds of Pure Titanium Plate Using Ultrasonic Attenuation)

  • 선상원;이원;박희동;황영탁
    • 비파괴검사학회지
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    • 제33권2호
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    • pp.205-211
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    • 2013
  • 초음파 감쇠를 이용하여 티타늄 용접부에 대해 기계적 특성, 파단면 및 초음파특성을 연구하였다. 준비된 티타늄 시험편은 아르곤 가스를 이용하여 제작하였다. 티타늄 용접 시험편이 파단 되었을 때 변화하는 초음파 신호변화를 확인하기 위해서 인장시험을 실시하였다. 주사전자현미경을 이용하여 파단면을 관찰하고, 4 MHz 수직 탐촉자를 이용하여 초음파 시계열 신호를 획득하였다. 티타늄 판재에서 용접부는 모재부와 열영향부에 비하여 기계적 특성이 떨어지며 파단면분석을 통해 용접부의 입자크기가 모재부보다 큼을 확인할 수 있었다. RMS 신호 처리한 초음파 포락선의 면적과 인장강도의 상관관계를 나타내었다. 따라서 초음파를 이용하여 티타늄 용접부의 건전성 평가 방법이 유용함을 알 수 있었다.