• Title/Summary/Keyword: SEM analysis

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Investigation of Oxidation Sensitivity with Temperature of Steel Plate Type (강판 종별 온도에 따른 산화 민감도 조사)

  • KIM, JUHAN;LEE, KEEMAN
    • Journal of Hydrogen and New Energy
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    • v.30 no.5
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    • pp.455-464
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    • 2019
  • Experiments were conducted to investigate the sensitivity of steel plate oxidation with temperature in a simulated furnace. Used steel plates were a general steel and a high tensile steel. Porous media burner (PM burner) used in model furnace was made for uniform temperature profile. The surrounding temperature was controlled by adjusting the flow rate of the mixture in the combustor. Oxide layer analysis was performed using SEM image analysis and EDS line scanning. Both steel sheets showed a tendency to increase the thickness of the steel sheet surface oxide layer as the temperature increases, and it was confirmed that the flaking phenomenon in surface oxidation layer appeared when the temperature was above a certain temperature.

Availability Analysis of Xilinx 7-Series FPGA against Soft Error (Xilinx 7-Series FPGA의 소프트 에러에 대한 가용성 분석)

  • Ryu, Sang-Moon
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2016.10a
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    • pp.655-658
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    • 2016
  • Xilinx 7-Series FPGA(Field Programmable Gate Array)s mainly used for the implementation of high-performance digital circuit have SRAM-type configuration memory and can malfunction when soft errors occur in their configuration memory. SEM(Soft Error Mitigation Controller) offered by Xilinx helps users mitigate the influence of soft errors in configuration memory. When soft errors occur, SEM Controller can recover the state of FPGA through partial reconfiguration if the soft errors are correctable by ECC(Error Correction Code) and CRC(Cyclic Redundancy Code). This paper presents the availability analysis of Xilinx 7-Series FPGAs against soft errors under the protection of the SEM Controller. Availability functions are derived and compared according to the correction capability of the SEM Controller. The result may help to estimate the reliability of SRAM-based FPGA running in an environment where soft errors may occur.

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Synthesis of Nickel Oxide (NiO) nanoparticles using nickel(II) nitrate hexahydrate as a precursor (Nickel(II) nitrate hexahydrate를 전구체로 사용한 산화니켈(NiO) 나노입자의 합성)

  • Soo-Jong Kim
    • The Journal of the Convergence on Culture Technology
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    • v.9 no.3
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    • pp.593-599
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    • 2023
  • Nickel oxide (NiO) nanoparticles were successfully synthesized by a simple liquid phase process for producing ceramics powder using a precursor impregnated with a nickel(II) nitrate hexahydrate aqueous solution in an industrial pulp. The microfibrile structure of the precursor impregnated with nickel nitrate hexahydrate aqueous solution was confirmed by scanning electron microscope (SEM), and the crystal structure and particle size of nickel oxide (NiO) particles produced as the heat treatment temperature of the precursor were analyzed by X-ray diffraction (XRD) and SEM. As a result, it was confirmed through XRD and SEM analysis that the temperature at which the organic material of the precursor is completely thermally decomposed was 495-500℃, and the size and crystallinity of the nickel oxide particles produced increased as the heat treatment temperature increased. The size of the nickel oxide particles obtained by heat treatment at 500-800℃ for 1 hour was 50-200 nm. It was confirmed by XRD and SEM analysis that a NiO crystal phase was formed at a heat treatment temperature of 380℃, only a single NiO phase existed until 800℃.

Biomedical Applications of Stereoscopy for Three-Dimensional Surface Reconstruction in Scanning Electron Microscopes

  • Kim, Ki Woo
    • Applied Microscopy
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    • v.46 no.2
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    • pp.71-75
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    • 2016
  • The scanning electron microscope (SEM) offers two-dimensional (2D) micrographs of three-dimensional (3D) objects due to its inherent operating mechanisms. To overcome this limitation, other devices have been used for quantitative morphological analysis. Many efforts have been made on the applications of software-based approaches to 3D reconstruction and measurements by SEM. Based on the acquisition of two stereo images, a multi-view technique consists of two parts: (i) geometric calibration and (ii) image matching. Quantitative morphological parameters such as height and depth could be nondestructively measured by SEM combined with special software programs. It is also possible to obtain conventional surface parameters such as roughness and volume of biomedical specimens through 3D SEM surface reconstruction. There is growing evidence that conventional 2D SEM without special electron detectors can be transformed to 3D SEM for quantitative measurements in biomedical research.

Removal of Heavy Metals(Pb, Cr) Using Waste Eggshell

  • Park, Heung-Jai;Bong, Sang-Hun;Jeong, Seong-Ug
    • Proceedings of the Korean Environmental Health Society Conference
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    • 2005.06a
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    • pp.386-393
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    • 2005
  • The calcination characteristic of waste eggshell were examined by thermal gravimetric analysis (TGA), qualitative and quantitative analysis by X-ray fluorescence, and microstructural analysis by scanning electronic microscopy(SEM). The calcined sample was lager grain and pore size.

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An Importance-Performance Analysis(IPA) for Bus Users Travel Time by Using Structural Equation Model(SEM) (구조방정식모형(SEM)을 활용한 버스 이용자의 통행시간 중요도-만족도 분석(IPA))

  • Ahn, Woo-Young;Lee, Sol
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.35 no.3
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    • pp.663-670
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    • 2015
  • In most public transportation related master plans, decisions for investment priorities are initially made by facilities with lower installation rates or lower satisfaction (performance) levels. In general, the decisions are made without conducting importance factor analysis. In this study, a combined method of importance-performance analysis (IPA) model for bus users related in travel time is proposed by using Structural Equation Model (SEM). The results of the IPA for Metropolitan users show that the categories need improvement are number of bus stops, number of intersections, headways, waiting times for boarding and traffic signal operations in order. On the other hand, Non-Metropolitan uses show that the categories need improvement are traffic signal operations, waiting times for boarding, headways, bus exclusive lanes and number of intersections that is in reverse order to Metropolitan users.

The Analysis of Slag Exacavated from Jisa area (지사동 출토 제철슬래그의 금속학적 조사 연구)

  • Park, Sung-Taik;Choi, Chang-Ock
    • Journal of Conservation Science
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    • v.16 s.16
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    • pp.64-76
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    • 2004
  • This study was performed by chemical analysis and metallographic observation. Chemical properties were analized by ICP, XRD and SEM-EDS and slag structures were observed by microscope and SEM. Total Fe amounts in A, C area of slag can be observed $39\~45\%$ by chemical analysis results. It was average of acient times. CaO was $3\~8\%$. It's not plentiful but we think that was artificial. Ti was found in A area a little, and Ti, V were found in C area so much. The compounds, as if Fayalite, Wustite, Magnetite, Ilmenite, Pseudo-brookite, Ulvospinel, Forsterite, Fephroite, Olivine were observed in the result XRD. These structures were also observed in microscope and SEM image. Therefore, The furnance of A area usually used an iron mine, An Iron furnance of C area considered it which refined using a raw iron mine and a raw iron sand.

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