• 한국진공학회지
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• 제1권2호
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• pp.291-297
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• 1992

알루미늄 박막 stripe에 d.c. 전류를 인가하여 electromigration에 의한 결함을 분 석하였다. 6 $\times$ 10-8Torr의 진공동에서 전자빔 증착기를 사용하여 현미경을 유리기판에 $1000AA$의 두께로 알루미늄 박막을 증착하였다. Al/glass 박막의 초기 비저항은 2.7 $\pm$ 0.15($\mu$$\Omega$cm)이였다. 알루미늄 stripe에 electromigration에 의해 양극쪽에 물질 축적영역 (hillocks)과 음극쪽에는 물질 고갈영역(voids)이 형성되었다. SEM, EDAX와 Optical microscope로 hillocks과 voids를 분석하였다. 또한 결함에 대한 SiO2 보호막효과에 대하여 도 분석하였으며, SiO2 보호막에 의하여 Al 박막의 신뢰성은 향상되었다.

• 한국산학기술학회:학술대회논문집
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• 한국산학기술학회 2009년도 추계학술발표논문집
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• pp.663-666
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• 2009

본 논문에서는 폭발법에 의해 합성된 나노다이아몬드의 열분해 및 연소특성에 대해 조사하였다. 나노 다이아몬드의 열분해 및 연소는 열중량 분석장치를 이용하여 측정하였으며, 소성된 나노다이아몬드의 표면 및 결합구조는 XRD, FT-IR, SEM-EDAX를 이용하여 측정하였다. 열분해 조건에서 나노다이아몬드는 $105{\sim}210^{\circ}C$와 $400^{\circ}C$ 부근에서 2중 피크가 나타난다. 또한 연소분위기하에서는 $420^{\circ}C$와 $490^{\circ}C$에서 2중 피크가 나타난다.

• 보존과학회지
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• 제2권2호
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• pp.25-30
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• 1993

Materials (refractory, stone) of iron making furnace excavated from Kalcheon were investigated by the scanning electron microscopy(SEM) with an energy dispersive X-ray analysis (EDAX), X-ray fluorescence(XRF), and X-ray diffraction(XRD). Chemical composition of the refractory materials were $SiO_2(68.74\%),\;Al_2O_3(18.40\%),\;CaO(0.42\%),\;MgO(1.04\%)\;and\;K_2O(2.26\%)$ in weight ratio, which were the typical components presented in common clay. The results of chemical analysis for the stone and the glaze coated, alkali ion(K, Na, Ca) components of the glaze contained high concentration than that the stone. It was suggested that this change had a close relationship with the kinds of fuels used.

• 한국세라믹학회지
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• 제31권6호
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• pp.651-659
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• 1994

BaTiO3 ceramics were sintered on Al2O3, MgAl2O4, MgO and Mg-, Ca-, Y-stabilized zirconia setters. Then the influence of setters on the microstructure of BaTiO3 ceramics and the stability of setters were investigated by SEM, EDAX and XRD analyses. The microstructure of BaTiO3 ceramics sintered on Al2O3, MgAl2O4, MgO and Mg-PSZ showed large grain growth, but little grain growth on Ce-TZP(Tetragonal Zirconia Policrystal). Mg-PSZ(Partially Stabilized Zirconia), Ca-PSZ, Ce-TZP setters showed extensive phase transformation. Y-TZP and fused Y-SZ (Stabilized Zirconia) setters were stable. The liquid sintering aids of BaTiO3 ceramics accelerate mass transport. The reaction of SrTiO3 in BaTiO3 with ZrO2 resulted in the formation of SrZrO3.

• 한국세라믹학회지
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• 제28권2호
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• pp.160-166
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• 1991

Microstructure and phase changes during the sintering of ZnO varistors were studied in ZnO-Bi2O3-CoO-Sb2O3 and ZnO-Bi2O3-CoO-Sb2O3-Cr2O3 systems using acanning electron microscopy (SEM) with an energy dispersive X-ray analysis (EDAX), X-ray diffraction (XRD) and differential thermal analysis (DTA). The spinel phase and the Bi2O3 phase were formed by the decomposition of the pyrochlore phase during heating. The spinel particles (2-4$\mu\textrm{m}$), which were formed both along ther grain boundaries and within the ZnO grain, were always found near the pyrochlore phase. Intergranular phases (Bi2O3 and pyrochlore) were precipitated from the liquid phase during cooling. The Bi2O3 phases were located at the triple (or multiple) point of the ZnO grains. Cr2O3 played a role in decreasing the formation temperature of the spinel phase and Bi2O3 phase during sintering, and inhibited the grain growth.

• 대한치과의사협회지
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• 제22권9호통권184호
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• pp.781-792
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• 1984

The purpose of this experiment was to study the effects of laser on a base metal alloy for dental casting. In this study, microhardness, corrosion resistance, wear resistance, interaction behavior of metal-ceramic interface, and bond strength were tested before and after the laser treatment for metal-ceramic alloy. The conclusion arised from this study are as follows: 1. The hardness of lased area was higher than that of unlased area. 2. The corrosion resistance was higher in lased specimen than in unlased specimen. 3. the wear resistance was higher in Iased specimen than in unlased specimen. 4. The EDAX showed that Mo, Si and Al were increased in lased surface but Ni and Cr not increased. 5. The SEM of lased area revealed a typical microstructure. 6. The bond strength of lased specimen was increased in 11.2% than of unlased specimen.

• 한국레이저가공학회지
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• 제2권1호
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• pp.38-42
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• 1999

As very large scale integration technology has been developed, much more accurate, reliable technology is needed for outer lead bonding. Laser soldering has been researched as an alternative for fine pitch device bonding. This study is focused on how to select optimal laser soldering variables with which solder wets parent material, the microstructural results of laser soldering and the reliability test One of popular packages, QFP100 was soldered successfully with two kinds of solder. The inspection of the joint for reliability was carried out by optical microscope, SEM, EDAX and pull test, which demonstrated the superiority of laser soldering.

• 한국표면공학회지
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• 제21권4호
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• pp.176-182
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• 1988

Effects of Cr, Ni and W on the anodic polarization behavior were investigated for Fe-Cr-Ni-W alloys in deaerated 1N HCI solution. Surface films formed on the polarization were analysed using AES, SEM and EDAX. A higerconcentration of tungten was found in the surface oxide film compared to the matrix. It played an importanet role on incresing the stability of the passive film. The presence of an adequate amount of Cr was essential to increase the pitting resistance of the alloys in acid chloride media. Under 12 wt%cr,alloys containing 6wt%W did not exhidit any passivity at all. The main role of Ni was to control the microstructure rather than to modify the corrosion resistance. In 23 cr-14Ni-^W alloy, the duplex microstructure of ferrite($\delta$-phase) in an austenic matrix was developed. The reson why proferred pitting appeared in austenite and ferrite/austenite interface was that ferrite had more amount of Cr and W than austenite.

• 한국표면공학회지
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• 제45권1호
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• pp.31-36
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• 2012

In order to improve the mechanical roperties of the Gangjin celadon $BaTiO_3$ was added into the raw materials of celadon matrix. Through SEM and XRD analysis the structural changes were observed and the hardness values were measured. We could confirm that the mechanical strength considerably increased in the $BaTiO_3$ added celadon through the measurement of hardness values. The increase of mechanical strength values in the celadon may result from the compositional change in the microstructure such as grain boundary area through EDAX analysis. We might suggest a fundamental idea to improve the mechanical intensity of the celadon.

• 한국분말재료학회지
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• 제1권1호
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• pp.21-26
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• 1994

Aluminum was deposited on aluminum oxide powders using a fluidized bed reactor at atmospheric pressure. The aluminum oxide powders were irregular flakes with acute angles and the average particle size was 26 $\mu\textrm{m}$. The fluidized bed was formed by flowing argon gas at the velocity of 60 cm/sec. The optimal fluidization condition was obtained with the reactor designed to be tapered so that the fluid velocity decreases as the fluidizing gas goes up along the reactor. Aluminum was deposited by flowing TiBA(Triisobutylaluminum) evaporated at$250^{\circ}C$ through the fluidized bed reactor heated to 350~$450^{\circ}C$. The result from the analysis by XRD and EDAX confirmed the coating of aluminum and an SEM micrograph showed the conformality.