• 제목/요약/키워드: SEM/EDS analysis

검색결과 519건 처리시간 0.024초

치과 주조용 Co-Cr-Mo alloy에서 전해용액 온도와 전해시간에 따른 전해연마의 특성 (Effect of polishing solution temperature and times by electro-polishing in dental casting Co-Cr-Mo alloy)

  • 장재영;송재상;나정숙
    • 대한치과기공학회지
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    • 제34권2호
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    • pp.145-153
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    • 2012
  • Purpose: The purpose of this study was to investigate to effect of the electro-polishing condition according to electrolyte temperature and current and polishing time on surface morphology and composition by scanning electron microscopy(SEM) and energy dispersive X-ray spectrometer(EDS) in dental casting Co-Cr-Mo alloys. Methods: 16 specimens were divided into 4 groups which have each 4 specimens. The size of specimens were 10mm wide and 5mm height. the electro-polishing of specimens are by polishing solution temperature and times in Co-Cr-Mo alloy by SEM and EDS analysis. Results: The results shows that most smooth surface is obtained when electro-polishing is performed at $49^{\circ}C$ for 30-40sec with electro gap of 10mm and 8 voltage. Conclusion: The morphologies of specimens after electro-polishing were scratch absent and significant between at $40^{\circ}C$ for 45sec and at $49^{\circ}C$ for 45sec.

Effects of Nb5+ Addition on Microstructure and Dielectric Properties of BaTiO3

  • Kim, Yeon Jung;Hyun, June Won
    • Applied Science and Convergence Technology
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    • 제26권5호
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    • pp.143-147
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    • 2017
  • Structural studies on the addition characteristics of Nb ions to $BaTiO_3$ solid solutions were performed by XRD and SEM/EDS technique. The X-ray diffraction peaks of the (111), (200) and (002) planes of Nb-doped $BaTiO_3$ solid solutions with different mole% of Nb were analyzed. We also investigated the relationship between the dielectric and structural properties of Nb-doped $BaTiO_3$. The transition temperatures of $BaTiO_3$ solid solution doped with 0.5mole%Nb and 1.0 mole%Nb were ${\sim}116^{\circ}C$ and ${\sim}87^{\circ}C$, respectively, which were found to be shifted to very low temperature from the transition temperature of pure $BaTiO_3$ (about $125^{\circ}C$). As a result of analysis of 1/K versus T and ln[$(1/K)-(1/K_m)$ versus ($T-T_m$)] of the two compositions used in this experiment, the diffusivity slightly differs from that of pure $BaTiO_3$ at temperatures above Curie temperature. And this characteristic was analyzed by applying the modified Curie-Weiss law.

의성 탑리리 오층석탑의 염풍화 특성과 메커니즘 해석 (Salt Weathering Characteristics and Mechanism Interpretation of the Five-Storied Stone Pagoda in Tapri-ri, Uiseong)

  • 이미혜;이명성;이재만;전유근
    • 보존과학연구
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    • 통권33호
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    • pp.57-67
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    • 2012
  • 의성 탑리리 오층석탑은 박리박락, 입상분해, 표면변색 등 물리적 및 화학적 훼손이 발생하여 석탑의 표면이 심하게 훼손되어 있으며, 특히 주요 훼손영역에서는 염에 의한 백화현상이 발생하고 있다. 석탑에서 발생한 염의 SEM-EDS 분석 및 X-선 회절분석 결과, 대표적인 염은 석고로 나타났으며, 일부 영역에서 타라나카이트도 확인되었다. 석탑과 동일한 암석을 선택하여 염풍화 실험을 실시한 결과, 암석의 표면은 염 결정 성장과 함께 염에 의한 백화현상이 발생하였으며 내부는 미세균열 및 공극을 따라 염 수용액이 이동하고 결정화되면서 풍화(박리박락, 입상분해)되는 것으로 나타났다.

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알칼리 자극제를 사용한 고로슬래그 경화체의 반응 및 강도특성 (Strength and Reaction Characteristic of the Hardened Blast Furnace Slag Paste using the Alkali Accelerator)

  • 김윤미;박선규;이상수;송하영
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2013년도 춘계 학술논문 발표대회
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    • pp.313-314
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    • 2013
  • The study carried out the experiment with presenting as the fundamental data for developing non-cement by using red mud generated in blast furnace slag and bauxite generated in the process of manufacturing the pig iron process of manufacturing Al(OH)3/Al2O from as the binding material using the accelerator of NaOH. After fixing the thing and the NaOH adding the blast furnace slag and NaOH 10, 20, 30 (%) with 10, 20, 30 (%) substituted the red mud in the blast furnace slag and the experimental method carried out the experiment. And it measured the flexural strength and compressive strength and took a photograph EDS analysis and SEM. Consequently, the compressive strength was improved as the addition rate of the NaOH was high and the compressive strength according to the replacement ratio of the red mud was degraded. This is determined that film of the blast furnace slag is destroyed and it makes the hydration reaction condition and the intensity is revealed.

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RCD 접점형태에 따른 산화특성 분석 (The Analysis of Oxidization Characteristics according to the shapes of RCD contacts)

  • 김동우;김향곤;길형준;한운기;최충석
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.576-577
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    • 2005
  • In this paper, the oxidization characteristics were analyzed according to the shapes of Residual Current Protective Device(RCD) contacts. RCD is an electrical safety device specially designed to immediately switch the electricity off when electric leakage is detected at a level harmful to a person using electrical equipment. The shapes of RCD contacts are a little bit different according to the models. When RCD is turned on, stationary and moving contact do not fit together. So, it can cause the increase of contact resistance. To discover the deterioration characteristics of RCD contacts by switching repetition, the contacts were analyzed by stereo microscope, Scanning Electron Microscope(SEM) and Energy Dispersive X-ray Spectrometer(EDS).

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지하역사내 식생바이오필터의 입자상 오염물질 저감특성 연구 (Study on Particulate Pollutant Reduction Characteristics of Vegetation Biofilters in Underground Subway Stations)

  • 김태한;오지은;김미주
    • 반도체디스플레이기술학회지
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    • 제21권4호
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    • pp.99-105
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    • 2022
  • Public attention to the indoor environment of underground subway stations, which is a representative multi-use facility, has been increasing along with the increase in indoor activities. In underground stations, fine iron oxide, which affects the health of users, is generated because of the friction between wheels and rails. Among particulate pollutant reduction technologies, plants have been considered as a non-chemical air purification method, and their effects in reducing certain chemical species have been identified in previous studies. The present study aimed to derive the total quantitative and qualitative reduction effects of a bio-filter system comprising air purifying plants, installed in an underground subway station. The experiment proceeded in two ways. First, PM(particulate matter) reduction effect by vegetation biofilter was monitored with the IAQ(indoor air quality) station. In addition, chemical speciation analysis conducted on the samples collected from the experimental and control areas where plants and irrigation using SEM-EDS(scanning electron microscopy-energy dispersive X-ray spectroscopy). This study confirmed the effect of the vegetation bio-filter system in reducing the accumulation of particulate pollutants and transition and other metals that are harmful to the human body.

부산 북항 주변지역에서 포집된 PM2.5의 개별입자 특성 (Characteristics of Individual Particles for PM2.5 Collected around Busan North Port)

  • 현상민;천성우;김원년;강나연;박정호
    • 한국환경과학회지
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    • 제31권9호
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    • pp.781-791
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    • 2022
  • In order to investigate the characteristics of the effects of various emission sources such as ships around the Busan North Port area, PM2.5 samples were analyzed by SEM/EDS (scanning electron microscopy with energy dispersive x-ray spectrometer). In the port city Busan, the main emission source of PM2.5 is ships, and soot was observed as the main exhaust particles of a ship diesel engine. As a result of the individual particle analysis of PM2.5 at the sampling site, carbonaceous particles such as soot and water droplet-shaped, which are considered to be exhausted from ships, were constantly observed. And some spherical Fe-rich particles also appeared.

낙랑칠기(樂浪漆器)의 칠기법(漆技法) 조사(調査)(I) (A Study on the Manufacturing of Lacquer Ware Objects of Nangnang(I))

  • 김경수;유혜선;이용희
    • 박물관보존과학
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    • 제4권
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    • pp.79-88
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    • 2003
  • 국립중앙박물관 보존과학실에서 보존처리한 낙랑칠기 7점의 칠기법을 조사하였다. 현미경과 SEM-EDS 등을 사용하여 조사한 결과 칠막은 하지층과 상부 칠층으로 구성되어 있었다. 하지층은 골분(骨粉)과 광물질(鑛物質)등 여러 가지 물질을 섞어 제작하였으며 골분(骨粉)의 여러 형태도 관찰되었다. 안료로 황화수은(HgS), 산화납(PbO), 황화은(AgS)을 사용하였다는 것을 알 수 있었다. 또한 조사대상의 수가 작아 단언할 수는 없지만 제작시 일정한 공정과 재료가 사용된 것을 알 수 있었다.