• Title/Summary/Keyword: Round robin test

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RRT Study for the Quantitative Analysis of Boron in Silicon (실리콘에 도핑된 붕소의 정량분석에 대한 공동분석연구)

  • 김경중;김현경;문대원;홍태은;정칠성;김이경;김재남;임철호;김정호
    • Journal of the Korean Vacuum Society
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    • v.11 no.4
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    • pp.218-224
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    • 2002
  • A domestic round robin test(RRT) for the quantitative analysis of minor impurities was performed by a standard procedure and standard reference material. The certified reference material(CRM)s for B-doped Si thin film and analysis specimens and the analysis specimens were prepared by an ion beam sputter deposition method. These samples were certified by inductively coupled plasma mass spectrometry(ICP-MS) with isotope dilution method which il one of the most quantitative methods in chemical analysis. By using an international standard procedure(ISO/DIS-l4237) for the quantitative analysis of B in Si by SIMS, a domestic RRT was performed for these specimens. Although only a few laboratories participated in this RRT, the average B concentration well agreed with the certified value within 2% error.

Influence of Analysis Models on Variation of Ground Response during Earthquake (지반응답해석기법의 차이에 의한 지반응답 분산도 평가)

  • Kim, Sung-Ryul;Choi, Jae-Soon;Kim, Soo-Il;Park, Dae-Young;Park, Seong-Yong;Kim, Ki-Poong
    • Proceedings of the Korean Geotechical Society Conference
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    • 2007.09a
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    • pp.317-333
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    • 2007
  • The Round-Robin Test (RRT) for ground response analysis was performed by Division of Geotechnical Earthquake Engineering of Korean Geotechnical Society. This research analyzed the influence of analysis methods on variation of ground response by using the results of this RRT. The analysis methods include equivalent linear analysis, non-linear analysis and effective stress analysis. A total of 5 teams among 12 teams applied two kinds of analysis methods. This research compared the results of these 5 teams and analyzed the variation of the results according to analysis methods. The compared results were shear stress-shear strain relation, transfer function, time history and the response spectrum of ground surface acceleration, peak ground acceleration, peak shear strain and maximum excess pore pressure ratio.

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Measurement of Traceability Error for Calibration Service Center Using Type S Thermocouples (S형 열전대를 이용한 교정검사기관의 소급성 오차측정)

  • Gam, Kee-Sool;Kim, Yong-Gyoo;Kim, Sun-Gon
    • Journal of Sensor Science and Technology
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    • v.4 no.1
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    • pp.43-50
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    • 1995
  • We measured the traceability error for nine high temperature calibration service centers including KRISS through the round-robin test. In this test the type S thermocouple, which used as a calibration standard thermometer commonly, was accommodated as a test thermocouple. Intercomparison data of three institutions were coincident with KRISS's data within ${\pm}0.5^{\circ}C$, which was the calibration uncertainty of the type S thermocouple, but the remaining six institution's data were deviated from the assigned uncertainty level. Deviation of the intercomparison data increased gradually according to the increase of the test temperature. and the maximum difference was so large as about $2.0^{\circ}C$ at the highest test temperature, gold point. In this study we found the traceability error of high temperature calibration service center for a high temperature standard was within $2.0^{\circ}C$.

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Variation of Image Analysis Results for Determining the Characteristics of the Air-Void System on Hardened Concrete (콘크리트 공극구조 분석을 위한 화상분석결과의 변동성 분석)

  • Jeon, Sung-Il;An, Ji-Hwan;Lee, Jin-Beom;Kwon, Soo-Ahn
    • International Journal of Highway Engineering
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    • v.13 no.1
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    • pp.157-168
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    • 2011
  • Recently, the cases of freeze-thaw distress on concrete pavement in domestic have been reported periodically. Hereupon, the necessity to establish the standard of spacing factor came to the fore. The test method for analyzing spacing factor is provided in the standard of ASTM C 457. Since researchers tend to judge study results subjectively, the results should be revised throughly. Image analysis program for determining the characteristics of air-void system on hardened concrete identify air void through the difference of a color. The pixel intensity values used in this program have a significant effect on the analysis results. This study compared the automated void count by varying pixel intensity values with the manual void count in order to determine the optimum range of pixel intensity values. Also, this study analyzed the air-void characteristics on eight kinds of concrete mixtures. In this study, it was confirmed that the variation of void counted manually was around 10% from the results of round robin test, and that the optimum range of pixel intensity values is around 80~90. And it was also confirmed that air content (as a whole) was increased generally and spacing factor was decreased by increasing air-entrainer content. But some concrete mixtures showed a tendency that air content was constant and spacing factor was decreased by increasing air-entrainer content. This causes the air entrained by air-entrainer has more influence on spacing factor than air content. Also, the deviation of spacing factor by cutting position of concrete specimen was about 30~100${\mu}m$ because of the limit of 2-D image analysis. The additional study about variation of spacing factor by cutting position of concrete specimen will be performed later.

Models of Reliability Assessment of Ultrasonic Nondestructive Inspection (초음파 비파괴검사의 신뢰도 평가 모델)

  • Park, I.K.;Park, U.S.;Kim, H.M.;Park, Y.W.;Kang, S.C.;Choi, Y.H.;Lee, J.H.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.6
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    • pp.607-611
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    • 2001
  • Ultrasonic inspection system consist of the operator, equipment and procedure. The reliability of results in ultrasonic inspection is affected by its ability. Furthermore, the reliability of nondestructive testing is influenced by the inspection environment, materials and types of defect. Therefore, it is very difficult to estimate the reliability of NDT due to the various factors. In this study, the probability of detection by logistic probability model and Monte Carlo simulation is used for the reliability assessment of ultrasonic inspection. The utility of the NDT reliability assesment is verified by the analysis of the data from round robin test nth these models.

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Quantitative Surface Analysis of Co-Ni and Au-Cu alloys by XPS and SIMS (XPS와 SIMS에 의한 Co-Ni과 Au-Cu 합금표면 정량분석 연구)

  • 김경중;문대원;이광우
    • Journal of the Korean Vacuum Society
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    • v.1 no.1
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    • pp.106-114
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    • 1992
  • Abstract-Quantitative surface analysis of Co-Ni and Au-Cu alloys by XPS and SIMS was studied. For Co-Ni alloy, quantitative XPS analysis could be done within 1-2% relative error with pure element standards without any correction. For Au-Cu, quantitative XPS analysis was not possible without any correction. But it could be done with standard alloys of various composition within 1-2% relative error. Without standard alloys, Au-Cu alloys could be analyzed by XPS within 10% relative error with pure element standards. For SIMS analysis of Co-Ni alloys, the relative secondary ion yields of Co+/Nit has linear relation with ratio of each composition so that quantitative SIMS analysis was possible for Co-Ni alloys. Preliminary results of XPS round robin test of VAMAS-SCA Japan Project are given.

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A Study on the Quality Deviation of High-Strength Concrete from Multiple Ready Mixed Concrete Companies (다수 레미콘사에서 납품된 콘크리트 품질 편차에 관한 연구)

  • Park, Dong-Cheon;Seok, Won-Kyun;Jeon, Hyun-Soo;Kim, Young-Sun
    • Journal of the Korea Institute of Building Construction
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    • v.22 no.6
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    • pp.577-583
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    • 2022
  • On large-scale sites, concrete is often delivered from a number of ready-mixed concrete companies, but even if the same concrete mixture table is used, it is thought that there will be a difference in quality due to differences in materials and manufacturing equipment. Due to a lack of previous research in this area, this study measured the properties of fresh concrete, compressive strength, and chlorine ion diffusion coefficient using the concrete supplied by 12 ready-mixed companies in Busan. The fresh concrete properties met the criteria. The compressive strength increased by 137% for 30MPa, 131% for 45MPa, and 117% for 80MPa by specified compressive strength. For the chlorine ion diffusion coefficient, the average value for each specified compressive strength could be derived without significant variation. The higher the compressive strength, the greater the deviation , and the lower the compressive strength, the greater the deviation in the chlorine ion diffusion coefficient.