• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2005.05a
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• pp.291-294
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• 2005

In this study, we compared and analyzed the floor impact sound insulation performance produced by the rating methods. The rating methods are using reversed A-weighting curve, A-weighted sound pressure levels and arithmetic average. On-site floor impact sound pressure levels of living room and room are measured. The results of this study are 1)the rating using reversed A-weighting curve for heavy-weight impact sound's standard deviation is lower than that of light-weight impact sound, 2)the number of rating using A-weighted sound pressure levels and arithmetic average is larger than that of using reversed A-weighting curve, and 3)the number of rating using reversed A-weighting curve mainly depends on impact sound pressure level of 63Hz in heavy-weight impact sound.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2006.11a
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• pp.612-615
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• 2006

In this study, we compared and analyzed the floor impact noise insulation performance produced by the rating methods. The rating methods are using reversed A-weighting curve, A-weighted sound pressure levels(dB(A)). The results of this study are(1)dB(A) by the specified frequency is 0.5dB(A) at light weight and 2.5dB(A) at heavy weight upper than all pass dB(A)(2)the rating using reversed A-weighting curve is 5dB lower than dB(A)(3)the number of rating using reversed A-weighting curve mainly depends on impact noise pressure level of 63Hz in heavy weight but dB(A) does not.

• Analytical Science and Technology
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• v.31 no.4
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• pp.161-170
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• 2018

The epidemic of disorders associated with synthetic stimulants, such as methamphetamine (MA) and amphetamine (AP), is a health, social, legal, and financial problem. Owing to the high potential of their abuse and addiction, reliable analytical methods are required to detect and identify MA, AP, and their metabolites in biological samples. Thus, a dilute-and-shoot liquid chromatography-tandem mass spectrophotometry (LC-MS/MS) was developed for simultaneous determination of MA, 4-hydroxymethamphetamine (4HMA), AP, and 4-hydroxyamphetamine (4HA) in urine. Urine sample ($100{\mu}L$) was mixed with $50{\mu}L$ of mobile phase consisting of 0.4 % formic acid and methanol and $50{\mu}L$ of working internal-standard solution. Aliquots of $8{\mu}L$ diluted urine was injected into the LC-MS/MS system. For all analytes, chromatographic separation was performed using a C18 reversed-phase column with gradient elution and a total run time of 5 min. The identification and quantification were performed by multiple reaction monitoring (MRM). Linear least-squares regression was conducted to generate a calibration curve, with $1/x^2$ as the weighting factor. The linear ranges were 2.0-200, 1.0-800, and 10-2500 ng/mL for 4HA and 4HMA, AP, and MA, respectively. The inter- and intraday precisions were within 6.6 %, whereas the inter- and intraday accuracies ranged from -14.9 to 11.3 %. The low limits of quantification were 2.0 ng/mL (4HA and 4HMA), 1.0 ng/mL (AP), and 10 ng/mL (MA). The proposed method exhibited satisfactory selectivity, dilution integrity, matrix effect, and stability, which are required for validation. Moreover, the purification efficiency of high-speed centrifugation was clearly higher than 6-15 % for QC samples (n=5), which was higher than that of the membrane-filtration method. The applicability of the proposed method was tested by forensic analysis of urine samples from drug abusers.