• Title/Summary/Keyword: Resin matrix

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MICROLEAKAGE OF POSTERIOR PACKABLE COMPOSITE RESIN hi THE GINGIVAL MARGINS OF CLASS II CAVITIES (제 2급 와동에서 구치부 복합레진의 미세변연누출에 관한 연구)

  • Choi, Su-Jin;Kim, Mi-Ja;Kwon, Hyuk-Choon
    • Restorative Dentistry and Endodontics
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    • v.27 no.3
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    • pp.249-256
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    • 2002
  • The use of flowable composite resins as liners in class II packable composite restoration has been suggested by some manufacturers. However, the contributions of this technique are unproven. The purpose of this study was to compare the gingival microleakage in class II packable composite restorations with or without the use of flowable composite resins as liners. Slot cavities were prepared on both proximals of 80 extracted human molars and randomly assigned to 8 groups of 20 each. The gingival margins were located at 1mm above CEJ in 80 cavities (group1-4) and 1mm below CEJ in 80 cavities (group5-8). The prepared teeth were mounted in the customized tray with adjacent teeth to simulate clinical conditions and metallic matrix band (Sectional matrix) and wooden wedges were applied. After acid etching and application of Single Bond, each group was restored with the following materials using incremental placement technique: Group 1,5 (Filtek P60), group 2, 3, 4 and group 6, 7, 8 (AeliteFlo, TetricFlow, Revolution/ Filtek P60). All specimens were thermocycled 500 times between 5$^{\circ}C$ and 55$^{\circ}C$ with 1 mimute dwell time, immersed 2% methylene blue dye for 24 hours and then rinsed with tab water. The specimens were embedded in clear resin and sectioned longitudinally through the center of restoration with a low speed diamond saw. Dye penetration at gingival margin was viewed at 20 magnification and analyzed on a scale of 0 to 4. Kruscal-Wallis One way analysis and Mann-Whitney Rank sum test were used to analyze the results. The results of this study were as follows. 1. The leakage values seen at the enamel margin were significantly lower than those seen at the dentin margin(P<0.05). 2. On the enamel margin, packable composite resins with flowable liners showed lower leakage than those without flowable liners, but there were no significant differences among the four groups(P>0.05). 3. On the dentin margin, four groups demonstrated moderate to severe leakage, and there were no significant differences in leakage values(P>0.05).

A Study on the Frictio Characteristics of Pitch/CVI and Phenolic Resin/CVI Hybrid Matrix Derived Carbon/Carbon Composites (핏치/CVI계 및 페놀/CVI계를 Matrix로 하는 탄소/탄소 복합재료의 마찰특성 연구)

  • Park, Jong-Gyu;Lee, Jin-Yong
    • Korean Journal of Materials Research
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    • v.6 no.10
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    • pp.986-990
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    • 1996
  • 본 논문에서는 정속마찰 시험기를 사용하여 공기중에서 핏치/CVI계와 페놀/CVI계 낱소/탄소 복합재료의 마찰특성을 평가하고 상호 비교하였다. 운용조건(마찰거리, 마찰속도, 마찰압력)에 관계없이 페놀/CVI계의 평균 마찰계수가 핏치/CVI계 보다 높은 값을 나타내었다. 마찰거리가 4Km이하 일때는 평균 마찰계수가 불안정한 경향을 나타내고 그 이후에서는 안정한 평균 마찰계수 값을 갖는다. 또한 마찰속도와 마찰압력이 증가할수록 평균 마찰계수는 감소하는 경향을 나타내며, 페놀/CVI계의 평균 마찰계수가 핏치/CVI계 보다 높고 마찰면 온도 상승률과 최대 마찰면 온도도 높다. 마찰계수는 마찰면 온도의 영향을 받으며, 마찰속도와 3kg/$\textrm{cm}^2$이하에서 마찰압력이 커질수록 최대 마찰계수를 갖는 마찰면 온도는 높아진다.

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A STUDY ON THE ROUGHNESS OF THE VISIBLE LIGHT CURED COMPOSITE RESINS (가시광선(可視光線) 중합형(重合型) 복합(複合)레진의 표면조도(表面粗度)에 관(關)한 연구(硏究))

  • Lee, Myung-Jong
    • Restorative Dentistry and Endodontics
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    • v.16 no.2
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    • pp.197-212
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    • 1991
  • The purpose of this study was to roughness on the polished surface of visible light composite resins and was to observe the polished surfaces under Scanning Electrom Microscope(ISI DS 130 AKASHI Co. JAPAN). The surface roughness tester(Surfcom 700A Seimtsu profilometer Tokyo, Japan) was used to measure roughness of polished surfaces. In this study, 5 brands of visible of composite resins were examined, Pyrofile light bond Anterior Lite fil anterior Photo clearfil anterior & posterior Palfique light Anterior and posterior Silux Anterior. White point, Silicure point, Super snap Sof-Lex medium disk as cutting instrument, and celluloid matrix were used. The results obtained were as follows. 1. The Celluloid matrix produced the smoothest surfaces. 2. The surfaces made by Soflex medium disk was smoother than the surfaces made by any other polishing instruments. 3. The values of surface roughness made by White point, Silicon point and Super snap were similer. 4. Palfique light (AP) visible light composite resin showed the smoothest surface after polishing with Silicone point, Super snap disk and Soflex mediuem disk in all tested materials.

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Characterization of Polymer and Nano-MMT-composite as Binder of Recycled-Pet Polymer Concrete (폴리머콘크리트의 결합제로서 PET재활용 폴리머와 나노 MMT 복합체의 특성)

  • Jo, Byung-Wan;Park, Seung-Kook
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.05a
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    • pp.292-295
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    • 2004
  • Recently, polymer-clay hybrid materials have received considerable attention from both a fundamental research and application point of view. This organ-inorganic hybrid, which contains a nanoscale dispersion of the layered silicates, is a material with greatly improved thermal and mechanical characteristics. Two classes of nanocomposites were synthesized using an unsaturated polyester resin as the matrix and sodium montmorillonite as well as an organically modified montmorillonite as the reinforcing agents. X -ray diffraction pattern of the composites showed that the interlayer spacing of the modified montmorillonite were exfoliated in polymer matrix. The mechanical properties also supported these findings, since in general, tensile strength, modulus with modified montmorillonite were higher than the corresponding properties of the composites with unmodified montmorillonite. Adding organically modified clay improved the tensile strength of unsaturated polyester by $22\%$ and the tensile modulus of unsaturated polyester was also improved by $34\%$.

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Mechanical Behavior of Fiber Metal Laminates with Local Delamination Defects (국부적 적층분리결함을 갖는 섬유금속적층판의 기계적 거동 특성)

  • Choi, Heungsoap;Choi, Hyungjip;Choi, Wonjong;Ha, Minsu
    • Journal of Aerospace System Engineering
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    • v.1 no.1
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    • pp.25-35
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    • 2007
  • In this paper, the interlaminar crack problems of a fiber metal laminate (FML) under generalized plane deformation are studied using the theory of anisotropic elasticity. The crack is considered to be embedded in the matrix interlaminar region (including adhesive zone and resin rich zone) of the FML. Based on Fourier integral transformation and the stress matrix formulation, the current mixed boundary value problem is reduced to solving a system of Cauchy-type singular integral equations of the 1st kind. Within the theory of linear fracture mechanics, the stress intensity factors are defined on terms of the solutions of integral equations and numerical results are obtained for in-plane normal (mode I) crack surface loading. The effects of location and length of crack in the 3/2 and 2/1 ARALL, GLARE or CARE type FML's on the stress intensity factors are illustrated.

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Temperature Dependent Failure Machanisms of CaCO3 / PP Particulates ($CaCO_3$ / PP 입자 강화 복합재료의 온도변화에 따른 파괴기구)

  • Koh, Sung-Wi;Kim, Hyung-Jin
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.30 no.3
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    • pp.220-226
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    • 1994
  • In this paper the failure mechanisms of polypropylene resin composites filled with calcium carbonate particulates have been studied in the temperature range $-50^{\circ}C$ to $-50^{\circ}C$ The fillers used are both untreated and surface treated with stearic acid. The impact fracture toughness is evaluated from the impact energy absorbed divided by the uncut ligament area of the specimen. Impact fracture toughness increases as temperature is raised whether the fillers are coated or not. The static fracture toughness of these particular composites is evaluated based on the linear clastic fracture toughness of these particular composites is evaluated based on the linear clastic fracture mechanics. Static fracture toughess decreases with increasing temperature whether the fillers are coated or not. An extended stress whitened zone are observed through a large number of availabel sites for cavitation/debonding along particle matrix interface and matrix deformation.

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A Study on the Fracture Toughness of Glass-Carbon Hybrid Composites (유리-탄소 하이브리드 복합재료의 파괴인성에 관한 연구)

  • No, Ho-Seop;Go, Seong-Wi
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.28 no.3
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    • pp.295-305
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    • 1992
  • The critical strain energy release rate and the failure mechanisms of glass-carbon epoxy resin hybrid composites are investigated in the temperature range of the ambient temperature to 8$0^{\circ}C$. The direction of laminates and the volume fraction are [(+45, -45, 0, 0) sub(2) ] sub(s), 50%, respectively. The major failure mechanisms of these composites are studied using the scanning electron microscope for the fracture surface. Results are summarized as follows: 1) The critical strain energy release rate shows a maximum at ambient temperature and it tends to decrease as temperature goes up. 2) The critical strain energy release rate increases as the content of glass increases, and especially shows dramatic increase for the high glass fiber content specimens. 3) Major failure mechanisms can be classfied such as localized shear yielding, fiber-matrix debonding, matrix micro-cracking, and fiber pull-out and/or delamination.

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Flexural behavior of reinforced concrete beams strengthened with a hybrid inorganic matrix - steel fiber retrofit system

  • Papakonstantinou, Christos G.;Katakalos, Konstantinos
    • Structural Engineering and Mechanics
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    • v.31 no.5
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    • pp.567-585
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    • 2009
  • The aim of this study was to investigate the flexural behavior of reinforced concrete beams strengthened with a novel strengthening system. Concrete beams were strengthened with a hybrid retrofit system consisting of high strength steel cords impregnated in an inorganic fireproof matrix (Geopolymer). The strengthened reinforced concrete beams along with non-strengthened control beams were tested monotonically under four point bending loading conditions. Moreover, an analytical model is introduced, that can be used to analyze the flexural performance of the strengthened beams. The experimental results indicate that the failure of the strengthened beams was based on the yielding of the reinforcement in the tension face of the beams, followed by a local slippage of the steel cords. The flexural stiffness of the strengthened beams was significantly improved compared to the stiffness of the non-strengthened beams. In conclusion, the strengthening system can provide an effective alternative to commercially available systems.

Effect of Graphitic Nanofibers on Interfacial Adhesion and Fracture Toughness of Carbon Fibers-reinforced Epoxy Composites

  • Kim, Seong-Hwang;Park, Soo-Jin
    • Composites Research
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    • v.34 no.2
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    • pp.82-87
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    • 2021
  • The mechanical properties of carbon fiber-reinforced epoxy composites (CFRPs) are greatly dependent on the interfacial adhesion between the carbon fibers and the epoxy matrix. Introducing nanomaterial reinforcements into the interface is an effective approach to enhance the interfacial adhesion of CFRPs. The main purpose of this work was to introduce graphitic nanofiber (GNFs) between an epoxy matrix and carbon fibers to enhance interfacial properties. The composites were reinforced with various concentrations of GNFs. For all of the fabricated composites, the optimum GNF content was found to be 0.6 wt%, which enhanced the interlaminar shear strength (ILSS) and fracture toughness (KIC) by 101.9% and 33.2%, respectively, compared with those of neat composites. In particular, we observed a direct linear relationship between ILSS and KIC through surface free energy. The related reinforcing mechanisms were also analyzed and the enhancements in mechanical properties are mainly attributed to the interfacial interlocking effect. Such an effort could accelerate the conversion of composites into high performance materials and provide fundamental understanding toward realizing the theoretical limits of interfacial adhesion and mechanical properties.

Experimental and microstructural evaluation on mechanical properties of sisal fibre reinforced bio-composites

  • Kumar, B. Ravi;Hariharan, S.S.
    • Steel and Composite Structures
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    • v.33 no.2
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    • pp.299-306
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    • 2019
  • The natural fibre composites are termed as bio-composites. They have shown a promising replacement to the current carbon/glass fibre reinforced composites as environmental friendly materials in specific applications. Natural fibre reinforced composites are potential materials for various engineering applications in automobile, railways, building and Aerospace industry. The natural fibre selected to fabricate the composite material is plant-based fibre e.g., sisal fibre. Sisal fibre is a suitable reinforcement for use in composites on account of its low density, high specific strength, and high hardness. Epoxy is a thermosetting polymer which is used as a resin in natural fibre reinforced composites. Hand lay-up technique was used to fabricate the composites by reinforcing sisal fibres into the epoxy matrix. Composites were prepared with the unidirectional alignment of sisal fibres. Test specimens with different fibre orientations were prepared. The fabricated composites were tested for mechanical properties. Impact test, tensile test, flexural test, hardness test, compression test, and thermal test of composites had been conducted to assess its suitability in industrial applications. Scanning electron microscopy (SEM) test revealed the microstructural information of the fractured surface of composites.