• Title/Summary/Keyword: Resin adhesive

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Study on Adhesion and Mechanical Properties of Adhesive Resin Using Microcapsule with Isocyanate Compound (이소시아네이트를 포함하는 Microcapsule을 사용한 접착수지의 특성에 관한 연구)

  • Kim, Dong Ho;Kim, Gu Ni
    • Journal of Adhesion and Interface
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    • v.15 no.3
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    • pp.109-115
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    • 2014
  • In this study, we synthesized and identified microcapsule containing isocyanate, and investigated the mechanical and adhesion properties of polyurethane resin by adding microcapsule. We found out that the core material of microcapsule and the component weight fraction of microcapsule from the FT-IR and TGA analysis. From the results of adhesion and mechanical property tests, we confirmed that in case of using microcapsule for adhesive resin composition, adhesion strength, tensile strength and abrasion were improved by cross-linking reaction between urethane and IPDI in microcapsule.

THE FILM THICKNESS AND RETENTION OF CAST CROWN USING ADHESIVE RESIN CEMENTS (접착성 레진 시멘트를 이용한 주조관의 피막후경과 유지력에 관한 연구)

  • Jung Young-Wan;Cho Hye-Won;Jin Tai-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.30 no.3
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    • pp.437-443
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    • 1992
  • This study was performed to investigate the availability of adhesive resin cement for luting agent of cast crown. The resin cements used in this study were Panavia-Ex(Kuraray Co., Japan) and C & B-Metabond (Parkell Bio-Materials U.S.A.). Zinc phosphate cement was Flecks zinc cement(Mizzy Inc., U.S.A.) The film thickness of cast crown at gingival margin, lateral wall and occlusal surface was observed with measuring microscope(Modek MXT 70 Matsuzawa Seiki Co., Japan) and the retention of cast crown was measured with Instron Universal Test Machine (Instron Engineering Co., U.S.A.) The results were as follows : 1. The value of retention of cast crown was the highest in the use of Panavia-EX, followed by C & B-Metabond and 2inc phosphate cement, respectively. 2. There was no difference in film thickness among the three cements, but the film thickness in all cements was highest at occlusal surface.

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COMPARISON OF MICROTENSILE BOND STRENGTH OF COMPOSITE RESTORATION TO ERODED ENAMEL BY SURFACE TREATMENT (접착제의 종류에 따른 침식치아에 대한 복합레진의 결합강도)

  • Lee, Soon-Young;Lee, Kyung-Ho;Noh, Hong-Seok;Jeong, Tae-Sung;Kim, Shin
    • Journal of the korean academy of Pediatric Dentistry
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    • v.38 no.4
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    • pp.348-354
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    • 2011
  • Composite resin has been widely used for eroded enamel. But, as there have been many reports about the differences in physicochemical characteristics of eroded enamel compared with sound enamel, an additional effort was thought necessary to obtain the optimal bond strength. As a possible answer, we came to think about the application of infiltrant resin which is known to have an excellent penetration capacity into enamel. This study was performed for the purpose of comparing the bond strength of composite restoration with or without infiltrant resin under adhesives on the artificially eroded enamel. 60 extracted sound maxillary primary incisors were selected and divided into group 1, 2, 3 according to the number of artificial erosion cycling for 5 minute duration in 1% citric acid of pH 3.2 at $37^{\circ}C$. And the labial surfaces were divided into 3 areas; group A, only resin adhesive was used, group I, only infiltrant resin, group IA, infiltrant resin followed by resin adhesive. Afterwards, every specimen was restored with composite resin. Microtensile bond strength was measured and failure modes were observed. The obtained results were as follows: 1. In comparing the bond strength by the degree of enamel erosion, it was revealed the highest bond strength in group 1, followed by group 2 and 3, showing the lowest bond strength in most eroded group(p<0.05). 2. In comparing the bond strength by surface treatment methods, group IA and I showed higher value than group A(p<0.05), with unsignificant difference between group I and IA(p>0.05). 3. In observation of failure mode, it was shown higher frequency of cohesive failure in order of 1-2-3 and IA-I-A. Conclusively, it was shown decreasing tendency of bond strength as the enamel is more eroded, and infiltrant resin was thought helpful to replace or add to the resin adhesive for optimal bonding with eroded enamel.

A Study on Physical Properties of Epoxy Adhesives Modified with Polybutadiene Rubber (Polybutadiene 고무 변성 에폭시 접착제의 물성에 관한 연구)

  • Hong, Suk-Pyo;Choi, Sang-Goo
    • Elastomers and Composites
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    • v.26 no.3
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    • pp.193-201
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    • 1991
  • Epoxy resin and CTBN(carboxyl terminated butadiene acrylonitrile) rubber were reacted at $150^{\circ}C$. Epoxy mixtures containing reactant in a ratio $0{\sim}75%(wt%)$ of total liquid component were with dicyandiamide(DICY) at $130{\sim}200^{\circ}C$. Cure, thermal and adhesive properties were investigated in relation to rubber content, cure temperature, hardner content and promoter content. $CTBN{\times}13$ showed better properties in miscibility, curing time and adhesive strength. 2PZ-CNS was more excellent in Tg, and melamine was in adhesive strength. Adhesive strength represented best at rubber content $12{\times}15%$.

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Study on Heat Resistance Anaerobic Adhesive Which Expands When Post Cured

  • Zhai, Haichao;Li, Yinbai;Lin, Xinsong
    • Journal of Adhesion and Interface
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    • v.3 no.1
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    • pp.9-12
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    • 2002
  • In this paper, N,N-m-phenyenedimaleimide (m-PDM), Polyamide Resin (PI) and Metallic dimethacrylate etc. influencing the heat resistance of anaerobic adhesive has been studied, an anaerobic adhesive composition capable of post-cure expansion and $230^{\circ}C$ temperature resistance comprising a multifunctional methacrylate and m-PDM capable of effectuating expansion upon post-cure has been developed. A homogeneous mixture of a monomer and m-PDM are subjected to a first cure heat stage (Room Temperature) wherein a rigid partially-cured plastic is formed and a post-cure heat stage ($150^{\circ}C$) to effectuate permanent expansion of cured adhesive composition.

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The Influence of Resin Mixture Ratio for the Use of Prepreg on the Fatigue Behavior Properties in FRMLs

  • Song, Sam-Hong;Kim, Cheol-Woong
    • International Journal of Precision Engineering and Manufacturing
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    • v.1 no.1
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    • pp.33-41
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    • 2000
  • Fiber reinforced metal laminates(FRMLs) were new type of hybrid materials. FRMLs consist of high strength metals(Al 5052-H34) and laminated fiber with structural adhesive bond. The effect of resin mixture ratios on the fatigue crack propagation behavior and mechanical properties of aramid fiber reinforced aluminum composites was investigated. The epoxy, diglycidylether of bisphenol A(DGEBA), was cured with methylene dianiline(MDA) with or without an accelerator(K-54). Eight kinds of resin mixture ratio were used for the experiment ; five kinds of FRMLs(1)(mixture of epoxy and curing agent) and three kinds of FRMLs(2)mixture of epoxy, curing agent and accelerator). The characteristic of fatigue crack propagation behavior and mechanical properties FRMLs(2) shows more effecting than that of FRMLs(1).

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A Study on Fundamental Performance of Epoxy Resin Mortar Mixed Special Cement for Concrete Surface Control (특수시멘트 혼입 에폭시 수지계 콘크리트용 바탕조정재의 기초물성에 관한연구)

  • 최성민;김용현;황원주;오상근
    • Proceedings of the Korea Concrete Institute Conference
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    • 1998.10c
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    • pp.145-150
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    • 1998
  • This study deals with the effect on performance of epoxy resign mortar mixed special cement for surface control and maintenance of aging concrete construction. The test of main property of epoxy resign in this study are the evaluation on the adhesive strength between substrate and epoxy resign mortar under the environment of wet or concrete substrate surface. We gained the test results of good adhesive strength over 15 kgf/$\textrm{cm}^2$ under the wet and dry condition of concrete surface.

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Study on Tile Waterproof Adhesive Using Geopolymer (지오폴리머를 이용한 타일방수접착제에 관한 연구)

  • Kang, Byeong-Kwen;Chang, Jin-Ho;Chang, Sung-Joo;Bae, Gi-Seon
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.11a
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    • pp.35-36
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    • 2017
  • This study used Geopolymer to study tile waterproofing adhesives. The materials used in this study were polymer and acrylic resin, and were evaluated based on adhesion and water resistance. In particular, the adhesion was evaluated under various conditions, and the substrate was comparatively evaluated on the concrete and tile surface conditions.

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High Efficiency Hybrid Ion Exchange Chemical Filter for Removal of Acidic Harmful Gases (산성유해가스 제거를 위한 고효율 음이온교환 복합 폼 화학필터의 제조)

  • Jung, Youn Seo;Kim, In Sik;Hyeon, Seung Mi;Hwang, Taek Sung
    • Applied Chemistry for Engineering
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    • v.28 no.5
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    • pp.539-546
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    • 2017
  • In this study, an outstanding anion exchange chemical filter was prepared for acidic gas removal. Commercial anion exchange resin was attached to polyurethane (PU) foam by using different types of pressure sensitive adhesive (PSA). The water and chemical resistance and also adhesive elongation were investigated. Also, the behavior of HCl and HF adsorption was evaluated as functions of the initial concentration and flow rate. ATE-701, AT-4000C and HCA-1000 showed 900, 1,500% and 2,400% of the elongation, respectively. It was confirmed that the desorption ratio of HCA-1000 was less than 6% and had excellent durability in water and chemical resistance tests. The adsorption occurred faster as the concentration and flow rate of HCl and HF increased. But 100% adsorption equilibrium occurred after 110 minutes, regardless of the concentration and flow rate. In addition, SEM morphology showed that the adhesive was uniformly dispersed, while the porous structure of the ion exchange resin was maintained, and the chemical filter exhibited excellent durability for the adsorption/desorption process.