• 소성∙가공
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• 제11권7호
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• pp.581-588
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• 2002

Among the processes to produce micro lens, the process using press molding is a new technology to simplify the process, but it contains many unknown variables. The press-molding process proposed in this paper was simplified into two step process, the first step is the pressing to design the preform for glass element, the second step is the annealing to reduce the residual stress. It is important to estimate the amount of shrinkage of glass gob and the residual stress during process. It Is difficult to evaluate the process variables as mentioned above through the experiment. The influences due to process variables was evaluated by using FEM parametric analysis. The results in this paper can be applicable to produce micro lens.

• Corrosion Science and Technology
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• 제20권1호
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• pp.22-25
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• 2021

In the past, Alloy 600 nickel-based alloys have been widely used in steam generators. However, most of them have been replaced by thermally treated alloy 690 tubes in recent years because mill annealed alloy 600 materials are known to be susceptible to stress corrosion cracking. Unlike this general perception, some steam generators using mill annealed alloy 600 tubes show excellent performance even though they are designed, manufactured, and operated in the same way. Therefore, various analyses were carried out to determine causes for the degradation of steam generators. Based on the general stress corrosion cracking mechanism, tube material susceptibility, residual stress, and sludge deposits of steam generators were compared to identify factors affecting stress corrosion cracking. It was found that mill annealed alloy 600 steam generator tubes showed higher resistance to stress corrosion cracking when the amount of sludge deposits on tube surface was smaller and residual stress generated during the fabrication was lower.

• Journal of Oral Medicine and Pain
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• 제23권2호
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• pp.193-209
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• 1998

In identifying bodies that are severely decayed or damaged, methods using fingerprints and various biochemical tests are known to have its limits. To overcome this, forensic odontological method which is based on the analysis of the cranium, tooth and dental restoration is used to enhance the accuracey of individual identification. For this reason, I have come to analysis of the dental materials that exists between the teeth that is perceived to have been previously restored and the one adjacent to it. By analyzing the constituents of gold crown-restored, non-precious metal-restored, gold inlay-restored and amalgam -restored teeth, and adjacent teeth using EDX(energy dispersive X-ray microanalysis) which was invented to analyze very small amount of elements, the nature of the restoration could be predicted and the results obtained were as follows. 1. Some of constitute of gold alloy was extracted from residual cement of gold crown restoration, but that was not extracted from the restored tooth and the one adjacent to it. 2. Some of constituents of non-precious metal alloy was extracted both in the residual cement on the tooth with no-precious metal restoration and in the tooth with the restoration itself. However, none of its constituents were found in the tooth adjacent to it. 3. Some of constituents of gold alloy were found in the residual cement of gold inlay, but they were not found in the restored tooth and the adjacent tooth. 4. Some of constituents of amalgam alloy were found both in tooth restored with amalgam and in the adjacent tooth. From the results obtained above, it is possible to utilize the data obtained from analyizing residual dental materials in a more effective way. This data compensates for the lost data due to any harm done to the restorations prior to individual identification and further enhances the accuracy. Therefore, it could be concluded that this process of analyzing residual dental materials could be beneficial to individual identification in the area of forensic odontoldogy.

• 한국환경농학회지
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• 제39권1호
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• pp.44-49
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• 2020

BACKGROUND: Benzo(a)pyrene is a highly toxic substance which has been listed as a Group I carcinogen by the International Agency for Research on Cancer. There have been numerous studies by researchers worldwide on benzo(a)pyrene. Soxhlet, ultrasound-assisted, and liquid-liquid extractions have been widely used for the analysis of benzo(a)pyrene. However these extraction methods have significant drawbacks, such as long extraction time and large amount of solvent usage. To overcome these disadvantages, we aimed to establish a rapid residual analysis of benzo(a)pyrene content in agricultural products and soil samples. METHODS AND RESULTS: A Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method was used as the pretreatment procedure. For rapid residual analysis of benzo(a)pyrene, a modified QuEChERS method were used, and the best codition was demonstrated after various performing instrument analysis. The extraction efficiency of this method was also compared with Soxhlet extraction, the current benzo(a)pyrene extracting method. Although both methods showed high recovery rates, the rapid residual analysis method markedly reduced both the measurement time and solvent usage by approximately 97% and 96%, respectively. CONCLUSION: Based on these results, we suggest the rapid residual analysis method established through this study, faster and more efficient analysis of residual benzo(a)pyrene in major agricultural products such as rice, green and red chili peppers and also soil samples.

• 콘크리트학회논문집
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• 제17권6호
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• pp.893-902
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• 2005

화재에 노출된 철근콘크리트 구조물의 안정성 판단 및 보강정도를 결정하기 위하여 화해손상을 입은 철근콘크리트 기둥의 잔존거동을 예측하기 위한 합리적 모델이 필요하다 . 화해 손상을 입은 철근콘크리트 기둥의 잔존거동을 예측하기 위한 이론모델 은 기둥 내부에 전달되는 열, 구성 재료의 열화 정도, 그리고 여러 형태의 기둥단면 형상을 고려할 수 있어야 한다. 본 연구에 서 제안한 수치해석 모텔은 이러한 영향인자들을 고려한다. 개발된 모델은 화해를 입은 기둥의 잔존거동을 적절하게 예측하였다. 개발된 모델을 이용하여 피복두께, 화해노출시간, 기둥의 기하학적 형상 등이 철근콘크리트 기둥의 잔존거동에 미치는 영향 에 대하여 변수 고찰하였다. 변수고찰 결과 장기간 화해에 따른 기둥의 잔존내력 감소가 심각하게 나타났으나 기타 변수들의 차이에 따른 잔존거동의 차이는 적은 것으로 나타났다.

• Journal of Welding and Joining
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• 제14권5호
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• pp.95-105
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• 1996

Korea Gas Corporation has operated high pressure gas transmission line of about 600 kilometers and, therefore, a series of repair welding processes are required in order to cope with external defects such as dent, gouge, cracking usually due to mechanical attacks. Most of gas pipelines repair processes are performed after completely venting remaining gas. However, in some case, though it is very unusual, repairs require without venting gas. For instance, this case is that damaged pipeline is remedied with split sleeve by welding. In this paper, in an effort to confirm a safe application of the split sleeve welding, residual stress, strain and temperature distributions are evaluated by computer simulation and experiments. The results obtained are as follows : 1) Computer modelling is supposed to be reasonable because microstructure changes due to welding is simulated coincidently as compare to that of real condition. 2) The maximal temperature on inside surface of pipeline is 50$0^{\circ}C$ for the repair welding process. 3) The amount of residual stress is estimated as the stress corresponding to 0.8% strain. 4) The repair process employed is determined to be technically preferable because of its avoiding cracks and fractures in the course of welding.

• 생약학회지
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• 제35권4호통권139호
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• pp.276-282
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• 2004

This study has been conducted to investigate the amount of residual sulfur dioxide for herbal medicines of 30 species which are purchased in 13 different regions (Bonghwa, Busan, Chunju, Jecheun, Kwangiu, Keumsan, Seoul, Taeku, Cheungdu, Xian, Beijing, Tokyo and Osaka). The sulfur dioxide residues were determined in the collected 386 samples by the modified Monier-Williams method. The residues of sulfur dioxide in 386 samples ranged from ND (under detection limit) to 2808 ppm. The sulfur dioxide in Cassiae Semon, Cinnamomi Ramulus, Cervi Cornu, Hoelen, Crataegi Fructus, Artemisiae Argyi Herba, Scolopendrae Corpus, Schizandrae Fructus and Cyperi Rhizoma were detected under the detection limit regardless of the collected regions. The sulfur dioxide residues in herbal medicines collected in domestic regions were relatively lower than those in foreign regions. There are no standards for sulfur dioxide residual limits of herbal medicines in Korea. This results will provide the scientific basis for the standardization of sulfur dioxide residues in Korea Pharmacopoeia.

• 한국환경과학회지
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• 제16권1호
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• pp.39-44
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• 2007

This study was conducted to investigate the contents of residual solvents and mineral components(11 kinds) in ginseng extracts with different extracting conditions(5 types) and commercial ginseng extract products(domestic, imported). Fine root was extracted with solution having various ethanol concentration after hexane treatment. Among 5 type extracts, residual solvent(hexane) was detected ginseng extracts treated ethanol mixed with hexane. But extracts that dried after soaked in hexane wasn't detected hexane. Mineral components(Al, Mn, Fe, Cu and Zn) were detected in fine root and 5 types of extracts. The contents of mineral components between fine root and extracts with various extracting conditions were similar, however, extracts that dried after soaked in hexane showed the lower amount in Al, Fe, Pb than the others. In comparison with commercial ginseng ex-tract products(domestic, imported), the distribution pattern of mineral was similar but the contents were a little different.

• 한국자동차공학회논문집
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• 제18권2호
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• pp.61-66
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• 2010

A virtual manufacturing system that is composed of JMatPro, a material modeler and $DEFORM^{TM}$-HT, a finite element package is applied to the hot press forming process: high temperature material properties for each phase such as flow stress, elastic modulus, Poisson's ratio, thermal expansion coefficient, in addition to TTT curve are predicted by JMatPro and taken into $DEFORM^{TM}$-HT to predict the material behavior considering phase transformation and heat transfer simultaneously. In order to verify the accuracy of computation, the residual stress and the springback were compared with the experimental measurements. Both the predicted and measured principal residual stresses and amount of springback were in good agreement. It was also found that the residual stresses generated from hot press forming are not negligible as it has been generally assumed, although the springback deformation is quite small.

• 한국산학기술학회논문지
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• 제5권4호
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• pp.282-285
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• 2004

Pt/MoO₃로의 수소 이동 속도론은 소성 온도에 따라 변하는 잔존 Cl량에 의하여 영향을 받았다. 선택적 CO화학흡착 법을 사용하여 소성 온도의 증가에 다른 Pt표면적의 감소를 측정하였다. 50℃등온 실험에서 소성 후에 Cl 량의 빠른 감소 현상을 규명하기 위하여 여러 특성화 분석을 실시하였다. Pt결정 표면에서 잔존 Cl 량의 감소는 MoO₃로의 수소 공급을 증가시켰고, 수소 흡착 속도론을 조절하였다.