• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.11
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• pp.118-123
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• 2017

To manufacture MG-Si (Metallurgical grade silicon) for use in various industries, Acid leaching experiments were performed to remove aluminum (Al) and iron (Fe), which are the most common impurities found in the silicon raw material. The silicon raw material was reacted with five types of acids (HCl, HF, H2SO4, HNO3, H3PO4) at 1, 2, 4, and 6M; 1M HF showed the highest Al and Fe removal rates, 97.9% and 95.2%, respectively. HF, however, resulted in an 18% reduced yield due to the silicon corrosion properties. To minimize the yield reduction, 2M HCl, which has a second removal ratio result, was mixed with 1M HF and applied to the silicon raw material. The experiment was conducted to select the optimal conditions for the mixed solution, which were $80^{\circ}C$ and 2hr. Under the optimal conditions, the residual Al and Fe concentrations were 141 ppmw and 93 ppmw, respectively, and it very easy to produce MG-Si with 3N grade purity.

• Journal of Korean Society of Water and Wastewater
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• v.31 no.6
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• pp.539-549
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• 2017

In water treatment process using microfiltration membranes, manganese is a substance that causes inorganic membrane fouling. As a result of analysis on the operation data taken from I WTP(Water Treatment Plant), it was confirmed that the increase of TMP was very severe during the period of manganese inflow. The membrane fouling fastened the increase of TMP and shortened the service time of filtration or the cleaning cycle. The TMP of the membrane increased to the maximum of $2.13kgf/cm^2$, but it was recovered to the initial level ($0.17kgf/cm^2$) by the 1st acid cleaning step. It was obvious that the main membrane fouling contaminants are due to inorganic substances. As a result of the analysis on the chemical waste, the concentrations of aluminum(146-164 mg/L) and manganese(110-126 mg/L) were very high. It is considered that aluminum was due to the residual unreacted during coagulation step as a pretreatment process. And manganese is thought to be due to the adsorption on the membrane surface as an adsorbate in feed water component during filtration step. For the efficient maintenance of the membrane filtration facilities, optimization of chemical concentration and CIP conditions is very important when finding the abnormal level of influent including foulants such as manganese.

• The Korean Journal of Food And Nutrition
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• v.23 no.1
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• pp.23-29
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• 2010

Pigment concentrates with violet-red color and sweet taste were obtained from purple-fleshed sweet potato(PFSP) using ethyl alcohol and water. Extract from general potato(GP) were used as a control. The relative stability of PFSP pigment concentrate(PFSPPC) in a storage test over 15 days was confirmed in the order of dark > fluorescence > sun-light irradiation. The relative stability of GP pigment concentrate(GPPC) in a storage test over 15 days was confirmed in the order of sun-light > fluorescence > dark storage. The RRP of PFSPPC was higher than that of GPPC, but the color strength of GPPC was 1/2 that of PFSPPC. Treatment of PFSPPC with aluminum potassium sulfate(0.2~0.3%, w/w) best improved its stability. The improved RRPs of PFSPPC were 45.16~47.31% in sun light irradiation, 55.91~60.22% in fluorescence irradiation, and 76.34~75.97% in dark storage conditions. In substituting aluminum potassium sulfate for chitosan, an amount of 0.2~0.3%(w/w) was suitable, giving similar results in improving pigment stability for all concentrates tested. Also, freeze-dried PFSPPC powder was manufactured as a substitute for dextrin, and also as a substitute for chitosan to the extent of 0.25%(w/w). The results of storage stabilite for freeze-dried PFSPPC and GPPC powder over 15 days, irradiation were, PRRs of 74.47~89.36% and 61.54~76.92%, respectively. The stability improving effect of freeze dried PFSPPC powder was confirmed by the results of storage experiments at various conditions. The use of freeze-dried PFSPPC powder was therefore confirmed to be an effective treatment for general foods.

• Proceedings of the International Microelectronics And Packaging Society Conference
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• 2000.04a
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• pp.118-118
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• 2000

New single-source precursor, [AlCI3:NH2tBu] was synthesized for AlN thin f film processing with AICI3 (Aluminum Chloride) and tBuNH2 (tert-butylamine). AlN thin films for packaging aspplication were deposited on sapphire substrate by a atmosph하ie-pressure MOCVD. In most of other study methyl-based AI precursors w were used for source, But herein Aluminum Chloride was used for as AI source i in order to prevent the carbon contamination in the films and stabilize the p precursor. New precursor showed the very high gas vapor pressure so it allowed to m make the film under atmospheric-pressure and get the high purified film. High q quality AlN thin film was obtained at 700 to $900^{\circ}C$. The new precursor was p purified by a sublimation technique and help to fabricate high purity film. It s showed high vapor pressure, which is able to a critieal factor for the high purity a and atmospheric CVD of AlN. High Quality AIN thin film was obtained at $700-900^{\circ}C$. The AIN film was characterized by RBS

• Journal of the Korean Vacuum Society
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• v.9 no.2
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• pp.162-166
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• 2000

High quality $Si_3N_4$ metal-insulator-metal (MIM) capacitors were realized by plasma enhanced chemical vapor deposition (PECVD). Titanium nitride (TiN) adapted as a diffusion barrier reduced the interfacial reaction between $Si_3N_4$ dielectric layer and aluminum metal electrode showing neither hillock nor observable precipitate along the interface. The capacitance and the current-voltage characteristics of the MIM capacitors showed that the minimum thickness of $Si_3N_4$ layer should be limited to 500 $\AA$ under the present process, below which most of the capacitors were electrically shorted resulting in the devastation of on-wafer yield. According to the transmission electron microscopy (TEM) on the cross-sectional microstructure of the capacitors, the dielectric breakdown was caused by slit-like voids formed at the interface between TiN and $Si_3N_4$ layers when the thickness of $Si_3N_4$ layer was less than 500 $\AA$. Based on the calculation of thermally-induced residual stress, the formation of voids was understood from the mechanistic point of view.

• Composites Research
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• v.19 no.4
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• pp.31-38
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• 2006

In this study, effects of curing temperature and autofrettage pressure on a Type 3 cryogenic propellant tank, which is composed of composite hoop/helical layers and a metal liner, were investigated by thermo elastic analysis and composite/aluminum ring specimen tests. Temperature field of a Type 3 tank was obtained from solving the heat transfer problem and, in turn, was used as nodal temperature boundary conditions during the elastic analyses for curing temperature and autofrettage pressure effects. As a result, it was shown that the higher curing temperature was, the more residual compressive stress and tensile stress were induced in composites and metal liner, respectively. On the contrary, autofrettage pressure brought the reduction of these residual thermal stresses caused by cryogenic environments to the tank structure. This tradeoff for curing temperature and autofrettage pressure must be considered in the design and manufacturing stages for a Type 3 cryogenic tank.

• Journal of the Society of Naval Architects of Korea
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• v.38 no.1
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• pp.99-107
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• 2001

Manufacture of fishing vessel is needed the effective material for light, strength, fire and corrosion of water in order to improve durability by high-speed and fishing. These fishing vessel can be divided into FRP and AI alloys fishing vessel. FRP fishing vessel is light and effective for strength but highly ignited and susceptible to heat during the manufacturing ship by-produce noxious component for human. In the case of a scrapped ship, it cause environmental pollution. On the other hand, aluminum is a material in return for FRP and has merit of high-strength and lightness. It's more heat proof and durable than FRP and superior to prevent from corrosion. Al alloys fishing vessel development is rising as an urgent matter. But, al alloy has some defect of bad weldability, welding transformation, cracks and overcost of construction. Therefore this study is to develop the new welding joint shape solving aluminum defects and mechanical behavior. First of all, strength was compared and reviewed by analysis of plate, stiffen plate, new model simplified by using plate theory. On the base of this result, plate and new model of temperature distribution, weld residual stress and strength of tensile, compressive force were compared and reviewed by finite element computer program has been developed to deal with heat conduction and thermal elasto plastic problem. Also, new model is proved application possibility and excellent mechanic by strength comparison is established to tensile testing result.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.1 s.173
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• pp.52-61
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• 2000

The role of quantitative nondestructive evaluation of defects is becoming more important to assure the reliability and the safety of structure, which can eventually be used for residual life evaluation of structure on the basis of fracture mechanics approach. Although ultrasonic technique is one of the most widely used techniques for application of practical field test among the various nondestructive evaluation technique, there are still some problems to be solved in effective extraction and classification of ultrasonic signal from their noisy ultrasonic waveforms. Therefore, crack size determination through a neural network based on the back-propagation algorithm using back-scattered ultrasonic signals is established in this study. For this purpose, aluminum plate containing vertical or inclined surface breaking crack with different crack length was used to receive the back-scattered ultrasonic signals by pulse echo method. Some features extracted from these signals and sizes of cracks were used to train neural network and the neural network's output of the crack size are compared with the true answer.

• Journal of environmental and Sanitary engineering
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• v.10 no.1
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• pp.106-125
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• 1995

Recently, in accordance with elevation of life style and economics, the public demand became increasingly concerned about drinking water quality. Without an adequate supply of safe water, healthy and comfortable life could not exist. Therefore, the purpose of this study is to provide the guidelines and the basic informations to enable supply of clean, tasty and healthy drinking water acceptable for various demands. We analyzed the quality of tap water, mineral water, purified tap water using home tap water purifier. And we researched on the sense of the public complaint over the tap water. We proposed several items relating to the comfortableness of water quality and the target value. Also we presented a case of water supply system for purity and the points at problem The items and target value are as follows 1. turbidity : not more than 1 degree 2. dry residue : $30~200{\;}mg/{\ell}$ 3. hardness : $10~100mg/{\ell}$ 4. free carbon dioxide : not more than $20mg/{\ell}$ 5. $KMnO_{4}$ consumption not more than $3mg/{\ell}$ 6. odor threshold not abnormal 7. residual chlorine : not more than $0.4mg/{\ell}$ 8. water temperature' not more than $20^{\circ}C$ 9. manganese : not more than $0.01mg/{\ell}$ 10. iron : not more than $0.02mg/{\ell}$ 11. aluminum : not more than $0.1mg/{\ell}$

• Journal of the Korean Institute of Gas
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• v.4 no.1 s.9
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• pp.55-62
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• 2000

A surface acoustic wave method for the evaluation of small fatigue crack initiated from a pit-type surface flaw is presented. In-situ ultrasonic experiments are performed for aluminum 2024-T3 alloy samples under the fatigue test. During the fatigue test, the surface acoustic wave reflection signal from the pit and crack is measured under different hold-stress levels. From the measured and predicted surface wave reflections the depths of fully and partially open cracks are determined and results are verified by comparing with SEM fractography The crack opening behavior of the fatigue crack is evaluated from the predicted effective crack depths. The method developed in this study can be applied to monitor and characterize crack initiation and propagation from pit-type surface flaws in the early stage of fatigue life.