• 제목/요약/키워드: Residual Al

검색결과 429건 처리시간 0.03초

Investigation of S-wave Velocity Based on SPS Field Tests (부유형 PS(SPS) 속도검층을 통한 전단파 특성 고찰)

  • Jeong, Nam-Hoon;Lee, Chong-Kyu
    • Journal of the Korean Geotechnical Society
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    • 제24권10호
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    • pp.161-174
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    • 2008
  • To investigate the characteristics of the shear wave velocity of cohesive soils and residual soils in Korea, Standard Penetration Test (SPT), Suspension PS Logging tests (SPS) and other soil tests were performed to analyze the shear wave velocity at each layer For these purposes, 2 study sites are selected: one is cohesive soils and the other is residual soils. As a results, new empirical formulas are proposed from the relationship between strength of the ground (N value) and shear wave velocity from the test data at each layer. In the case of cohesive soils, the proposed relationships are nearly similar to empirical formulas, however, in the case of residual soils there was a little difference between the empirical formulas and measured velocities in this study. Case examples for shear wave velocites are presented with depth, N-values and compared with Ohta et al. (1978) empirical formula.

Characteristics of Heavy Metal Distribution in Surface Sediments from the south Sea of Korea (남해 대륙붕 표층퇴적물 중 중금속 원소의 분포 특성)

  • 조영길;이창복
    • 한국해양학회지
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    • 제29권4호
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    • pp.338-356
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    • 1994
  • Sediment samples from the continental shelf of the South Sea of Korea are analysed to determine the concentration of Al, Fe, Mn, cu, Ni, Zn, Co, Cr and Pb. among these samples, fine-grained sediments were also analysed by a sequential extraction technique to know geochemical forms of the metals in this environments. The total concentration of Al, Fe, Cr, Ni, Cu and Zn in bulk sediments decreased gradually with the increase of distance from the coastal zone. This distribution patterns are well coincide with grain size distribution. However, the patterns of Mn, co and Pb do not follow such and overall distribution. The concentration of Pb, particularly, did not show any features in areal distribution, which may be result from different pathways to the sediments, compared to the other metals. the speculation data show that a considerable amount of Cd, Mn and Co are bounded in the carbonate fraction, accounting for 42.8%, 40.3% and 30.6%, respectively. Cu, Zn, Mn and Fe are largely associated to oxide fraction with proportions of 34.4%, 23.1%, 15.5% and 13.7%, respectively. However, the metals in residual fraction account for more than 50% of the total metal concentration, except for Mn. These observations emphasize that residual fraction in the dominant component controlling the elemental concentration.quartz and glauconite grains.Accordingly,these sediments are interpreted as an extension part of transgressive sand deposit that are widely distributed on the continental shalf floor of southern Yellow Sea.

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Optimization of Crack-Free Polytypoidally Joined Dissimilar Ceramics of Functionally Graded Material (FGM) Using 3-Dimensional Modeling (폴리타이포이드 경사 방식으로 접합 된 이종 세라믹간의 적층 수의 최적화 및 잔류응력 해석에 대한 연구)

  • Ryu, Sae-Hee;Park, Jong-Ha;Lee, Sun-Yong;Lee, Jae-Sung;Lee, Jae-Chul;Ahn, Sung-Hoon;Kim, Dae-Keun;Chae, Jae-Hong;Riu, Do-Hyung
    • Korean Journal of Materials Research
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    • 제18권10호
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    • pp.547-551
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    • 2008
  • Crack-free joining of $Si_3N_4\;and\;Al_2O_3$ using 15 layers has been achieved by a unique approach introducing Sialon polytypoids as a functionally graded materials (FGMs) bonding layer. In the past, hot press sintering of multilayered FGMs with 20 layers of thickness $500{\mu}m$ each has been fabricated successfully. In this study, the number of layers for FGM was reduced to 15 layers from 20 layers for optimization. For fabrication, model was hot pressed at 38 MPa while heating up to $1700^{\circ}$, and it was cooled at $2^{\circ}$/min to minimize residual stress during sintering. Initially, FGM with 15 layers had cracks near 90 wt.% 12H / 10 wt.% $Al_2O_3$ and 90 wt.% 12H/10 wt.% $Si_3N_4$ layers. To solve this problem, FEM (finite element method) program based on the maximum tensile stress theory was applied to design optimized FGM layers of crack free joint. The sample is 3-dimensional cylindrical shape where this has been transformed to 2-dimensional axisymmetric mode. Based on the simulation, crack-free FGM sample was obtained by designing axial, hoop and radial stresses less than tensile strength values across all the layers of FGM. Therefore, we were able to predict and prevent the damage by calculating its thermal stress using its elastic modulus and coefficient of thermal expansion. Such analyses are especially useful for FGM samples where the residual stresses are very difficult to measure experimentally.

High -Rate Laser Ablation For Through-Wafer Via Holes in SiC Substrates and GaN/AlN/SiC Templates

  • Kim, S.;Bang, B.S.;Ren, F.;d'Entremont, J.;Blumenfeld, W.;Cordock, T.;Pearton, S.J.
    • JSTS:Journal of Semiconductor Technology and Science
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    • 제4권3호
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    • pp.217-221
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    • 2004
  • [ $CO_2$ ]laser ablation rates for bulk 4H-SiC substrates and GaN/AIN/SiC templates in the range 229-870 ${\mu}m.min^{-1}$ were obtained for pulse energies of 7.5-30 mJ over diameters of 50·500 ${\mu}m$ with a Q-switched pulse width of ${\sim}30$ nsec and a pulse frequency of 8 Hz. The laser drilling produces much higher etch rates than conventional dry plasma etching (0.2 - 1.3 ${\mu}m/min$) making this an attractive maskless option for creating through-wafer via holes in SiC or GaN/AlN/SiC templates for power metal-semiconductor field effect transistor applications. The via entry can be tapered to facilitate subsequent metallization by control of the laser power and the total residual surface contamination can be minimized in a similar fashion and with a high gas throughput to avoid redeposition. The sidewall roughness is also comparable or better than conventional via holes created by plasma etching.

Thermal Stress Analysis of Functuonally Graded Ceramic/Metal Composites(I)-Plasma Spraying Material- (경사기능성 세라믹/금속 복합재료의 열응력 해석(1)-플라즈마 용사재-)

  • Song, Jun-Hee;Lim, Jae-Kyoo;Chung, Se-Hi
    • Transactions of the Korean Society of Mechanical Engineers A
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    • 제21권3호
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    • pp.439-446
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    • 1997
  • A traditional notion of composites has been composed as a uniform dispersoid, but now it is proposed without regard to such rule with process development. Functionally Graded Material(FGM) consists of a new material design that is to make intentionally irregular dispersion state. In this study, thermal stress analysis of plasma spraying PSZ/NiCrAlY gradient material was conducted theoretically using a finite-element program. A formations of the model are direct bonding material(NFGM) and FGM with PSZ and NiCrAlY component element. The temperature conditions were $700^{\circ}C$ to 1100.deg. C assuming a cooling-down precess up to room temperature. Fracture damage mechanism was analyzed by the parameters of residual stress.

Transparent Ceramics for Visible/IR Windows: Processing, Materials and Characterization

  • Jung, Wook Ki;Ma, Ho Jin;Kim, Ha-Neul;Kim, Do Kyung
    • Korean Journal of Materials Research
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    • 제28권10호
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    • pp.551-563
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    • 2018
  • Visible and IR windows require a combination of high optical transparency and superior thermal and mechanical properties. Materials, fabrication and characterization of transparent ceramics for visible/IR windows are discussed in this review. The transparent polycrystalline $Y_2O_3$, $Y_2O_3-MgO$ nanocomposites and $MgAl_2O_4$ spinel ceramics are fabricated by advanced ceramic processing and the use of special sintering technologies. Ceramic processing conditions for achieveing fully densified transparent ceramics are strongly dependent on the initial powder characteristics. In addition, appropriate use of sintering technologies, including vacuum sintering, hot-pressing and spark plasama sintering methods, results in outstanding thermal and mechanical properties as well as high optical transparency of the final products. Specifically, the elimination of light scattering factors, including residual pores, second phases and grain boundaries, is a key technique for improving the characteristics of the transparent ceramics. This paper discusses the current research issues related to synthesis methods and sintering processes for yttria-based transparent ceramics and $MgAl_2O_4$ spinel.

Analysis of the Esterification Process for Poly(ethylene terephthalate)

  • Ahn, Young-Cheol;Park, Soo-Myung
    • Macromolecular Research
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    • 제11권6호
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    • pp.399-409
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    • 2003
  • The first esterification reactor in the continuous polymerization of poly(ethylene terephthalate) has been analyzed by solving the material balances for the two-phase system with respect to the solubility of terephthalic acid. The Newton-Raphson method was used to solve the material balance equations instead of the Simplex method that is frequently used for finding a minimum point of a residual rather than a solution of an equation. A solution for the material balance equations, with the constraint of non-zero liquid phase fraction, could not be obtained with the solubility data of Yamada et al., but could be obtained with solubilities over a minimum value that is larger than their data. Thus, the solubility data of Yamada et al. are considered to be too small. On the other hand, the solubility data of Baranova and Kremer are so large that they gave a solution with the liquid phase only. Based on our results, several typical solubility curves satisfying the constraint of a non-zero liquid phase fraction are suggested in this study; we studied the reaction characteristics of the system using these curves. A higher temperature and a lower pressure are preferred for reducing the content of diethylene glycol.

Characteristics of Piezoelectric Microspeakers according to the Material Properties (물성변화에 따른 압전형 마이크로스피커의 특성)

  • Jeong, Kyong-Shik;Cho, Hee-Chan;Yi, Seung-Hwan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • 제21권6호
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    • pp.556-561
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    • 2008
  • This paper reports the characteristics of piezoelectric microspeakers that are audible in open air with high quality piezoelectric AlN thin film according to the materials properties. When we use a tensile-stressed silicon nitride diaphragm as a supporting layer, the Sound Pressure Level (SPL) is relatively small and constant at low frequency region and shows about 70 dB at 10 kHz. However, in case of a compressively stressed composite diaphragm, the SPL of the fabricated microspeakers shows higher output pressure than those of a tensile-stressed diaphragm. It produces more than 66 dB from 100 Hz to 15 kHz and the highest SPL is about 100 dB at 9.3 kHz with $20V_{peak-to-peak}$, sinusoidal input biases and at 10 mm distances from the fabricated microspeakers to the reference microphone. From the experimental results, it is superior to have a compressively composite diaphragm in order to produce a high SPL in piezoelectric microspeaker.

The Assessment of Ceramic Wear by the Parameter Scf (Scf 파라메타에 의한 세라믹 마멸 평가)

  • 김상우;김석삼
    • Tribology and Lubricants
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    • 제12권1호
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    • pp.56-65
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    • 1996
  • The result of wear test for ceramic materials was assessed by Scf parameter to verify the usefulness of the proposed Scf parameter. Friction and wear tests were carried out with ball on disk type. The materials used in this study were HIPed Alumina $(Al_2O_3)$, Silicon carbide (sic), Silicon nitride $(Si_3N_4)$ and Zirconia $(ZrO_2)$. The tests were carried out at room temperature with self mated couples of ceramic materials under lubricated condition. Turbine oil was used as a lubricant. In this test, increasing the load, specific wear rates and wear coefficients of four kinds of ceramic materials had a tendency to increase. The wear coefficients of ceramic materials were in order of $Al_2O_3, SiC, Si_3N_4, ZrO_2$. Worn surfaces investigated by SEM had residual surface cracks and wear particles caused by brittle fracture. As the fracture toughness of ceramic materials was higher, wear resistance more increased. The roughness of worn surface had correlation with wear rate. The wear rate(W$_{s}$) and Scf parameter showed linear relationship in log-log coordinates and the wear equation was given as $W_s = 5.52 $\times$ Scf^{5.01}$.

The Effect of Pre-chlorination on the Coagulation of Microcystis aeruginosa (전염소처리가 Microcystis aeruginosa 응집에 미치는 영향)

  • Lee, Tae-Gwan;Jin, Jung-Sook
    • Journal of Korean Society of Environmental Engineers
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    • 제22권3호
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    • pp.505-510
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    • 2000
  • In this study the effects of pre-chlorination on the coagulation of water which contain Microcystis aeruginosa. were investigated on the laboratory scale. We prepared the sample of $10^5cell/mL$ Microcystis aeruginosa and then applied 0.2, 1.0, 10 mg-Cl/L chlorine on the sample After reaction period(1 minute and 1 hour), each sample was coagulated. As a result, after 0.4 mg-Al/L coagulant dose, turbidities of all samples were below 2 mg-Kaolin/L. Turbidity was not affected by chlorine dose. As the dose of chlorine was increased, the residual aluminum was decreased, but result of $UV_{254}$ was adverse.

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