• Title/Summary/Keyword: Reference Standards

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Proficiency testing of cadmium and lead in polypropylene resin (폴리프로필렌 수지 중 카드뮴과 납 측정 숙련도시험)

  • Cho, K.H.;Lim, M.C.;Min, H.S.;Han, M.S.;Song, H.J.;Park, C.J.
    • Analytical Science and Technology
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    • v.20 no.3
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    • pp.183-192
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    • 2007
  • The various environmental regulation directives such as RoHS (restriction of hazardous substances in electrical and electronic products) and WEEE (waste from electrical and electronic equipments) are practically used as the technical barrier in international trade (TBT) of vehicles and electrical and electronic products recently. Regarding such an environmental regulation, Korea Research Institute of Standards Science (KRISS) organized a proficiency testing scheme to establish the reliability of measurement results produced by the relevant research institutes and test laboratories in Korea. Participants were 31 laboratories related to production of the electrical and electronic equipments and mobile vehicles. Two polypropylene samples of pellet type were employed as the proficiency testing materials (PTMs). Cadmium and lead were the analytes chosen among six components regulated in European Union (EU) RoHS directive. The PTMs were sent to the participants by post on September $1^{st}$ 2006, and deadline for results submission were October $10^{th}$ 2006. The results of each laboratory were evaluated in comparison with KRISS reference values using Robustic Z-score and Youden plot methods. The results of the various sample digestion methods were also compared. Most of participants reported good agreement within 10 % range of reference values. However, results from several laboratories showed significant biases from reference values. These laboratories should establish the quality assurance system for improvement of the measurement reliability.

Development of nitrogen and oxygen certified reference materials in 10 μmol/mol for the purity evaluation

  • Ahn, Byung Soo;Moon, Dong Min;Lee, Jin Bok;Kim, Jin Seog;Lee, Jin-Hong;Hong, Kiryong
    • Analytical Science and Technology
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    • v.33 no.2
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    • pp.68-75
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    • 2020
  • We have developed 10 μmol/mol nitrogen and oxygen certified reference materials (CRMs) in helium, as a SI-traceable gas standard for a quantifying of impurities in pure gases for the first time in Korea. The standard gas mixtures of nitrogen and oxygen were prepared in 5000 μmol/mol and sequentially were diluted to 250 μmol/mol and 10 μmol/mol according to the gravimetric preparation. In each dilution step, two cylinders of CRMs were prepared. The verification of internal consistency among the prepared gas mixtures was performed by using GC-TCD. The amount fractions and those expanded uncertainties (k = 2) of nitrogen and oxygen in the standard gas mixtures were (10.12 ± 0.08) μmol/mol and (10.18 ± 0.08) μmol/mol for nitrogen, and (9.88 ± 0.06) μmol/mol and (9.94 ± 0.06) μmol/mol for oxygen, respectively. We have conducted a purity assessment of two commercial helium gases using developed CRMs. As the results of the purity assessment, nitrogen and oxygen were detected by (1.66 ± 0.03) μmol/mol and (0.31 ± 0.02) μmol/mol, respectively, as the impurities in one of the pure helium.

A Study on the Establishment of Evaluation Indicator Standards on Development Stages of Rural Village (농촌마을 발전단계별 평가지표 기준 설정 연구)

  • Kim, Young-Taek;Choi, Soo-Myung;Cho, Eun-Jung;Yoon, Chi Wook;Im, Sang-Bong
    • Journal of Korean Society of Rural Planning
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    • v.20 no.3
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    • pp.131-141
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    • 2014
  • This study aimed at setting up the grading indicator standards on development stages for phasing the continuous development process. To achieve the objective of this study, after referring to the proposed cases derived from the reference analysis, the development stages were classified. Also grading criteria of indicators according to development stages were established through the statistical analysis and expert group checking. Development stages of rural village were stepped into 4-stages through the reviews and analysis of reference literature ; preparation-entry-development-advanced stage. Reasonable achievement level of each development stage was established by considering the necessary development period and benchmarking reference target together. On the basis of these clear stepwise development phases, the grading criteria were proposed for determination of the incumbent development stages.

The correlation of blood pressure with height and weight in Korean adolescents aged 10-19 years; The Korean National Health and Nutrition Examination Surveys (2009-2011)

  • Song, Young-Hwan
    • Clinical and Experimental Pediatrics
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    • v.57 no.1
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    • pp.35-40
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    • 2014
  • Purpose: Height-specific blood pressure (BP) is the standard parameter used to diagnose childhood hypertension. However, there has been some argument that weight may be a better variable than height in the reference BP standards. Therefore, before assessing the BP status using the reference BP standards, a basic understanding of the fundamental association of weight and height with BP is required. Methods: In the present study, we analyzed the correlation of BP with height and weight in Korean adolescents (age, 10-19 years), using data from the Korean National Health and Nutrition Examination Surveys (2009-2011). Results: Systolic BP (SBP) was more closely correlated with weight than with height in the normal weight (body mass index [BMI], ${\leq}85th$ percentile) and overweight (BMI, >85th percentile) groups and in the normal waist circumference (WC, ${\leq}90th$ percentile) and high WC (>90th percentile) groups in both sexes. Diastolic BP (DBP) had a higher correlation with height than with weight in the normal weight and normal WC groups, whereas weight was more closely associated with DBP than height in the overweight and high WC groups in both boys and girls. Conclusion: In Korean adolescents, weight had a greater effect on SBP than height in both the normal weight and overweight groups. DBP was mainly affected by height in the normal weight group, whereas weight was the major determinant of DBP in the overweight group. Therefore, it may be necessary to consider weight in the establishment of reference BP standards.

Electrical Power and Energy Reference Measurement System with Asynchronous Sampling (비동기 샘플링에 의한 전력과 에너지 측정 기준시스템)

  • Wijesinghe, W.M.S.;Park, Young-Tae
    • Proceedings of the KIEE Conference
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    • 2009.07a
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    • pp.684_685
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    • 2009
  • A digital sampling algorithm that uses a two high resolution integrating Voltmeters which are synchronized by Phase Lock Loop (PLL) time clock for accurately measuring the parameters, active and reactive power, for sinusoidal power measurements is presented. The PLL technique provides high precision measurements, root mean square (rms), phase and complex voltage ratio, of the AC signal. The system has been designed to be used at the Korean Research Institute of Standards and Science (KRISS) as a reference power standard for electrical power calibrations. The test results have shown that the accuracy of the measurements is better than $10 {\mu}W/VA$ and the level of uncertainty is valid for the power factor range zero to 1 for both lead and lag conditions. The system is fully automated and allows power measurements and calibration of high precision wattmeters and power calibrators at the main power frequencies 50 and 60 Hz.

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Measurement of the Reverberation Time of Rooms with Reference to Other Acoustical Parameters (실의 잔향시간 측정방법 고찰)

  • 오양기;주진수;정광용;김선우
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2001.05a
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    • pp.230-233
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    • 2001
  • Revision of KS, Korean Standards, is currently actively discussed. It is just the time for a new world class standards under the new system with WTO, World Trade Organization. This paper is a part of "Researches on the Standards in the Building Acoustic Field", as one of KS revision projects. The aim of this study is to define the requirements for measuring the reverberation time of rooms with reference to other acoustical parameters. In the former KS, there is no items matched with this purpose. Therefore measuring reverberation time and other room acoustical parameters with confidential test procedure was impossible. On these basis, a new part of KS is proposed, and some problems remained and further discussions in the proposed draft are described in this study.

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Precise Impedance Measurement of Coaxial Loads using Air Line Impedance Standards (Air Line 임피던스 표준을 이용한 동축형 부하의 임피던스 정밀 측정)

  • 강진섭;김정환
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.11 no.5
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    • pp.788-795
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    • 2000
  • In this paper, a method for the precise impedance measurement of coaxial loads using an offset open and short as the reflection standards and reference air lines with different lengths as the impedance standards is proposed. Measured input impedances of power sensors and thermistor mounts obtained from SWR bridges(5~400MHz) and a vector network analyzer(100~1,000MHz) are presented in the frequency range of 5MHz to 1,000 MHz.

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Development of a Mushroom Powder Certified Reference Material for Element Analysis

  • Betru, Tegegn Gizachew;Yim, Yong-Hyeon;Lee, Kyoung-Seok
    • Mass Spectrometry Letters
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    • v.11 no.4
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    • pp.108-112
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    • 2020
  • A certified reference material (CRM) for the analysis of nutrient elements in an edible mushroom (Ganoderma lyceum) powder has been developed (KRISS CRM 108-10-011). The mass fractions of calcium (Ca), iron (Fe), and zinc (Zn) were measured by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). To dissolve the fungi cell wall of mushroom consisted of chitin fibers, sample preparation method by single reaction chamber type microwave-assisted acid digestion with acid mixtures was optimized. The mean measurement results obtained from 12 sample bottles were used to assign as the certified values for the CRM and the between-bottle homogeneities were evaluated from the relative standard deviations. The certified values were metrologically traceable to the definition of the kilogram in the International System of Units (SI). This CRM is expected to be used for validation of analytical methods or quality control of measurement results in analytical laboratories when they determine the mass fractions of elements in mushroom or other similar samples.

A Standard Reference Model for Semantic Interoperability in Cloud Computing (클라우드 컴퓨팅에서의 의미 상호운용성을 위한 표준 참조 모델)

  • Jeong, Dong-Won
    • Journal of the Korea Society of Computer and Information
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    • v.17 no.8
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    • pp.71-80
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    • 2012
  • Much research has been recently accomplished for standardization in cloud computing. However, little research on standardization of data sharing and exchanging has been studied. Most of all, the corresponding standardization organization suggests no specific standardization items and reference model. This paper defines the current standardization problems and proposes a set of specific standardization items and a reference model for supporting the semantic interoperability. To achieve the goal of this paper, the overall standardization trend in cloud computing is first analyzed. Especially, this paper describes the status of standard development for addressing the semantic interoperability of data. This paper also defines the potential standardization items based on the concepts of standards in the data exchanging and management field, which are used for developing standards in various fields. Finally, the reference model is describe to show the relationships between items and overall semantic interoperability process. This paper can be used as a guideline for development of standards and also can facilitate standardization of cloud computing.

Meteorological basis for wind loads calculation in Croatia

  • Bajic, Alica;Peros, Bernardin
    • Wind and Structures
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    • v.8 no.6
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    • pp.389-406
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    • 2005
  • The results of reference wind speed calculation in Croatia as a base for the revision of the Croatian standards for wind loads upon structures are presented. Wind speed averaged over 10 minutes, at 10 m height, in a flat, open terrain, with a 50-year mean return period is given for 27 meteorological stations in Croatia. It is shown that the greatest part of Croatia is covered with expected reference wind speeds up to 25 m/s. Exceptions are stations with specific anemometer location open to the bura wind which is accelerated due to the channelling effects of local orography and the nearby mountain passes where the expected reference wind speed ranges between 38 m/s and 55 m/s. The methodology for unifying all available information from wind measurements regardless of the averaging period is discussed by analysing wind speed variability at the meteorological station in Hvar.