• Transactions of Materials Processing
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• v.13 no.4
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• pp.365-373
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• 2004

The sheet formability of single AA5182 sheets and sandwich sheets comprising of AA5182/polypropylene/AA5182 (AA/PP/AA) was studied. Rolling without lubrication and subsequent recrystallization annealing led to the formation of favorable ｛111｝//ND fiber textures in AA5182 sheets, which provided a higher plastic strain ratio of $R_m=1.5$. $R_m$ value of 1.58 was obtained in the AA/PP/Ah sandwich sheet sample. Furthermore, a proper combination of the sample direction of the upper and lower skin sheet gave rise to an optimization of the sheet formability of the sandwich sheets.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.53-56
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• 2004

The mechanical properties and optical micrographs are studied for rolled magnesium alloy sheet with hexagonal close packed structure(HCP) at room and elevated temperatures. Tensile properties such as tensile strength, elongation, R-value and n-value are also measured for AZ31 magnesium alloy. Magnesium with strong texture of basal plane parallel to the rolling direction usually has high R-value and plastic anisotropy at room temperature. As temperature increases, the R-value for AZ31 magnesium sheet decreases. In addition, the AZ31 sheet becomes isotropy and recrystallization above $200^{\circ}C$. Formability of magnesium alloy sheets remarkably poor at room temperature is improved by increasing temperature. Sheet forming of magnesium alloy is practically possible only at high temperature range where plastic anisotropy disappears.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.228-230
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• 2004

Samples of the aluminum alloy 3103 sheets were repeatedly deformed by ECAR up to twelve passes. Shear textures developed after the first passage of ECAR. However, the intensity of shear texture components decreased with increasing number of ECAR passages. Observations by TEM and EBSD revealed that the degree of misorientations within the deformed grains increased with increasing number of ECAR passes. Changes in textures and microstructures were hardly observed during recrystallization anneal. Upon subsequent annealing, the samples deformed by a large number of ECAR passes displayed a continuous grain growth. A higher deformation by ECAR resulted in a slower softening, which reflects the stability of ultra-fine grains against the grain growth.

• Journal of Magnetics
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• v.11 no.3
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• pp.103-107
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• 2006

In grain oriented electrical steel process, hot band annealing has thought to be essential for obtaining good magnetic properties. New hot rolling method of heavy reduction in early hot rolling stage was applied to obtain good magnetic properties in GO process without hot band annealing. Hot rolling was carried out by varyinghot rolling reduction distribution along hot rolling pass. The heavy hot rolling reduction in rear stand improves the magnetic flux density in the case of no hot band annealing. The hot band specimens of the heavy reduction in front stand shows the elongated hot deformed microstructures in the center layer and strong {001}<110> texture.On the contrary, the heavily reduced specimens in rear stand shows the recrystallization in the center layer of hot band and strong {111}<112> and {110}<001> textures.

• Nuclear Engineering and Technology
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• v.55 no.11
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• pp.4066-4076
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• 2023

Pressure resistance welding is usually used to seal the connection between the cladding tube and the end plug made of zirconium alloy. The seal welded joint has a direct effect on the service performance of the fuel rod cladding structure. In this paper, the pressure resistance welded joints of zirconium alloy tube-plug structure were obtained by thermal-mechanical simulation experiments. The microstructure and microhardness of the joints were both analyzed. The effect of processing parameters on the microstructure was studied in detail. The results showed that there was no β-Zr phase observed in the joint, and no obvious element segregation. There were different types of Widmanstätten structure in the thermo-mechanically affected zone (TMAZ) and heat affected zone (HAZ) of the cladding tube and the end plug joint because of the low cooling rate. Some part of the grains in the joint grew up due to overheating. Its size was about 2.8 times that of the base metal grains. Due to the high dislocation density and texture evolution, the microhardnesses of TMAZ and HAZ were both significantly higher than that of the base metal, and the microhardness of the TMAZ was the highest. With the increasing of welding temperature, the proportion of recrystallization in TMAZ decreased, which was caused by the increasing of strain rate and dislocation annihilation.

• Korean Journal of Materials Research
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• v.21 no.10
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• pp.556-562
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• 2011

We carried out this study to evaluate the grain refining in and the mechanical properties of alloys that undergo severe plastic deformation (SPD). Conventional rolling (CR) and cross-roll rolling (CRR) as SPD methods were used with Ni-20Cr alloy as the experimental material. The materials were cold rolled to a thickness reduction of 90% and subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. For the annealed materials after the cold rolling, electron back-scattered diffraction (EBSD) analysis was carried out to investigate the grain boundary characteristic distributions (GBCDs). The CRR process was more effective when used to develop the grain refinement relative to the CR process; as a result, the grain size was refined from $70{\mu}m$ in the initial material to $4.2{\mu}m$ (CR) and $2.4{\mu}m$ (CRR). These grain refinements have a direct effect on improving the mechanical properties; in this case, the microhardness, yield and tensile strength showed significant increases compared to the initial material. In particular, the CRR-processed material showed more effective values relative to the CR-processed materials. The different texture distributions in the CR (001//ND) and CRR (111//ND) were likely the cause of the increase in the mechanical properties. These findings suggest that CRR can result in materials with a smaller grain size, improved texture development and improved mechanical properties after recrystallization by a subsequent annealing process.

• Korean Journal of Materials Research
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• v.30 no.6
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• pp.308-314
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• 2020

A commercial AA1070 alloy for electrical wire is severely deformed by drawing process in which a rod with an initial diameter of 9mm into is reduced to a wire of 2mm diameter. The drawn AA1070 wire is then annealed at various temperatures from 200 to 450 ℃ for 2h. Changes in microstructure, mechanical properties and electrical properties of the specimens with annealing temperature are investigated in detail. The specimen begins partially to recrystallize at 250 ℃; above 300 ℃ it is covered with equiaxed recrystallized grains over all regions. Fiber textures of {110}<111> and {112}<111> components are mainly developed, and {110}<001> texture is partially developed as well. The tensile strength tends to decrease with annealing temperature due to the occurrence of recovery or/and recrystallization. On the other hand, the elongation of the annealed wire increases with the annealing temperature, and reaches a maximum value of 33.3 % at 300 ℃. Electric conductivity of the specimens increases with annealing temperature, and reaches a maximum value of 62.6 %IACS after annealing at 450 ℃. These results are discussed in comparison with those for the other aluminum alloy.

• Journal of Welding and Joining
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• v.33 no.2
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• pp.1-7
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• 2015

This article describes the basic technical concepts for applying the friction stir welding (FSW) process to titanium and its alloys. Titanium and its alloys are demanding applications of FSW. During FSW, a protective atmosphere is needed at the welding region to prevent the joints from oxidation due to the absorption of interstitial elements (O, N, and H) at high temperature. The process parameters for FSW have great influence on the microstructure and properties of the joints. No phase transformation occurred in CP Ti because FSW was achieved below the ${\beta}$-transus temperature. Therefore, the mechanical properties of the joints with CP Ti were governed by recrystallization and grain refinement. Furthermore, the strong crystallographic texture indicating <0001>//ND formed in the stir zone. On the other hands, the phase transformation occurred in Ti-6Al-4V alloy because the process temperature reached above ${\beta}$-transus temperature. For this reason, the mechanical properties of the joints with Ti-6Al-4V alloy were altered by not only recry stallization and grain refinement but also phase transformation during FSW. Engineers who want to get sound FSW joints with Ti-6Al-4V alloy have to pay attention to the control about process conditions.

• Korean Journal of Materials Research
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• v.27 no.1
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• pp.53-61
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• 2017

Magnesium alloys are of emerging interest in the automotive, aerospace and electronic industries due to their light weight, high specific strength, damping capacity, etc. However, practical applications are limited because magnesium alloys have poor formability at room temperature due to the lack of slip systems and the formation of basal texture, both of which characteristics are attributed to the hcp crystal structure. Fortunately, many magnesium alloys, even commercialized AZ or ZK series alloys, exhibit superplastic behavior and show very large tensile ductility, which means that these materials have potential application to superplastic forming (SPF) of magnesium alloy sheets. The SPF technique offers many advantages such as near net shaping, design flexibility, simple process and low die cost. Superplasticity occurs in materials having very small grain sizes of less than $10{\mu}m$ and these small grains in magnesium alloys can be achieved by thermomechanical treatment in conventional rolling or extrusion processes. Moreover, some coarse-grained magnesium alloys are reported to have superplasticity when grain refinement occurs through recrystallization during deformation in the initial stage. This report reviews the characteristics of superplastic magnesium alloys with high-strain rate and coarse grains. Finally, some examples of SPF application are suggested.

• Transactions of Materials Processing
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• v.27 no.1
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• pp.12-17
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• 2018

This paper outlines the research findings on the microstructure and mechanical properties of AZ31 Mg alloy fabricated by differential speed rolling (DSR) with respect to processing variables such as temperature, roll speed ratio (RSR), and deformation route. The resultant microstructure of the sample, deformed by 2-pass DSRs at 473 K, comprised finer grains with more uniform distribution than those at 573 and 623 K. This was due to active recrystallization, which was expected to appear during DSR at temperatures higher than 573 K. When the sample was deformed via DSR with RSR of 1:4 for the upper and lower rolls at 453 K, the values of yield and ultimate tensile strength were observed to be higher than their counterpart with RSR of 1:1. The application of sample rotation around the longitudinal axis would give rise to an excellent combination of tension strength (~330 MPa) and ductility (~20 %) at ambient temperatures. This is discussed based on its uniform fine grained structure and the softening of basal texture.