• Title/Summary/Keyword: Range of variation

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Simultaneous Determination of Aflatoxins and Ochratoxin A in Pork by LC-MS/MS (LC-MS/MS를 이용한 돼지고기 중 총아플라톡신 및 오크라톡신 A 동시분석법 확립)

  • Paek, Ockjin;Park, Songyi;Park, Ki Hun;Kim, Sheen-Hee;Suh, Saejung;Yoon, Hae Jung
    • Journal of Food Hygiene and Safety
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    • v.31 no.3
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    • pp.194-200
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    • 2016
  • Aflatoxins and ochratoxin A (AFTs and OTA) are secondary fungal metabolites produced by several moulds, mainly by Aspergillus flavus by Aspergillus ochraceus and Penicillium verrucosum, and these toxins can be transferred to animals and humans through the ingestion of contaminated feed and food. This study was to develop the analytical method for determination the levels of AFTs ($B_1$, $B_2$, $G_1$ and $G_2$) and OTA in pork. The AFTs and OTA were analyzed simultaneously by electrospray ionization in positive ion mode and mass reaction monitoring (MRM) after solid phase extract (SPE) columns clean-up. Performance characteristics, such as accuracy, precision, linear range, limit of detection (LOD) and quantification (LOQ), were also determined. Matrix-matched standard calibration was used for quantification, obtaining the recoveries in the range of 67.3~108.2% with the relative standard deviations of < 20%. Limits of detection and quantification were also estimated, obtaining the limits of quantification ranged in $0.7{\sim}1.3{\mu}g/kg$. The results of the inter-day study, which was performed with pork samples for 3 days, showed an accuracy of 92.0~109.9%. The precisions (expressed as relative standard deviation values) for the inter day variation were 2.6~17.8%. The method developed in this study was able to carry out the analysis with the satisfactory intensity and accuracy.

Quality characteristics of home-made doenjang, a traditional Korean soybean paste (가정에서 제조된 전통된장의 품질특성)

  • 박석규;서권일;손미예;문주석;이영환
    • Korean journal of food and cookery science
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    • v.16 no.2
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    • pp.121-127
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    • 2000
  • To assess the quality characteristics of home-made Doenjang prepared by traditional methods, general components, organic acids, amino acids and fatty acid composition of Doenjang were investigated. The contents of moisture, crude protein, crude lipid, salt and the titratable acidity(as milliliter of 0.1 N NaOH consumed) of Doenjang were 57.3%, 11.6%, 8.3%, 13.9%, and 11.8, respectively. There were wide variation in the contents of crude protein and salt among all samples. The average content of amino type nitrogen was 308.4mg%(w/w), however, it ranged from 202.3 to 416.3 mg% in which the contents some samples were 1.3∼2.1 folds greater than others. Hunter color values of L(lightness), a(redness) and b(yellowness) were 37.3, +19.6, and +17.5, respectively. Browning index value(expressed as optical density at 425 nm) of water-soluble compound(2.23) was more than 5.7 times higher than that of water-insoluble compound(0.39). The contents of free and total amino acids were 2908.9 and 9019.3 mg%, respectively, and the range of free amino acids(1.8∼6.2 times) were much wider than the range of total amino acids(1.2∼2.0 times). Glutamic acid was most abundant in free and total amino acids as 576 and 1,126 mg%, respectively. The main organic acid was lactic acid as 326.8 mg% ranging from 59.4 to 613.4 mg%. Linoleic acid(49.24%) showed the highest content in total fatty acids. Unsaturated fatty acid comprised 81.97% of total fatty acids and polyunsaturated fatty acid ranged from 51.79 to 62.97%.

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A Study on the Thermal Comfort Zone and Energy Use of Radiant Floor Heating by Residential Style and Clothing Level (생활특성과 착의량에 따른 바닥복사난방 공간의 열쾌적 범위 및 에너지 사용량에 관한 연구)

  • Kim, Sang-Hun;Chung, Kwang-Seop;Kim, Young-Il
    • Journal of Energy Engineering
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    • v.24 no.1
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    • pp.24-31
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    • 2015
  • The purpose of this study is to provide the thermal comfort range according to the residential style and clothing level at radiant floor heating space, and compare the annual energy consumption and energy cost for each condition. Lower neutral point temperature has been stood for floor sitting style than chair sitting style, which appears that the thermal sensation was affected by local heat transfer between floor surface and the human body. The result of research indicates that neutral point temperature was in inverse proportion with the clothing level. It is interpreted that the increasing of clothing level results decrement of heat loss from human body, and is available to achieve same thermal comfort at lower room temperature. It was analyzed that the floor sitting style is more economical residential style than the chair sitting style, because the energy consumption of the floor sitting style is saved by 6.0% in average to compare with that of the chair sitting style. It is analyzed that energy consumption has been decreased by 13.5% with the clothing level of 1.2 Clo than with that of 1.0 Clo, and decreased by 18.0% than with that of 0.8 Clo, which explains that the energy saving can be achieved with the variation in life habit to increase the clothing level.

Soil CO2 Efflux and Leaf-Litter Decomposition of Quercus variabilis and Pinus densiflora Stands in the Southern Region of Korean Peninsular

  • Kim, Sung Bin;Jung, Nam Chul;Lee, Kye-Han
    • Journal of Korean Society of Forest Science
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    • v.98 no.2
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    • pp.183-188
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    • 2009
  • It is necessary to determine the amount of carbon dioxide ($CO_2$) absorbed by plants and released from forest floor into atmosphere, to gain a better understanding how forests participate in the global carbon cycle. Soil $CO_2$ efflux, litter production, and decomposition were investigated in Q. variabilis and P. densiflora stands in the vicinity of Gwangju, Chonnam province. Soil $CO_2$ efflux was measured using Infrared Gas Analyzer (IRGA) at midday of the 10th day at every month over 12-month period, to quantify seasonal and annual budgets of soil $CO_2$ efflux. Soil temperature and soil moisture were measured at the same time. Seasonal soil $CO_2$ efflux in Q. variabilis and P. densiflora were the highest in summer season. In August, maximum soil $CO_2$ efflux in Q. variabilis and P. densiflora was 7.49, $4.61CO_2{\mu}mol{\cdot}m^{-2}{\cdot}s^{-1}$, respectively. Annual $CO_2$ efflux in each stand was 1.77, $1.67CO_2kg{\cdot}m^{-2}$ respectively. Soil $CO_2$ efflux increased exponentially with soil temperature and related strongly in Q. variabilis ($r^2$=0.96), and in P. densiflora ($r^2$=0.91). Litter production continued throughout the year, but showed a peak on November and December. Annual litter production in the Q. variabilis and P. densiflora stands were $613.7gdw{\cdot}m^{-2}{\cdot}yr^{-1}$ and $550.5gdw{\cdot}m^{-2}{\cdot}yr^{-1}$.$yr^{-1}$, respectively. After 1 year, % remaining mass of Q. variabilis and P. densiflora litter was 48.2, 57.1%, respectively. The soil $CO_2$ efflux rates in this study showed clear seasonal variations. In addition, the temporal variation in the $CO_2$ efflux rates was closely related to the soil temperature fluctuation rather than to variations in the soil moisture content. The range of fluctuation of soil $CO_2$ efflux and litter decomposition rate showed similar seasonal changes. The range of fluctuation of soil $CO_2$ efflux and litter decomposition rate was higher during summer and autumn than spring and winter.

Spatial Variability Analysis of Paddy Rice Yield in Field (필지내 벼 수량의 공간변이 해석)

  • 이충근;우메다미키오;정인규;성제훈;김상철;박우풍;이용범
    • Journal of Biosystems Engineering
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    • v.29 no.3
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    • pp.267-274
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    • 2004
  • Using geo-statistical method, yield data of different fields were analyzed to examine their field variability according to examining year, analysis method. Semivariogram and Kriged maps of geo-statistical analysis were used to examine their spatial dependence within a filed. The results obtained were as follows. 1) Descriptive statistical results of the yield showed that the yield and the difference of yield ranged from 100 to 946kg/10a and from 272 to 653kg/10a, respectively within a field. The coefficient of variation also ranged from 5.9 to 22.4 %. 2) More than 90% of yield data were placed between 350 to 850kg/10a. e results indicated that the gram mass flow sensor should have the measuring range from 0.34 to 0.82kg/s considering the yields when 4 rows head-feeding combine with 0.8 m/s of working speed was utilized. 3) A high spatial dependence was found within paddy field. The Q values ranged from 0.20 to 0.97, and the range of spatial dependence was from 6.9 to 53.3m. From this result, the rational sampling interval for yield investigation was estimated 6.9m. 4) Yields within a field between observation years showed considerable variability even if the field was evenly cultivated and managed. To apply precision agriculture in a paddy field, the field test should be continued to build a solid data-base including meteorological data, blight damage and insect damage.

Analysis of Stream Water Quality Improvement Using Surface-flow Wetland (자유수면형 인공습지에 의한 저농도 고유량의 하천수질개선 효과 분석)

  • Ham, Jong-Hwa;Yoon, Chun G.;Koo, Won-Seck;Kim, Hyung-Chul;Shin, Hyum-Bhum
    • Journal of The Korean Society of Agricultural Engineers
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    • v.47 no.1
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    • pp.79-91
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    • 2005
  • Wetland systems are widely accepted natural water purification systems around the world in nonpoint sources pollution control. Constructed wetlands have become a popular technology for treating contaminated surface and wastewater. In this study, the field experiment to reduce nonpoint source pollution loadings from polluted stream waters using wetland system was performed from June 2002 to March 2004, including winter performance using four newly constructed wetlands. The Dangjin stream water flowing into Seokmun estuarine lake was pumped into wetlands, and inflow and hydraulic residence time of the system was $500m^{3}{\~}1500m^{3}/day\;and\;2{\~}5$ days respectively. After 3 years operation plant-coverage was about $80~90\%$ from zero at initial stage even with no plantation. Average water quality of the influent in growing season was BOD_{5}\;3.96mg/L$, TSS 22.98 mg/L, T-N 3.29 mg/L, T-P 0.30 mg/L. The average removal rate of four wetlands for $BOD_{5},\;TSS,\;T-N\;and\;T-P$ in growing season was $24\%$, $62\%$, $54\%$, and $51\%$, respectively. And average water quality of the influent in winter season was $BOD_{5}$ 4.92 mg/L, TSS 12.47 mg/L, T-N 5.54 mg/L, and T-P 0.32 mg/L, respectively. The average removal rate of four wetlands for them was $-21\%$. $23\%$, $33\%$, and $53\%$, respectively. The reason of higher BOD_{5} effluent concentration in winter season might be that low temperature restrained microorganism activity and a organic body from the withered plant and algae was flown out. Except the result of $BOD_{5}$, the effectiveness of water quality improvement in winter season was satisfactory for treating polluted stream waters, and $BOD_{5}$ variation was within the range of background concentration. Performance of the experimental system was compared with existing data base (NADB), and it was within the range of general system performance. Overall, the wetland system was found to be satisfactory for NPS control such as improvement of polluted stream water.

A Study on Comparison of Density Test Methods for Quality Control of Cement and Mineral Admixture (시멘트 및 혼화재의 품질관리를 위한 밀도 시험방법 비교 연구)

  • Jae-Seung, Lee;Sang-Kyun, Noh;Cheol, Park;Hong-Chul, Shin
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.10 no.4
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    • pp.435-442
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    • 2022
  • In this study, the density of KS L 5110 was compared with that of gas pycnometer and electronic densimeter for efficient density management of cement, blast furnace slag powder and fly ash. Correlation and usability according to the test method were reviewed, and based on the results of the experiment, the availability of alternative test methods was analyzed. As a result of the density test according to test methods, the density of cement, blast furnace slag powder and fly ash tended to decrease in the order of gas pycnometer, KS L 5110 and electronic densimeter. Because the volume range of the sample to be evaluated is different depending on test methods. The coefficient of determination R2 was in the range of 0.71 to 0.93, and the correlation according to test methods showed a relatively good correlation. If correction is applied through correlation, it is analyzed that alternative test methods can be used. As a result of the usability review considering the test procedure, measurement time and coefficient of variation, the gas pycnometer had the simplest test procedure and good reliability. In addition, it is expected that the reproducibility between the testers is relatively high because the skill is not greatly required.

Tritium Concentrations of Tritiated Water Vapor and Tritiated Hydrogen in the Atmosphere in Taejon (대전지역 대기중 수증기상태 (HTO) 및 가스상태 (HT) 삼중수소의 농도)

  • Kim, C.K.;Han, M.J.;Kim, K.H.
    • Journal of Radiation Protection and Research
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    • v.22 no.2
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    • pp.97-101
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    • 1997
  • During the period of March 1995 to December 1995, tritium concentrations of tritiated water vapor (HTO) and tritiated hydrogen (HT) in the atmosphere in Taejon were measured to evaluate present background levels of tritium in the atmosphere. Air samples were collected continuously for three weeks with a sampling system for tritium in the atmosphere and were analyzed by a liquid scintillation counting system. The range of the atmospheric HTO concentrations was 3.2-36 mBq $m^{-3}$ with a mean value of 16.2 mBq $m^{-3}$. The atmospheric HTO concentrations were the highest in summer and the lowest in winter. This trend was similar to the variation of atmospheric absolute humidity. The specific activities of tritium in atmospheric water vapor in Taejon ranged from 0.62 Bq $L^{-1}$ to 3.82 Bq $L^{-1}$ with a mean value of 2.04 Bq $L^{-1}$. The atmospheric HT concentrations were in the range of 35.7 mBq $m^{-3}$ to 48.9 mBq $m^{-3}$ with a mean value of 41.1 mBq $m^{-3}$.

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An Experimental Study on the Rheological Properties of the Combined Self-Compacting Concrete by Quality Variations (품질변동에 따른 병용계 자기충전 콘크리트의 유동특성에 관한 실험적 연구)

  • Kwon, Yeong-Ho
    • Journal of the Korea Concrete Institute
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    • v.26 no.3
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    • pp.277-285
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    • 2014
  • The purpose of this study is to investigate experimentally the variation factors range having influence on the rheological properties of the combined self-compacting concrete according to materials quality, weighting error and site conditions. Two types cement (blast-furnace slag cement and belite cement), lime stone powder as binder and the optimum mix proportions in the preceded study are selected for this study. Also, variations for sensitivity test are as followings; (1) Concrete temperature 3 cases (2) Surface moisture of sand 5cases (3) Fineness modulus of sand 5cases (4) Specific surface of lime stone powder 3cases (5) Dosage of chemical admixture 5cases. Slump flow ($650{\pm}50mm$), 500 mm reaching time (($7{\pm}3sec$), V-type flowing time ($15{\pm}5sec$) and U-box height (min. 300 mm) are tested for sensitivity. As test results, the variations range for quality control are as followings. (1) Concrete temperature; $10{\sim}20^{\circ}C$(below $30^{\circ}C$) (2) Surface moisture of sand; $base{\pm}0.6%$ (3) Fineness modulus of sand; $2.6{\pm}0.2$ (4) Dosage of chemical admixture; $base{\pm}0.2%$ (5) Specific surface of lime stone powder $6000cm^2/g$. Compared with two types cement including based belite cement (binary type) and based slag cement (ternary type), the combined self-compacting concrete used belite cement type is most stable in the quality control because of high contents for lime stone powder and $C_2S$. It is to propose a control scheme of the combined self-compacting concrete in the actual construction work.

Design and Performance Evaluation of Two-Layered Microwave Absorbers(Dielectric/Magnetic) for Wide Oblique Incidence Angles Used for ITS (ITS용 2층형 전파 흡수체(유전체/자성체) 설계 및 경사 입사 흡수 특성 해석)

  • Kim, Jae-Woong;Kim, Sung-Soo
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.18 no.11
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    • pp.1217-1223
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    • 2007
  • Advanced microwave absorbers for wide oblique incidence angles are required in many applications including wireless communication or vehicle identification in ITS(Intelligent Transport System) where 5.8 GHz DSRC(Dedicated Short Range Communication) system is applied. In this study, two-layered microwave absorber(with a laminate structure of dielectric/magnetic composites) has been designed for the achievement of low reflection coefficient over wide incidence angles at 5.8 GHz. Iron flake particles are used as the filler in the absorbing layer, and the magnetic composite sheet exhibits high magnetic loss due to ferromagnetic resonance in gigahertz frequencies. The surface layer of low dielectric constant containing small amount of carbon black is used as the impedance transformer. On the basis of transmission line theory, the reflection loss has been calculated for the two-layer structure with variation of incident angles for both TE(Transverse Electric) and TM(Transverse Magnetic) polarizations. At the optimum thickness of the composite layers, a low value of reflection loss(less than -10 dB) has been predicted for wide incidence angles up to $55^{\circ}$ which is in good agreement with the measured value determined by free-space measurement.