• 한국약용작물학회지
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• 제16권6호
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• pp.446-454
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• 2008

An advanced extraction method by ultrasonic extraction with applied solid phase extraction (SPE) has been developed for the determination of simultaneous eight major ginsenosides, namely ginsenosides Rg1, Re, Rf, Rb1, Rg2, Rc, Rb2, and Rd in the root of Panax ginseng. Four extraction methods including n-BuOH reflux extraction (Method A), 70% EtOH reflux extraction (Method B), 50% MeOH reflux extraction with SPE (Method C), and 50% MeOH ultrasonication with SPE clean-up process (Method D) were investigated for the determination of eight major ginsenosides. Total contents of ginsenosides were highest by extraction of Method C as $2.408{\pm}0.011%$. However, Method D was evaluated as relatively simpler and more efficient method due to short extraction time, small solvent consumption and less expensive, compared to conservative reflux method. Ginsenosides were also satisfactorily separated with good resolution and the accuracy range was between 1.05 and 4.06% as relative standard deviation (RSD) by Method D. SPE condition and HPLC condition were further optimized for determination of eight major ginsenosides by the ultrasonic extraction method. Conclusively, ultrasonic extraction of 2 g sample of ginseng using ultrasonic bath and 1 loading for SPE was evaluated as proper condition for extraction of ginseng.

• 한국약용작물학회지
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• 제16권6호
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• pp.434-438
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• 2008

To selection of optimal shading material, two-year-old ginseng (Panax ginseng C. A. Meyer) of new cultivar, 'Cheonpoong' (CP), and native species 'Hwangsookjong' (HS) were cultured under three kinds of shading materials such as three-layered blue and a one-layered black PE (polyethylene) net (TBSB), blue PE sheet (BS), and aluminium coated PE sheet (AS) in imperfectly drained paddy soil. Growth characteristics, yield and ginsenoside contents were investigated under three shading materials. Yield and ginsenoside contents of ginseng were distinctly affected by intensity and quality of sunlight penetrated through shading materials. Light transmission ratio, air and soil temperature according to shading materials were higher in order of BS, AS, and TBSB. However, ratio of aerial phase and porosity of the soil were higher in order of AS, BS, and TBSB, respectively. There was no significantly difference in the ratio of rusty colored root by shading materials. CP showed higher stem length, leaf area, and root weight than that of HS, while the former showed distinctly lower discolored leaf ratio than that the other. Eight kinds of ginsenosides content of CP were higher than that of HS in $Rg_1$, Re, Rf, $Rb_1$ and Rc except $Rg_2$, $Rb_2$, and $Rb_3$. Total ginsenoside contents of CP was distinctly higher than that of HS. Total ginsenoside contents as affected by shading materials was higher in order of BS, TBSB, and AS in CP, while TBSB, BS, and AS in HS.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2012년도 춘계학술발표대회
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• pp.65-65
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• 2012

Copper zinc tin sulfide ($Cu_2ZnSnS_4$, CZTS) is a very promising material as a low cost absorber alternative to other chalcopyrite-type semiconductors based on Ga or In because of the abundant and economical elements. In addition, CZTS has a band-gap energy of 1.4~1.5eV and large absorption coefficient over ${\sim}10^4cm^{-1}$, which is similar to those of $Cu(In,Ga)Se_2$(CIGS) regarded as one of the most successful absorber materials for high efficient solar cell. Most previous works on the fabrication of CZTS thin films were based on the vacuum deposition such as thermal evaporation and RF magnetron sputtering. Although the vacuum deposition has been widely adopted, it is quite expensive and complicated. In this regard, the solution processes such as sol-gel method, nanocrystal dispersion and hybrid slurry method have been developed for easy and cost-effective fabrication of CZTS film. Among these methods, the hybrid slurry method is favorable to make high crystalline and dense absorber layer. However, this method has the demerit using the toxic and explosive hydrazine solvent, which has severe limitation for common use. With these considerations, it is highly desirable to develop a robust, easily scalable and relatively safe solution-based process for the fabrication of a high quality CZTS absorber layer. Here, we demonstrate the fabrication of a high quality CZTS absorber layer with a thickness of 1.5~2.0 ${\mu}m$ and micrometer-scaled grains using two different non-vacuum approaches. The first solution-processing approach includes air-stable non-toxic solvent-based inks in which the commercially available precursor nanoparticles are dispersed in ethanol. Our readily achievable air-stable precursor ink, without the involvement of complex particle synthesis, high toxic solvents, or organic additives, facilitates a convenient method to fabricate a high quality CZTS absorber layer with uniform surface composition and across the film depth when annealed at $530^{\circ}C$. The conversion efficiency and fill factor for the non-toxic ink based solar cells are 5.14% and 52.8%, respectively. The other method is based on the nanocrystal dispersions that are a key ingredient in the deposition of thermally annealed absorber layers. We report a facile synthetic method to produce phase-pure CZTS nanocrystals capped with less toxic and more easily removable ligands. The resulting CZTS nanoparticle dispersion enables us to fabricate uniform, crack-free absorber layer onto Mo-coated soda-lime glass at $500^{\circ}C$, which exhibits a robust and reproducible photovoltaic response. Our simple and less-toxic approach for the fabrication of CZTS layer, reported here, will be the first step in realizing the low-cost solution-processed CZTS solar cell with high efficiency.

• Journal of the Optical Society of Korea
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• 제13권1호
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• pp.8-14
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• 2009

In a laser-plasma wakefield accelerator, the ponderomotive force of an ultrashort high intensity laser pulse excites a longitudinal wave or plasma bubble in a way similar to the excitation of a wake wave behind a boat as it propagates on the water surface. Electric fields inside the plasma bubble can be several orders of magnitude higher than those available in conventional RF-based particle accelerator facilities which are limited by material breakdown. Therefore, if an electron bunch is properly phase-locked with the bubble's acceleration field, it can gain relativistic energies within an extremely short distance. Here, in the bubble regime we show the generation of stable and reproducible sub GeV, and GeV-class electron beams. Supported by three-dimensional particle-in-cell simulations, our experimental results show the highest acceleration gradients produced so far. Simulations suggested that the plasma bubble elongation should be minimized in order to achieve higher electron beam energies.

• 한국자기학회지
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• 제7권5호
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• pp.237-242
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• 1997

초미세결정 구조를 갖는 Fe-Hf-O계 연자성박막을 Ar+ $O_{2}$ 혼합가스 중에서 산소분압을 10%로 고정하고 Hf의 면적비를 변화시켜 반응성 스퍼터링에 의해 제조하였다. 가장 우수한 연자기 특성을 나타낸 F $e_{82}$H $f_{3.4}$ $O_{14.6}$의 초미세결정 박막의 경우 증착상태에서 각각 포화자속밀도 17.7 kG, 보자력 0.7 Oe 및 실효투자율 (0.5 ~ 100 MHz) 2,500을 나타내었다. Fe-Hf-O계 박막의 조성은 고정된 산소분압 하에서 Hf함량의 변화에 따라 박막내 산소의 함량이 비례하여 변화하였다. 또한 미세구조는 Hf-oxide의 함량이 적은 경우에는 .alpha. -Fe 결정상에 Hf-oxide가 석출된 형태로 나타났으며 Hf-oxide의 양이 증가할수록 .alpha. -Fe 결정상과 Hf-oxide 비정질의 혼상을 거쳐 전체적으로 비정질로 변화하는 경향을 나타내었다. Fe-Hf-O계 박막의 전기비저항은 Hf-oxide의 양이 증가할수록 증가하는 경향을 나타내었고 가장 우수한 연자기 특성을 나타내는 F $e_{82}$H $f_{3.48}$ $O_{14.6}$ 박막의 경우, 약 150 .mu. .ohm. cm로 $O_{2}$를 첨가하지 않은 경우의 30 .mu. .ohm. cm에 비하여 약 5배 증가된 값을 나타내었다. 또한 Fe-Hf-O 박막의 성능지수는 수십 MHz 영역에서 20 ~ 50의 값을 나타내었다.내었다.다.내었다.다.

• 한국진공학회지
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• 제14권4호
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• pp.207-214
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• 2005

본 연구에서는 스위치, 위상변위기, 감쇄기등 전파제어회로를 설계 및 제작할 수 있는 pHEMT스위치 소자에 적합한 에피구조를 설계하였다. 고성능의 스위치 소자를 위한 pHEMT 채널층 구조는 이중 면도핑층을 가지며 사용 중 게이트 전극의 전계강도가 약한 깊은 쪽 채널층의 Si 면농도가 상층부보다 약 1/4정도 낮을 경우 격리도등 우수한 특성을 보였다. 설계된 에피구조와 ETRI의 $0.5\mu$m pHEMT MMIC 공정을 이용하여 2.4GHz 및 5GHz 대역 표준 무선랜 단말기에 활용 가능한 SPDT Tx/Rx MMIC 스위치를 설계 및 제작하였다. 제작된 SPDT형 스위치는 주파수 6.0 GHz, 동작전압 0/-3V에서 삽입손실 0.849 dB, 격리도 32.638 dB, 그리고 반사손실 11.006 dB의 특성을 보였으며, 전력전송능력인 $P\_{1dB}$는 약 25dBm, 그리고 선형성의 척도인 IIP3는 42 dBm 이상으로 평가되었다. 이와 같은 칩의 성능은 본 연구에서 개발된 SPDT 단일고주파집적회로 스위치가 2.4GHz뿐만 아니라 SGHB 대역 무선랜 단말기에 활용이 충분히 가능함을 말해준다.

• 한국체육학회지인문사회과학편
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• 제54권1호
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• pp.505-514
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• 2015

이 연구는 다양한 불안정면에서의 스쿼트 운동이 체간과 하지근육의 활성도에 미치는 영향을 비교하는데 목적이 있다. 10명의 피험자가 안정면, 불안정면인 스타빌리티 블루와 블랙, 보수에서 75% 1RM의 강도에서 스쿼트 동작을 실시하였다. 체간근육으로는 복직근, 외복사근, 내복사근 및 다열근에 근전도를 부착하였고, 하지근육으로는 대둔근, 중둔근, 대퇴이두근, 대퇴직 근, 외측광근, 내측광근, 내측비복근, 외측비복근, 가지미근, 전경근에 근전도를 부착하여 스쿼트 동작의 상승과 하간구상의 근활성도를 측정하였다. 안정면과 불안정면에서의 근활성도를 비교하기 위하여 일원변량분석을 실시하였으며, 사후검증으로 sheffe를 이용하였다. 하강구간에서 근활성도는 보수에서의 스쿼트 동작 시 내측광근, 다열근, 대둔근과 중둔근의 활성도가 안정면과 다른 불안정면에서의 스쿼트 동작 시보다 높게 나타났다. 상승구간에서 근활성도는 보수에서의 스쿼트 동작 시 대둔근의 활성도가 안정면과 다른 불안정면에서의 스쿼트 동작 시보다 높게 나타났다. 이러한 결과는 보수에서의 스쿼트 동작이 체간근육과 둔근의 활성도를 증가시키는데 효과적이라고 제시할 수 있다. 그러나 하지근육의 활성도는 불안정성에 따른 차이가 없는 것으로 사료된다.