• Bulletin of the Korean Chemical Society
• /
• 제18권7호
• /
• pp.706-710
• /
• 1997

Isotope ratios of K, Ca, Cr and Fe are measured at cool plasma condition generated using high carrier flow rate and relatively low RF power of 900 W. Background molecular ions are suppressed to below 100 counts which give isobaric interference to the analytes. The background ions show different attenuation characteristics at increased carrier flow rate and hence for each element different carrier flow rate should be used to measure isotope ratios without isobaric interference. Isotope ratios are measured at both scan and peak-hopping modes and compared with certified or accepted ratios. The measured isotope ratios show some mass discrimination against low mass due to low ion energy induced from a copper shield to eliminate capacitive coupling of plasma with load coil.

• Bulletin of the Korean Chemical Society
• /
• 제19권5호
• /
• pp.501-503
• /
• 1998

In this work, we applied the 1D $11^B$ nutation NMR method for the analysis of the local structural environments in powdered borosilicates $(SiO_2-B_2O_3)$. Spin dynamics during a rf irradiation for spin I=3/2 was analytically calculated with a density ma trix formalism. Spectral simulation programs were written in MATLAB on a PC. Two borosilicates prepared by the sol-gel process at different stabilization temperature were used for the 1D $11^B$ nutation NMR experiment. The $11^B$ NMR parameters, quadrupole coupling constants $(e^2qQ/h)$ and asymmetry parameters (η), for each borosilicate were extracted from the nonlinear least-squares fitting. The effects of heat treatments on the local structures of boron sites in borosilicates were discussed.

• Bulletin of the Korean Chemical Society
• /
• 제19권5호
• /
• pp.519-524
• /
• 1998

In this work, we applied the 1D 11B nutation NMR method for the analysis of the local structural environments in powdered borosilicates (SiO2-B2O3). Spin dynamics during a rf irradiation for spin I=3/2 was analytically calculated with a density matrix formalism. Spectral simulation programs were written in MATLAB on a PC. Two borosilicates prepared by the sol-gel process at different stabilization temperature were used for the 1D 11B nutation NMR experiment. The 11B NMR parameters, quadrupole coupling constants (e2qQ/h) and asymmetry parameters (η), for each borosilicate were extracted from the nonlinear least-squares fitting. The effects of heat treatments on the local structures of boron sites in borosilicates were discussed.

• Journal of Magnetics
• /
• 제10권3호
• /
• pp.99-102
• /
• 2005

Modification in exchange bias of a NiFe/FeMn/NiFe trilayer, on introduction of a nonmagnetic Al layer at the top FeMn/NiFe interface, is investigated in multilayers prepared by rf magnetron sputtering. The introduction of Al layer leads to vanishing of bias of the top NiFe layer. But the bias for the bottom NiFe layer increases steadily with increasing Al layer thickness and attains bias (230 Oe) which is greater than that of the trilayer without the Al layer (150 Oe). When the top NiFe layer thickness is varied, exchange bias has highest value at 12 nm thickness for 1 nm thicknes of Al layer. Ion beam etching of the top NiFe layer also leads to an enhancement in bias for the bottom NiFe layer.

• 한국진공학회:학술대회논문집
• /
• 한국진공학회 2000년도 제18회 학술발표회 논문개요집
• /
• pp.174-174
• /
• 2000

A strong antiferromagnetic coupling in Fe/Si multilayered films (MLF) had been recently discovered and much consideration has been given to whether the coupling in the Fe/Si MLF system has the same origin as the metal/metal MLF. Nevertheless, the nature of the interfacial ron silicide is still controversial. On one hand, a metal/ semiconductor structure was suggested with a narrow band-gap semiconducting $\varepsilon$-FeSi spacer that mediates the coupling. However, some features show that the nature of coupling can be well understood in terms of the conventional metal/metal multilayered system. It is well known that both magneto-optical (MO) and optical properties of a metal depend strongly on their electronic structure that is also correlated with the atomic and chemical ordering. In this study, the nature of the interfacial regions is the Fe/Si multilayers has been investigated by the experimental and computer-simulated MO and optical spectroscopies. The Fe/Si MLF were prepared by rf-sputtering onto glass substrates at room temperature with the number of repetition N=50. The thickness of Fe sublayer was fixed at 3.0nm while the Si sublayer thickness was varied from 1.0 to 2.0 nm. The topmost layer of all the Fe/Si MLF is Fe. In order to carry out the computer simulations, the information on the MO and optical parameters of the materials that may constitute a real multilayered structure should be known in advance. For this purpose, we also prepared Fe, Si, FeSi2 and FeSi samples. The structural characterization of Fe/Si MLF was performed by low- and high -angle x-ray diffraction with a Cu-K$\alpha$ radiation and by transmission electron microscopy. A bulk $\varepsilon$-FeSi was also investigated. The MO and optical properties were measured at room temperature in the 1.0-4.7 eV energy range. The theoretical simulations of MO and optical properties for the Fe/Si MLF were performed by solving exactly a multireflection problem using the scattering matrix approach assuming various stoichiometries of a nonmagnetic spacer separating the antiferromagnetically coupled Fe layers. The simulated spectra of a model structure of FeSi2 or $\varepsilon$-FeSi as the spacer turned out to fail in explaining the experimental spectra of the Fe/Si MLF in both intensity and shape. Thus, the decisive disagreement between experimental and simulated MO and optical properties ruled out the hypothesis of FeSi2 and $\varepsilon$-FeSi as the nonmagnetic spacer. By supposing the spontaneous formation of a metallic ζ-FeSi, a reasonable agreement between experimental and simulated MO and optical spectra was obtained.

• 조명전기설비학회논문지
• /
• 제20권4호
• /
• pp.7-11
• /
• 2006

본 논문에서는 $Mo/SiO_2/Si(100)$ 기판 위에 MOCVD(Metal-Organic-Chemical-Vapor Deposition)법을 이용하여 C축 방향으로 성장시킨 AIN(Aluminum Nitride) 박막을 이용하여 GHz대역 무선 통신에서 사용할 수 있는 FBAR(Film-Bulk-Acoustic Resonator)을 제작하였다. 제작된 공진부의 공진주파수와 반공진주파수는 각각 3.189[GHz]와 3.224[GHz]으로 측정되었으며, Q값(Quality Factor)과 유효한 전기기계 결합계수(${k_{eff}}^2$)는 각각 24.7과 2.65[%]로 평가되었다. AIN의 증착(Deposition) 조건은 $950[^{\circ}C]$의 기판표면(Substrate) 온도, 20Torr의 압력, 25000의 N/Al의 V/III비로 증착하였다. $4{\times}10^{-5}[\Omega{cm}]$의 Mo 하부전극 고유저항과 $Mo/SiO_2/Si(100)$ 기판 위에 AIN(0002) FWHM(Full-Width at Half-Maximum) 4를 갖는 C축 방향성의 AIN 박막을 성공적으로 성장시켰다. 따라서 증착된 AIN박막의 FWHM값은 GHz대역 무선 통신용 RF(Radio Frequency) 밴드 패스 필터 설계에 유용하게 사용될 것이다.

• 한국위성정보통신학회논문지
• /
• 제2권2호
• /
• pp.41-47
• /
• 2007

2009년 발사예정인 우리나라가 개발한 최초의 정지궤도위성 COMS에는 기상센서, 해양센서 및 Ka대역 통신탑재체등 세개의 탑재체가 실리며 해양센서 및 기상센서의 측정데이타를 전송하기위한 L대역 통신중계기가 있다. 또한 S대역의 원격 측정 및 원격명령서브시스템과 Ka대역 비콘등이 있다. Ka대역 통신탑재체는 스위칭 중계기로서 부품의 우주인증 및 재난통신서비스에 활용될 전망이다. 또한 Ka대역 비콘은 지상국 안테나의 포인팅 및 강우감쇠 실험을 포함한 Ka대역 전송실험에 활용될 예정이다. 본 논문은 L대역 센서데이타 전송용 중계기 및 S 대역 원격명령/측정 서브시스템의 RF 복사가 Ka 대역 중계기 및 비콘에 어떤 영향을 주며, Ka밴드 비콘이 L 대역 및 S 대역 중계기에 어떤 영향을 주는지 조사하였다. 중계기들의 상향/하향 링크시 출력, 안테나들의 기하학적 위치 및 거리 및 중계기들에 포함되어 있는 필터들의 rejection 그리고 편파에 의한 degradation factor등을 포함하여 coupling factor를 고려하여 상호 호환성을 고려하였다. 분석결과 L대역 및 S대역 중계기에 의한 Ka대역 탑재체에 대한 영향은 미미한 것으로 계산되었으며, Ka대역 비콘의 영향도 무시할 정도임을 밝혔다.

• 한국산학기술학회논문지
• /
• 제12권7호
• /
• pp.3169-3175
• /
• 2011

본 논문에서는 가유전체 기판구조의 증가하는 유효 유전율 효과를 이용하여 방향성결합기를 소형화하여 설계하는 것에 대하여 기술한다. 방향성결합기는 RF 신호의 크기를 간접적으로 측정하거나 신호전력을 결합하는데 널리 사용되는 회로이다. 가유전체 기판구조는 다수의 도금된 비어홀에 의하여 표준형 기판보다 유효 유전율이 증가하는 특성을 지니는데, 이 특성이 바로 회로 소형화에 이용된다. 한 예로써 2GHz대에서 15dB의 결합계수를 갖는 방향성결합기가 표준형 기판과 가유전체 기판구조에 대하여 각각 설계되고 그 크기가 비교된다. 표준형 회로와 비교할 때, 가유전체 기판구조로 소형화된 방향성결합기는 동일한 성능을 유지하면서도 1/3로 줄어든 회로의 크기를 갖는다. 또한 소형화된 방향성결합기를 제작하여 측정한 성능은 예측 결과와도 매우 유사함을 보여준다. 측정한 성능 결과는 2GHz대에서 -14.62B의 결합도, -24.1dB의 정합도, -0.38dB의 삽입손실 특성을 보여준다.

• 한국초전도ㆍ저온공학회논문지
• /
• 제16권3호
• /
• pp.21-25
• /
• 2014

As wireless power transfer (WPT) technology using strongly coupled electromagnetic resonators is a recently explored technique to realize the large power delivery and storage without any cable or wire, this technique is required for diffusion of electric vehicles (EVs) since it makes possible a convenient charging system. Typically, since the normal conducting coils are used as a transmitting coil in the CPT system, there is limited to deliver the large power promptly in the contactless EV charging system. From this reason, we proposed the combination CPT technology with HTS transmitting antenna, it is called as, superconducting contactless power transfer for EV (SUWPT4EV) system. As the HTS coil has an enough current density, it can deliver a mass amount of electric energy in spite of a small scale antenna. The SUCPT4EV system has been expected as a noble option to improve the transfer efficiency of large electric power. Such a system consists of two resonator coils; HTS transmitting antenna (Tx) coil and normal conducting receiver (Rx) coil. Especially, the impedance matching for each resonator is a sensitive and plays an important role to improve transfer efficiency as well as delivery distance. In this study, we examined the improvement of transmission efficiency and properties for HTS and copper antennas, respectively, within 45 cm distance. Thus, we obtained improved transfer efficiency with HTS antenna over 15% compared with copper antenna. In addition, we achieved effective impedance matching conditions between HTS antenna and copper receiver at radio frequency (RF) power of 370 kHz.

• 한국전자파학회논문지
• /
• 제28권6호
• /
• pp.478-486
• /
• 2017

본 논문은 광대역 컨포멀 위상배열 안테나 빔형성 시 발생하는 조향오차를 보상하고, 목적하는 빔형성을 위한 알고리즘을 제안한다. 광대역 빔 조향을 위하여 본 연구에서는 TTD(True Time Delay) 방식을 채택하였으며, 긴 시간의 지연을 위하여 기판 회로상에 구현을 하였다. 빔 조향 오차의 원인은 배열 안테나 소자간의 상호간섭, 지연회로 기판의 분산 특성 및 디지털 제어에 의한 quantization 오차 등이 있다. 본 논문에서 TTD 회로의 분산 및 quantization 오차는 절대적인 지연시간보다 배열소자간의 상대적인 지연시간 차이를 최적화 하는 방향으로 분산 및 quantization 오차의 영향을 최소화하였다. 제안된 조향오차 보상기법을 2~4 GHz 대역의 컨포멀 위상배열 구조에 적용하여 측정값과 비교하여 그 타당성을 검증하였다.