• Analytical Science and Technology
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• v.32 no.2
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• pp.35-47
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• 2019

In this study, high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was employed to detect 26 antidiabetic compounds in adulterated dietary supplements using a simple, selective method. The work presented herein may help prevent incidents related to food adulteration and restrict the illegal food market. The best separation was obtained on a Shiseido Capcell Pak(R) C18 MG-II ($2.0mm{\times}100mm$, $3{\mu}m$), which improved the peak shape and MS detection sensitivity of the target compounds. A gradient elution system composed of 0.1 % (v/v) formic acid in distilled water and methanol at a flow rate of 0.3 mL/min for 18 min was utilized. A triple quadrupole mass spectrometer with an electrospray ionization source operated in the positive or negative mode was employed as the detector. The developed method was validated as follows: specificity was confirmed in the multiple reaction monitoring mode using the precursor and product ion pairs. For solid samples, LOD ranged from 0.16 to 20.00 ng/mL and LOQ ranged from 0.50 to 60.00 ng/mL, and for liquid samples, LOD ranged from 0.16 to 20.00 ng/mL and LOQ ranged from 0.50 to 60.00 ng/mL. Satisfactory linearity was obtained from calibration curves, with $R^2$ > 0.99. Both intra and inter-day precision were less than 13.19 %. Accuracies ranged from 80.69 to 118.81 % (intra/inter-day), with a stability of less than 14.88 %. Mean recovery was found to be 80.6-119.0 % and less than 13.4 % RSD. Using the validated method, glibenclamide and pioglitazone were simultaneously determined in one capsule at concentrations of 1.52 and 0.53 mg (per capsule), respectively.

• Journal of Korean Society for Atmospheric Environment
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• v.30 no.6
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• pp.545-554
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• 2014

In general, odorant was added to fuel gases, such as LPG, LNG and city gas, to prevent gas poisoning, ignition, explosion, or other accident caused by fuel gases, and to enable immediate and easy detection of fuel-gas leakage by emitting an offensive smell. This study describes a study on the exhaust emissions characteristics and fuel economy of liquefied petroleum gas (LPG) vehicle using LPG fuel with new sulfur free odorant. New sulfur free odorant was added to LPG to reduce sulfur content of the LPG. Its performance and exhaust emission were compared to those of LPG with sulfur containing odorant (EM, ethyl mercaptan). Engine performance using LPG with sulfur free odorant was similar to that with sulfur-containing odorant. Exhaust emissions from the LPG vehicle with LPG including sulfur free odorant were also similar to those with LPG including sulfur containing odorant in the FTP 75 and NEDC mode. There experimental results suggest that the sulfur free odorant may substitute for the sulfur containing odorant in LPG fuel.

• Earthquakes and Structures
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• v.11 no.3
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• pp.461-481
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• 2016

The research described in this paper investigates the seismic behaviour of lightly reinforced concrete (RC) bearing sandwich panels, heavily conditioned by shear deformation. A numerical model has been prepared, within an open source finite element (FE) platform, to simulate the experimental response of this emerging structural system, whose squat-type geometry affects performance and failure mode. Calibration of this equivalent mechanical model, consisting of a group of regularly spaced vertical elements in combination with a layer of nonlinear springs, which represent the cyclic behaviour of concrete and steel, has been conducted by means of a series of pseudo-static cyclic tests performed on single full-scale prototypes with or without openings. Both cantilevered and fixed-end shear walls have been analyzed. After validation, this numerical procedure, including cyclic-related mechanisms, such as buckling and subsequent slippage of reinforcing re-bars, as well as concrete crushing at the base of the wall, has been used to assess the capacity of two- and three-dimensional low- to mid-rise box-type buildings and, hence, to estimate their strength reduction factors, on the basis of conventional pushover analyses.

• The Journal of the Institute of Internet, Broadcasting and Communication
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• v.18 no.5
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• pp.97-102
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• 2018

In this paper, W-band Waveform Generator for compact radar has been designed and fabricated. DDS (Direct Digital Synthesizer) is applied to generate CW (Continuous Wave) and FMCW (Frequency Modulation Continuous Wave) waveform at high speed. We designed two LO (Local Oscillator) paths for functions of distance delay and distance tracking tests at the prpposed system without extra test equipment. Two mode selections are provided by switch. It is observed that fabricated waveform generator performs -91 dBc/Hz phase noise at offset 1 kHz and -63.2 dBc spurious. Proposed W-band Waveform Generator is expected to apply for W-band compact radar transceiver module.

• Journal of Hydrogen and New Energy
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• v.26 no.2
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• pp.184-191
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• 2015

As the power electronics system increases the frequency, the power loss and thermal management are paid more attention. This research presents a real time model of dissipation power with junction temperature response for 120kw IGBT inverter which is applied to the thermal management of high power IGBT inverter. Since the computational time is critical for real time simulation, look-up tables of IGBT module characteristic curve are implemented. The power loss from IGBT provides a clue to calculate the temperature of each module of IGBT. In this study, temperature of each layer in IGBT is predicted by lumped capacitance analysis of layers with convective heat transfer. The power loss and temperature of layers in IGBT is then communicated due to mutual dependence. In the dynamic model, PWM pulses are employed to calculation real time IGBT and diode power loss. Under Matlab/Simulink$^{(R)}$ environment, the dynamic model is validated with experiment. Results showed that the dynamic response of power loss is closely coupled with effective thermal management. The convective heat transfer is enough to achieve proper thermal management under guideline temperature.

• Smart Structures and Systems
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• v.26 no.1
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• pp.117-134
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• 2020

Over recent years, the interest for vegetables and fruits in all seasons and places has much increased, from where diverse countries have directed to the commercial production in greenhouse. In this article, we propose an algorithm based on wireless sensor network technologies that monitor the microclimate inside a greenhouse and linear equations model for optimization plant production and material cost. Moreover, we also suggest a novel design of an intelligent greenhouse. We validate our algorithms with simulations on a benchmark based on experimental data made at lNRA of Montfavet in France. Finally, we calculate the statistical estimators RMSE, TSSE, MAPE, EF and R². The results obtained are promising, which shows the efficiency of our proposed system.

• Proceedings of the KIPE Conference
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• 2003.07b
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• pp.860-865
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• 2003

Recently, SRMs are used in automobiles for power assistant steering, accessory motion control and traction drives. Especially in the motion control and traction drives, safety and efficiency are of paramount important. The paper describes the essential elements, faced in designing and constructing drive circuits for a switched reluctance motor for automobiles. These converters will be referred to as energy efficient C-dump converter and modified C-dump converter Energy efficient C-dump converter topology eliminate all the disadvantages of the C-dump converter without sacrificing its attractive features, and also provide some additional advantages that have lower number of power devices, full regenerative capability, free-wheeling in chopping or PWM mode, simple control strategy, and faster demagnetization during commutation. The experiments are peformed to verify the capability of proposed control method on 6/4 salient type SRM.

• Food Science and Biotechnology
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• v.18 no.1
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• pp.60-65
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• 2009

Near infrared reflectance spectroscopy (NIRS) was used as a rapid and non-destructive method to determine the protein content in intact and ground seeds of pea (Pisum sativum L.) germplasms grown in Korea. A total of 115 samples were scanned in the reflectance mode of a scanning monochromator at intact seed and flour condition, and the reference values for the protein content was measured by auto-Kjeldahl system. In the developed ground and intact NIRS equations for analysis of protein, the most accurate equation were obtained at 2, 8, 6, 1 math treatment conditions with standard normal variate and detrend scatter correction method and entire spectrum (400-2,500 nm) by using modified partial least squares regression (n=78). External validation (n=34) of these NIRS equations showed significant correlation between reference values and NIRS estimated values based on the standard error of prediction (SEP), $R^2$, and the ratio of standard deviation of reference data to SEP. Therefore, these ground and intact NIRS equations can be applicable and reliable for determination of protein content in pea seeds, and non-destructive NIRS method could be used as a mass analysis technique for selection of high protein pea in breeding program and for quality control in food industry.

• Journal of international Conference on Electrical Machines and Systems
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• v.1 no.1
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• pp.8-16
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• 2012

Fixed speed wind turbine generators system that uses induction generator as a wind generator has the stability problem similar to a synchronous generator. On the other hand, doubly fed induction generator (DFIG) has the flexibility to control its real and reactive powers independently while being operated in variable speed mode. This paper focuses on a scheme where IG is stabilized by using DFIG during grid fault. In that case, DFIG will be heavily stressed and a remedy should be found out to protect the frequency converter as well as to allow the independent control of real and reactive powers without loosing the synchronism. For that purpose, a crowbar protection switch or DC-link protecting device can be considered. This paper presents a comparative study between two protective schemes, a crowbar circuit connected across the rotor of the DFIG and a protective device connected in the DC-link circuit of the frequency converter. Simulation analysis by using PSCAD/EMTDC shows that both schemes could effectively protect the DFIG, but the latter scheme is superior to the former, because of less circuitry involved.

• Proceedings of the KSME Conference
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• 2000.04a
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• pp.831-836
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• 2000

During machining, since more than 50% compliance of the cutting point in machine tool structures comes from headstocks, with the remainder coming from beds, slides and structural joints, the structural analysis of the headstock is very important to improve the static and dynamic performances. Especially, in case of machining hard and brittle materials such as glasses and ceramics with the grinding machine, the reinforced headstock with the high damping material is demanded. Since the fiber reinforced composite materials have excellent properties for structures, owing to its high specific modulus, high damping and low thermal expansion, it is expected that the dynamic and thermal characteristics of the headstock will be improved if they are employed as the materials fur headstock. In this paper, the design and the manufacturing methods as well as the static and dynamic characteristics of a steel-composite hybrid headstock were investigated analytically and experimentally to improve the performance of the grinding machine system.