• Korean Journal of Veterinary Service
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• v.42 no.4
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• pp.289-296
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• 2019

A novel rapid procedure with liquid chromatography tandem mass spectrometry (LC-MS/MS) detection has been developed by changing various conditions including sample preparation such as QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) methodology. This work has been involved the optimization and validation of detection method for fluoroquinolones which are widespread used in livestock especially in the chicken. Five grams of homogenized chicken muscle were extracted with QuEChERS EN and acetonitrile containing 5% formic acid and cleaned with anhydrous magnesium sulfate and C₁₈ sorbent. The separation was performed on Acquity UPLC HSS T3 (2.1 mm×100 mm, 1.8 ㎛) column. The mobile phase A and B were composed of water containing 0.1% formic acid and acetonitrile containing 0.1% formic acid, respectively. Flow rate was 0.25 mL/min and column temperate was 40℃. LC-MS/MS with multiple reaction monitoring has been optimized for ten fluoroquinolones (ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, ofloxacin, orbifloxacin, pefloxacin and sarafloxacin). The method developed in this study has been presented good linearity with correlation coefficient (R²) of 0.9971~0.9998. LOD and LOQ values ranged from 0.09 to 0.76 ppb and from 0.26 to 2.29 ppb, respectively. The average recoveries were from 77.46 to 111.83% at spiked levels of 10.0 and 20.0 ㎍/kg. Relative standard deviation (%) ranged 1.28~11.90% on intra-day and 3.10~8.38 % on inter-day, respectively. This analysis method was applicable to the livestock residue laboratories and was expected to be satisfactory for the residue surveillance system.

• Geophysics and Geophysical Exploration
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• v.5 no.4
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• pp.309-315
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• 2002

Conventional electromagnetic (EM) method using small loops as a source and receiver has been used in detection of conductive buried objects like a metal detector or in qualitative estimation of the subsurface conductivity variation. Recently, however, since detection of buried objects and imaging of the subsurface conductivity distribution in a relatively conductive area are in a high demand for environmental and engineering purposes, the quantitative interpretation technique of EM data is actively studied. In this regard, we introduce a brief principle of EM survey and show an example of the detection of buried conductive material and imaging of the subsurface conductivity distribution based on data measured at a test survey area. Through this study, we show that multi-frequency EM surveys using small loops may be a good solution to give quick and detail information of subsurface in a conductive survey area.

• Journal of the Korea Institute of Information Security & Cryptology
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• v.25 no.1
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• pp.61-73
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• 2015

In order to respond quickly to security threats that are increasing fast and variously, security control personnel needs to understand the threat of a massive amount of logs generated from security devices such as firewalls and IDS. However, due to the limitations of the information processing capability of humans, it takes a lot of time to analyze the vast amount of security logs. As a result, there is problem that the detection and response of security threats are delayed. Visualization technique is an effective way to solve this problem. This paper visualizes the security log using the RGB Palette, offering a quick and effective way to know whether the security threat is occurred. And it was applied empirically in VAST Challenge 2012 dataset.

• Journal of Power Electronics
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• v.17 no.1
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• pp.56-66
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• 2017

Fast and accurate fault detection is the primary step and one of the most important tasks in fault tolerant converters. In this paper, a fast and simple method is proposed to detect and diagnosis the faulty cell in a cascaded H-bridge multilevel inverter under a short circuit fault. In this method, the reference voltage is calculated using switching control pulses and DC-Link voltages. The comparison result of the output voltage and the reference voltage is used in conjunction with active cell pulses to detect the faulty cell. To achieve this goal, the cell which is active when the Fault signal turns to "0" is detected as the faulty cell. Furthermore, consideration of generating the active cell pulses is completely described. Since the main advantage of this method is its simplicity, it can be easily implemented in a programmable digital device. Experimental results obtained with an 11-level inverter prototype confirm the effectiveness of the proposed fault detection technique. In addition, they show that the diagnosis method is unaffected by variations of the modulation index.

• Food Science of Animal Resources
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• v.40 no.3
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• pp.350-361
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• 2020

Quality control of meat products is one of the main concerns of consumers, governmental control authorities, and retailers. The purpose of this study was to employ ribose-induced Maillard reaction in detection of meat adulteration and differentiation of fresh-chilled from frozen-thawed minced veal. The browning intensity was assessed through measuring the absorbance at 420 nm with a spectrophotometer as well as the direct analysis of the color and pH. The results showed that CIE b*, CIE a*, and A_420* values in the extract of fresh-chilled veal were significantly (p<0.05) higher than frozen-thawed samples. The extract of frozen meat samples stored at -18℃ became significantly darker and more yellowish compared to -4℃. The results showed that the A_420* value in the frozen-thawed veal stored at -4℃ and -18℃ was reduced by approximately 17.22±3.53% and 11.68±2.49%, respectively, compared with fresh-chilled veal. The findings also showed that the storage temperature of minced veal and the heating time in this reaction had a significant effect on all tested variables (p<0.0001). The proposed method can be considered as an easy, quick, and inexpensive test for differentiating between the fresh-chilled and frozen-thawed minced veal.

• Journal of Korea Society of Industrial Information Systems
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• v.17 no.3
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• pp.35-42
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• 2012

The database for driving patterns can be utilized in various system such as automatic driving system, driver safety system, and it can be helpful to monitor driving style. Therefore, we propose a driving pattern recognition system in which the sensor streams from a smartphone are recorded and used for recognizing driving events. In this paper we focus on the driving pattern recognition that is an essential and preliminary step of driving style recognition. We divide input sensor streams into 7 driving patterns such as, Left-turn(L), U-turn(U), Right-turn(R), Rapid-Braking(RB), Quick-Start(QS), Rapid-Acceleration (RA), Speed-Bump(SB). To classify driving patterns, first, a preprocessing step for data smoothing is followed by an event detection step. Last the detected events are classified by DTW(Dynamic Time Warping) algorithm. For assisting drivers we provide the classified pattern with the corresponding video stream which is recorded with its sensor stream. The proposed system will play an essential role in the safety driving system or driving monitoring system.

• The Journal of the Institute of Internet, Broadcasting and Communication
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• v.16 no.1
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• pp.129-137
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• 2016

Transmission Control Protocol as a transport layer protocol provides steady data transfer service. There are some serious concerns about the performance of TCP over diverse networks. The vital concern in TCP network environment is congestion which may occur due to quick transmission rates or because of large number of new connections entering the network at the same time. Size of queues in routers grows thus resulting in packet drops. Retransmission of the dropped packets, and reduced throughput can prove costly. Explicit Congestion Notification (ECN) in conjunction with Active Queue Management mechanisms (AQM) such as Random early detection (RED) is used for packet marking rather than dropping. In IP packet header ECN bits can be added as a sign of congestion thus avoiding needless packet drops. The proposed ECN and AQM mechanism can be implemented with help of ns2 simulator and the performance can be tested on different TCP variants.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.39 no.3
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• pp.225-231
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• 2011

The satellite clock anomalies, one of the abnormal signal factors of the GPS satellites, can have a significant impact on the GPS measurements. However, it can be difficult to detect the anomalies of the satellites clock before the range of the satellites clock error becomes bigger than the range of the other factors, due to the measurement including error of the orbit, ionosphere delay, troposphere delay, multipath and receiver clock. In order to perform quick and accurate detection by minimization of critical range in anomalies of the satellites clock, this paper suggested a solution to detect precise anomalies of the satellites clock after application of carrier smoothing filter from measurement by dual-frequency and adjustment of errors which can be occurred by other factor and the receiver clock errors. The performance of the proposed method was confirmed by comparing to the satellite clock biases which are provided by IGS.

• Korean Journal of Veterinary Service
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• v.34 no.4
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• pp.429-439
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• 2011

This article described the comparison of a quick, easy, cheap, effective, rugged and safe (QuEChERS) sample preparation and the classical method established by National Veterinary Research and Quarantine Service (NVRQS) for the determination of pesticide residues in livestock products using GC-tandem mass spectrometry. The classical method by NVRQS used liquid-liquid partioning followed by evaporizing. The modified QuEChERS entailed extraction of 2 g sample with 15 ml acetonitrile containing 1% acetic acid followed by addition of 6 g anhydrous magnesium sulfate and 1.5 g sodium acetate. After centrifugation, 6 ml of the extract underwent a cleanup step (in a technique known as column-based solid phase extraction) using 400 mg each of $C_{18}$ and primary secondary amine sorbents plus 1,200 mg magnesium sulfate. The quantitation of individual pesticides by both methods was based on tissue standard calibration curves with a correlation coefficient in excess of 0.98 for the 24 pesticides. The detection limits by the classical method were ranged 1.3~5.0 ${\mu}g$/kg, with mean recoveries between 76.2% and 114.3% except aldrin (59.3%) and deltamethrin (63.6%). The detection limits by modified QuEChERS were ranged 0.3~6.2 ${\mu}g$/kg, with mean recoveries between 68.0% and 114.3% except dimethipin (152.6%), chlorfenvinphos (138.1%), 4,4-DDT (61.5%), aldrin (60.4%) and chinomethionate (30.3%).

• Korean Journal of Environmental Agriculture
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• v.30 no.3
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• pp.323-329
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• 2011

BACKGROUND: The conazoles, difenoconazole, diniconazole, hexaconazole, penconazole and tetraconazole are a large class of synthetic fungicides used extensively for foliage and seed treatments in agricultural crops. The extensive use of conazoles has brought concerns on the potentiality of environmental contamination and toxicity. Thus studies on the development of methods for monitoring the conazoles are required. METHODS AND RESULTS: A modified quick, easy, effective, rugged and safe (QuEChERS) method was involved in sample preparation. Quadrapole time of flight mass spectrometer (Q-TOF MS) in electron spray ionization (ESI) mode was employed to determine conazoles in garlic samples. The limit of detection (LOD) and limit of quantification (LOQ) of conazoles by Q-TOF-MS ranged from 0.001 to 0.002 mg/L and 0.002 to 0.005 mg/L, respectively. Q-TOF-MS analysis exhibited less than 2.6 ppm error of accurate mass measurements for the detection of conazoles spiked at 0.05 mg/L in garlic matrix. Recovery values of conazoles fortified in garlic samples at 0.02, 0.05 and 0.1 mg/L were between 79.2 and 106.2% with a maximum 11.8% of standard deviation. No detectable conazoles were found in the domestic market samples by using the Q-TOF-MS method. CONCLUSION(s): High degree of confirmation for conazoles by accurate mass measurements demonstrated that Q-TOF-MS analysis combined with a QuEChERS method may be applicable to simultaneous determination of conazoles in garlic samples.