• 대한금속재료학회지
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• 제47권11호
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• pp.694-698
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• 2009

The $Co_{3}Ti$ phase hardens appreciably by the fine precipitation of disordered fcc Co-rich phase upon aging after quenching from solution annealing temperature. Transmission electron microscope (TEM) observations revealed that the precipitates are platelet in shape, lying nearly parallel to the {100} planes of the $Ll_{2}$-ordered matrix, and perfectly coherent with the matrix lattice at the beginning of aging. The high temperature strength increases appreciably with the fine precipitation of disordered Co-rich phase over the whole temperature range investigated. TEM observations of the under-aged and deformed alloys revealed that superdislocations are pinned by precipitates indicating an attractive interaction between dislocations and precipitates. In the over-aged state, thin twins are introduced in the fcc Co-rich precipitates during deformation.

• 한국진공학회지
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• 제7권s1호
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• pp.1-6
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• 1998

The influence of the order-disorder structural transition on the magnetic and mageto-optical, and transport properties of Fe-Al and Co-Al alloy films has been investigated. The disordered states in the alloy films were prepared by vapor quenching deposition on glass substrates cooled by liquid nitrogen. The experimental study of the magento-optical properties of the ordered and disordered Fe-Al and Co-Al alloy films has been carried out in 1.05-5.0 eV energy range at room temperature. The transport properties have been measured in 2-300K temperature range with and without magnetic field of 0.5T. The influence of the order-disorder structural transition on the magnetic and magneto-optical properties was discussed by using the effective medium approximation and the structural defect approach. That on the temperature dependence of the resistivity was analyzed in a framework of the partial localization of the electronic states and the variable range hopping conductivity.

• 열처리공학회지
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• 제21권2호
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• pp.79-86
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• 2008

As a basic research for developing 600 MPa yield strength reinforcing steel bars, the strengthening of 0.25 wt.% carbon steel by vanadium addition was studied. The changes of microstructure and mechanical properties were investigated for the specimen V0 (0.00 wt.% V), V1 (0.03 wt.% V) and V2 (0.06 wt.% V) processed by various heat treatments. To set the heat treatment conditions, the continuous cooling transformation (CCT) curves were drawn for austenitizing temperatures of $900^{\circ}C$ and $1100^{\circ}C$. For specimens tempered at $600^{\circ}C$ after quenching from $900^{\circ}C$ and $1100^{\circ}C$, yield strength was increased by 19 MPa and 21 MPa for 0.01 wt % V addition, and tensile strength was increased by 25 MPa and 28 MPa for 0.01 wt % V addition, respectively. Also, for 0.06 wt.% V added specimens tempered after quenching and normalized, tensile strength was increased by 50 MPa and 30 MPa for increasing austenitizing temperature of $100^{\circ}C$, respectively.

• Bulletin of the Korean Chemical Society
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• 제30권9호
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• pp.1973-1977
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• 2009

In the present study, at first, 2,4-Dihydroxy Salophen (2,4-DHS), has been synthesized by combination of 1, 2-diaminobenzene and 2,4-dihydroxybenzaldehyde in a solvent system. This ligand containing meta-quinone functional groups were characterized using UV-Vis and IR spectroscopies. Subsequently, the interaction between native calf thymus deoxyribonucleic acid (ct-DNA) and 2,4-DHS, was investigated in 10 mM Tris/HCl buffer solution, pH 7.2, using UV-visible absorption and fluorescence spectroscopies, thermal denaturation technique and viscosity measurements. From spectrophotometric titration experiments, the binding constant of 2,4-DHS with ct-DNA was found to be (1.1 ${\pm}\;0.2)\;{\times}\;10^4\;M^{-1}.$ The fluorescence study represents the quenching effect of 2,4-DHS on bound ethidium bromide to DNA. The quenching process obeys linear Stern-Volmer equation in extended range of 2,4-DHS concentration. Thermal denaturation experiments represent the increasing of melting temperature of DNA (about 3.5 ${^{\circ}C}$) due to binding of 2,4-DHS. These results are consistent with a binding mode dominated by interactions with the groove of ct-DNA.

• 대한기계학회논문집A
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• 제24권4호
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• pp.858-865
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• 2000

It is well recently recognized that quench is one of the serious problems for the integrity of superconducting magnets, which is mainly attribute to the rapid temperature rising in the magnet due to some extrinsic factors such as conductor motion, crack initiation etc. In order to apply acoustic emission(AE)echnique effectively to monitor and diagnose superconducting magnets, it is essential to identify the sources of acoustic emission. In this paper, an acoustic emission technique has been used to monitor and diagnose quenching phenomenon in racetrack shaped superconducting magnets at cryogenic environment of 4.2K. For these purposes special attention was paid to detect AE signals associated with the quench of superconducting magnets. The characteristics of AE parameters have been analyzed by correlating with quench number, winding tension of superconducting coil and charge rate by transport current. In addition, the source location of quench in superconducting magnet was also discussed on the basis of correlation between magnet voltage and AE energy.

• 한국정밀공학회지
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• 제18권4호
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• pp.78-84
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• 2001

This study deals with the heat-treatment technique of SM45C steel with respect to less of deformation in control. The whole process for the production of landing gear must go through with uniformally controlled heat treatment, where as most deformation usually occur in nonuniform cooling environment. When a heated metal is submerged into a certain quenchant, the rate of cooling rapidity can be measured rather slow during the early stage of the procedure due to an Occurrence of a vapor blanked. As the additional course of cooling action is applied and the vapor from a vapor blanked is destroyed simultaneously, the speed of cooling promptness can be considered rather swift. The object of this study is to control the certain deformations as in the procedure of a heat treatment for landing gear by analyzing and improving the conditions of different substance of quenching liquids. Several noticeable curves indicating the temperature variation on the ap-plied metals during the cooling procedures, along with detectable rates of water verses oil and that of different polymer solutions are illustrated.

• 한국결정성장학회지
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• 제25권3호
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• pp.121-126
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• 2015

A novel $Ce^{3+}$ doped $Lu_3MgAl_3SiO_{12}$ phosphor ($Lu_{2.94}Ce_{0.06}MgAl_3SiO_{12}$) was successfully synthesized by a conventional solid-state reaction at $1450^{\circ}C$ for 5 h. The crystal structure of the synthesized phosphor powder was characterized by X-ray diffraction and Rietveld refinement. The prepared phosphor powder showed a broad peak at 550 nm, and the temperature dependence on photoluminescence properties of the prepared $Lu_{2.94}Ce_{0.06}MgAl_3SiO_{12}$ phosphor was investigated from 300 to 525 K. The activation energy for thermal quenching was determined by Arrhenius fitting. The experimental results clearly indicate that prepared $Lu_{2.94}Ce_{0.06}MgAl_3SiO_{12}$ phosphor has great potential for a down-conversion yellow phosphor in white light-emitting diodes.

• 한국해양공학회지
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• 제5권1호
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• pp.97-105
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• 1991

In this paper, the fatigue strength and the fatigue crack propagation behaviors of the round bar specimens which were spirally built up by welding and subsequently hardened by quenching were investigated. The material used was SF60 which was whdely employed in mechanical components, especially shafts. Fatigue tests were conducted at the fully reversed condition(R=-1) and axial and load control in the room temperature ahd air environment. The experimental results were expressed by both the range of stress intensity factor ($\Delta{K}$) and the effective range of stress intensity factor ($\Delta{K}_{eff}$). It was clarified that applying of quenching after the building up welding process improved the fatigue strength and the gatigue crack propagation property in the low range of $\Delta{K}$ of the built up round bar specimen.

• 소성∙가공
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• 제15권8호
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• pp.621-627
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• 2006

Recently, micro-alloyed steels which could eliminate heat treatments after forging has been developed. These non heat-treated micro-alloyed steels have several advantages over the conventional quenched and tempered steel for cold forging. First of all, long components can be fabricated with a better dimensional accuracy since bending of long forged part after quenching treatment could be avoided. And it is possible to eliminate two energy consuming heat treatment steps, which are a spherodizing before forging and quenching/tempering after forging. Therefore, more cost effective and environment friendly process could be designed. However, there is non-uniform distribution of strain occurred across the forged part, since these non heat-treated micro-alloyed steel use strain hardening mechanism. In the present study, it was investigated how to lessen non-uniformity and increase strength together for cold forging when a baking heat treatment is applied in micro-alloyed steels. For this purpose, micro-alloyed steels developed by Se-A Besteel recently was used for the experiment.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2008년도 추계학술대회A
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• pp.167-172
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• 2008

This study is to evaluate the fatigue crack growth characteristics for base metals and welded metal of 9% Ni steels. Since this material has very excellent fracture toughness at low temperature, it has been widely used for inner walls of LNG storage tank. These materials to compare fatigue crack growth (FCG) behaviour are treated with heat by the method of quenching and tempering (QT), and quenching, lamellarizing and tempering (QLT). FCG tests using compact temsion (CT) specimen under stress ratio R=0.1, 0.5, and constant load are carried out. K-increasing tests are conducted by the standard test method described in ASTM E 647. To investigate the effect of welded metal on the crack growth rate, the locations of notch tip were chosen at the center of welded metal and heat affected zone (HAZ). Form the results, FCG rate has almost same tendency according to stress ratio, base and welded metal, the locations of welded metal. FCG rate of welded metal is somewhat faster than base metal. Also scanning electron microscope (SEM) is used to observe the striation of the fractured surface after fatigue crack tests.